Effect of Heat Treatment Schedules and Glass Powder Particle Size on Glass Infiltration in Porous Alumina Preforms

2013 ◽  
Vol 11 (3) ◽  
pp. 543-549
Author(s):  
Preeti Bajpai ◽  
Parag Bhargava
2011 ◽  
Vol 278 ◽  
pp. 265-270 ◽  
Author(s):  
J.R. May ◽  
M.C. Hardy ◽  
M.R. Bache ◽  
David D. Kaylor

This study evaluates the suitability of as-hot isostatically pressed (HIP) RR1000 for non-critical applications in aero-engine components. RR1000, an advanced powder nickel-based superalloy, was developed for disc rotor components in aero-engines. For these critical applications, the consolidated alloy powder particles are extruded to break down carbide and oxide networks, known as prior particle boundaries (PPBs), and to refine the structure into a fine grain size for isothermal forging. In this study, hot isostatically pressed compacts, made from two different powder particle size fractions have been assessed following heat treatments below and above the gamma prime solvus temperature. A microstructural evaluation shows a greater degree of PPB decoration occurs in the finer powder particle size fraction. Following a super-solvus heat treatment these PPBs pin grain boundaries of the fine powder particle size compacts, whilst the reduction of PPB decoration in coarse powder particle compacts allows significant grain growth. Tensile test results of as-HIP RR1000 show, good yield strengths, ultimate tensile strengths and ductility, which are comparable with extruded and isothermal forged RR1000 disc material. Dwell crack propagation tests show that finer powder particle size compacts, which have received a sub-solvus heat treatment, give the highest crack growth rates; whilst the remaining material conditions show markedly improved crack growth resistance. In conclusion, as-HIP RR1000 demonstrates clear potential for use in non-critical applications, employing either powder particle size fraction used in this study subject to the appropriate solution heat treatment.


2021 ◽  
Vol 13 (19) ◽  
pp. 10618
Author(s):  
Da Huang ◽  
Pengliang Sun ◽  
Pengfei Gao ◽  
Guangyan Liu ◽  
Yuanhao Wang ◽  
...  

The suppression of ASR expansion hazards of glass concrete has always been a key and hot issue in the research of glass concrete. According to the ASTM C1260-14 fast mortar rod method, glass sand and glass powder act as fine aggregate and auxiliary cementing material, respectively. The changes in expansion rate with different amounts of glass sand content and different particle sizes of glass powder in mortar rods were compared, and the effects of glass sand content and the glass powder particle size on the expansion of ASR were analyzed. SEM was used to compare and analyze the microstructure of mortar rods to explore the mechanism of ASR expansion of glass concrete, and the results showed that the addition of glass powder had a certain inhibitory effect on ASR expansion. The larger the particle size of glass powder was, the better the inhibition effect on ASR expansion and the longer its duration. Compared with the three groups of experiments of 0–13 μm, 13–38 μm, and 38–75 μm, it was found that the influence of the glass powder particle size on the expansion of ASR was weaker than that of dosage. The inhibitory effect of glass powder on ASR expansion is related to the fact that glass powder is more involved in pozzolanic reaction in the early hydration process.


2014 ◽  
Vol 936 ◽  
pp. 1694-1700
Author(s):  
Zhi Wei Li ◽  
Kai Yong Jiang ◽  
Fei Wang ◽  
Ji Liang Zhang

This paper mainly introduces the mechanism of microwave heating: electric conduction loss, eddy current loss and arc discharge. The microwave heating behavior of 316 stainless steel powder body which made by gel casting was investigated in the paper. Experiments on different microwave power, powder particle size, and the content of auxiliary heating material showed that the smaller the powder particle size, the larger microwave power and auxiliary heating materials help 316 stainless steel body for sintering.


2014 ◽  
Vol 46 (3) ◽  
pp. 365-375
Author(s):  
N. Labus ◽  
S. Mentus ◽  
Z.Z. Djuric ◽  
M.V. Nikolic

The influence of air and nitrogen atmosphere during heating on TiO2 nano and micro sized powders as well as sintered polycrystalline specimens was analyzed. Sintering of TiO2 nano and micro powders in air atmosphere was monitored in a dilatometer. Non compacted nano and micro powders were analyzed separately in air and nitrogen atmospheres during heating using thermo gravimetric (TG) and differential thermal analysis (DTA). The anatase to rutile phase transition temperature interval is influenced by the powder particle size and atmosphere change. At lower temperatures for nano TiO2 powder a second order phase transition was detected by both thermal techniques. Polycrystalline specimens obtained by sintering from nano powders were reheated in the dilatometer in nitrogen and air atmosphere, and their shrinkage is found to be different. Powder particle size influence, as well as the air and nitrogen atmosphere influence was discussed.


2021 ◽  
Vol 19 (10) ◽  
pp. 106-114
Author(s):  
Hani M Hussien

The polymer composites used in the present study were made of polyvinyl alcohol (PVA) as a matrix and glass powder as a filler. The glass powder was obtained from fluorescent tubes waste. The solution casting method was used to fabricate PVA/glass powder composite. Three groups of samples were prepared. The first was prepared by using PVA with the addition of glass powder (sieved less than 20 μm) in proportions 10, 20, 30, 40, and 50 %. The second: the mixing ratios of PVA and glass powder were 80% and 20%, respectively. The third: The mixing ratios of PVA and glass powder were 60% and 40%, respectively. In Both previous groups, the added glass powder used was sieved with sizes less than 20, 45, 105, and 125 μm. For all samples, the following properties were measured at room temperature: DC electrical conductivity, dielectric constant, electrical conductivity, and dissipation factor. The last three properties were measured with a range of frequencies from 1kHz to 5MHz. DC conductivity increases with increasing of glass powder. It was found that the highest conductivity values are for samples composed of glass powder with a particle size of less than 45 μm for both ratios of glass 20% and 40%. It is also noticed that within most frequencies, the sample with 30% glass has the largest dissipation factor. At 20% filler of glass powder, it is noted that the highest values of the dielectric constant are for samples composed of glass powder with a particle size of less than 45 μm and 125 μm. Below 1 MHz, the effect of glass powder particle size on the AC conductivity is minimal. It is found that the samples containing glass powder (less than 125 μm and 105 μm), have similar and lowest dissipation factor. At 40% filler of glass powder, it is noted that the lowest values of the dielectric constant are for samples composed of glass powder with a particle size little than 105 μm.


2016 ◽  
Vol 43 (2) ◽  
pp. 0203007
Author(s):  
闫岸如 Yan Anru ◽  
杨恬恬 Yang Tiantian ◽  
王燕灵 Wang Yanling ◽  
马志红 Ma Zhihong ◽  
杜云 Du Yun ◽  
...  

2020 ◽  
Vol 989 ◽  
pp. 816-820
Author(s):  
Roman Sergeevich Khmyrov ◽  
R.R. Ableyeva ◽  
Tatiana Vasilievna Tarasova ◽  
A.V. Gusarov

Mass transfer in the laser-interaction zone at selective laser melting influences the quality of the obtained material. Powder particles displacement during the formation of the single bead is experimentally studied. The so-called denudated zone was visualized by metallography. It was determined that increasing the powder particle size leads to widening the denudated zone. This can signify that the adhesion forces between powder particles prevail over the friction forces.


2020 ◽  
Vol 364 ◽  
pp. 115-122 ◽  
Author(s):  
Annika Linke ◽  
Jörg Hinrichs ◽  
Reinhard Kohlus

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