Non Isothermal Thermo Gravimetric Analysis (TGA) Measurements of Oxidative Aged Solid Insulation

2021 ◽  
Author(s):  
Sangineni Rohith ◽  
Deepak Kanumuri ◽  
Niharika Baruah ◽  
Sisir Kumar Nayak
Keyword(s):  
Thermo Gravimetric Analysis ◽  
Gravimetric Analysis ◽  
Thermo Gravimetric ◽  
Solid Insulation

Coordination Compounds of Some 3d-Transition Metal Ions with N1-[4-(4-bromo-phenylsulfonyl)-benzoyl]-N4-(4-methoxyphenyl)- thiosemicarbazide

2008 ◽  
Vol 59 (7) ◽  
Author(s):  
Madalina Angelusiu ◽  
Maria Negoiu ◽  
Stefania-Felicia Barbuceanu ◽  
Tudor Rosu
Keyword(s):  
Coordination Compounds ◽  
Magnetic Moments ◽  
Thermo Gravimetric Analysis ◽  
Electronic Spectroscopy ◽  
Transition Metal Ions ◽  
Synthesis And Characterization ◽  
Gravimetric Analysis ◽  
Thermo Gravimetric ◽  
New Compounds

The paper presents the synthesis and characterization of Cu(II), Co(II), Ni(II), Cd(II), Zn(II) and Hg(II) complexes with N1-[4-(4-bromo-phenylsulfonyl)-benzoyl]-N4-(4-methoxyphenyl)-thiosemicarbazide. The new compounds were characterized by IR, EPR, electronic spectroscopy, magnetic moments, thermo-gravimetric analysis and elemental analysis.

scholarly journals Development of Nervilia fordii Extract-Loaded Electrospun PVA/PVP Nanocomposite for Antioxidant Packaging

Foods ◽  
2021 ◽  
Vol 10 (8) ◽  
pp. 1728
Author(s):  
Peng Wen ◽  
Teng-Gen Hu ◽  
Yan Wen ◽  
Ke-Er Li ◽  
Wei-Peng Qiu ◽  
...  
Keyword(s):  
Food Packaging ◽  
Thermo Gravimetric Analysis ◽  
Xrd Analysis ◽  
Sem Analysis ◽  
Poly Vinyl Alcohol ◽  
Total Phenolic ◽  
Gravimetric Analysis ◽  
Thermo Gravimetric ◽  
Phenolic And Flavonoid ◽  
Thermal Stability Of

An ethyl acetate extract from of Nervilia fordii (NFE) with considerable suppression activity on lipid peroxidation (LPO) was first obtained with total phenolic and flavonoid contents and anti-LPO activity (IC50) of 86.67 ± 2.5 mg GAE/g sample, 334.56 ± 4.7 mg RE/g extract and 0.307 mg/mL, respectively. In order to improve its stability and expand its application in antioxidant packaging, the nano-encapsulation of NFE within poly(vinyl alcohol) (PVA) and polyvinyl(pyrrolidone) (PVP) bio-composite film was then successfully developed using electrospinning. SEM analysis revealed that the NFE-loaded fibers exhibited similar morphology to the neat PVA/PVP fibers with a bead-free and smooth morphology. The encapsulation efficiency of NFE was higher than 90% and the encapsulated NFE still retained its antioxidant capacity. Fourier transform infrared spectroscopy (FTIR) and X-ray powder diffraction (XRD) analysis confirmed the successful encapsulation of NFE into fibers and their compatibility, and the thermal stability of which was also improved due to the intermolecular interaction demonstrated by thermo gravimetric analysis (TGA). The ability to preserve the fish oil’s oxidation and extend its shelf-life was also demonstrated, suggesting the obtained PVA/PVP/NFE fiber mat has the potential as a promising antioxidant food packaging material.

The Experimental Study on Combustion Characteristics of Corn Straw and Coal Gangue

2011 ◽  
Vol 135-136 ◽  
pp. 1057-1059
Author(s):  
Heng Tao Zhou ◽  
Yong Wei
Keyword(s):  
Thermo Gravimetric Analysis ◽  
Combustion Characteristics ◽  
Combustion Characteristic ◽  
Gravimetric Analysis ◽  
Characteristic Parameters ◽  
Corn Straw ◽  
Kinetics Analysis ◽  
Thermo Gravimetric ◽  
Ignition Characteristic ◽  
Coal Residue

With a thermo gravimetric analysis apparatus combustion characteristics experiments of coal residue cornstalk and mixtures of them were done at 20 C/min heating rate. Then the combustion characteristic Parameters were obtained by above experiments. The c combustion activation energies were acquired by kinetics analysis. The results show those: the ignition characteristic and synthesis combustion characteristic of coal residue are bad. The ignition characteristic and synthesis combustion characteristic of cornstalk are better. The combustion characteristics of the mixture of coal residue and cornstalk are determined by mixing ratio. The ratio of cornstalk is more and the synthesis combustion characteristic is better.

Grafting of Chitosan: Structural, Thermal and Antimicrobial Properties

2019 ◽  
Vol 41 (2) ◽  
pp. 240-240
Author(s):  
Nevin Cankaya Nevin Cankaya
Keyword(s):  
Antimicrobial Activity ◽  
Graft Copolymers ◽  
Thermo Gravimetric Analysis ◽  
Antimicrobial Properties ◽  
Gravimetric Analysis ◽  
Analysis Method ◽  
Methacryloyl Chloride ◽  
Thermo Gravimetric ◽  
Thermal Stabilities ◽  
Ft Ir

In this study, some new chitosan materials were synthesized by the grafting of chitosan with the monomers such as 1-vinylimidazole (VIM), methacrylamide (MAm) and 2-acrylamido-2-methyl-1-propanesulfonic acid (AMPS). First of all, chitosan methacrylate was prepared by esterification of primary -OH group with methacryloyl chloride a 25.13% yield by mole. The monomers were grafted into chitosan methacrylate via free radical polymerization using 2,2and#39;-Azobisisobutyronitrile as an initiator in N,N-dimethylformamide. The graft copolymers were characterized by FT-IR spectra and elemental analysis. Thermal stabilities of the graft copolymers were determined by TGA (thermo gravimetric analysis) method. The synthesized chitosan methacrylate and its graft copolymers were tested for their antimicrobial activity against bacteria and yeast.

Functionalization of α-ZrP by 1,2-Epoxypropane for Further Modification

2017 ◽  
Vol 898 ◽  
pp. 2347-2353
Author(s):  
Ahmed Hossamaldin ◽  
Ping Liu ◽  
Ya Du ◽  
Xiao Ze Jiang ◽  
Bin Sun ◽  
...  
Keyword(s):  
Epoxy Group ◽  
Thermo Gravimetric Analysis ◽  
Mas Nmr ◽  
Interlayer Distance ◽  
Gravimetric Analysis ◽  
Thermo Gravimetric ◽  
Grafting Ratio ◽  
Internal Surfaces ◽  
Carbon Mass ◽  
Ft Ir

To prepare alpha zirconium phosphate (α-ZrP) with high interlayer distance, grafting ratio and thermal stability, 1,2-epoxypropane was used to modify α-ZrP as the epoxy group reacting with P-OH on the external and internal surfaces of α-ZrP to form P-O-C bonds after small amines pre-intercalation. Different characterization techniques were used, including X-ray Powder Diffraction (XRD), Fourier Transform Infrared Spectroscopy (FT-IR), Thermo-Gravimetric Analysis (TGA) and Carbon Mass Nuclear Magnetic Resonance (13C MAS NMR). The results of XRD confirmed the pre-intercalation of amino-propane and the intercalation of 1,2-epoxypropane, as the interlayer distance increased from 7.5 Å to 16.9 Å and 15.3 Å, respectively. FT-IR and 13C MAS NMR results confirmed the formation of P-O-C bonds between 1,2-epoxypropane and α-ZrP. TGA analysis showed that the grafting ratio of 1,2-epoxypropane was 19.44%.

Enhancement of Thermo-Oxidative Stability of Vegetable Oil Based Lubricant via Chemical Modification Techniques

2015 ◽  
Vol 813-814 ◽  
pp. 695-699
Author(s):  
S. Arumugam ◽  
G. Sriram ◽  
A. Hemanth Sai Kumar Chowdary ◽  
Janga Subramanya Sai
Keyword(s):  
Chemical Modification ◽  
Oxidative Stability ◽  
Vegetable Oils ◽  
Rapeseed Oil ◽  
Chemical Structure ◽  
Thermo Gravimetric Analysis ◽  
Gravimetric Analysis ◽  
Thermo Gravimetric ◽  
Transesterification Method ◽  
Unique Chemical

The rising demand for environmentally acceptable lubricant has led researchers to look to vegetable oils as an alternative to petroleum based lubricants. Vegetable oils have radically distinctive properties owing to their unique chemical structure which have greater ability to lubricate and have higher biodegradability. In spite of advantages, they are limited to inadequate thermo-oxidative stability and poor low-temperature properties which hinder their utilization. In the present study in order to produce a bio lubricant with good thermo-oxidative stability, rapeseed oil was subjected to two different chemical modification techniques viz., epoxidation method and successive transesterification method. The thermo-oxidative stability of formulated oil was analysed using Thermo Gravimetric Analysis (TGA). TGA analysis divulges that the thermo-oxidative stability of rapeseed oil was greatly improved with the epoxidation method in comparison with the successive transesterification method.

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