A new crystalline form of αβ-D-lactose prepared by oven drying a concentrated aqueous solution of D-lactose
2019 ◽
Vol 75
(7)
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pp. 904-909
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Keyword(s):
X Ray
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A new crystalline form of αβ-D-lactose (C12H22O11) has been prepared by the rapid drying of an approximately 40% w/v syrup of D-lactose. Initially identified from its novel powder X-ray diffraction pattern, the monoclinic crystal structure was solved from a microcrystal recovered from the generally polycrystalline mixed-phase residue obtained at the end of the drying step. This is the second crystalline form of αβ-D-lactose to be identified and it has a high degree of structural three-dimensional similarity to the previously identified triclinic form.
2011 ◽
Vol 396-398
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pp. 284-287
2007 ◽
Vol 63
(3)
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pp. i70-i72
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Vol 71
(4)
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pp. 330-337
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Vol 92
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pp. 1986-1992
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1996 ◽
Vol 51
(5)
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pp. 646-654
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Vol 71
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pp. 51-55
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