scholarly journals Deposition of ultrasonic nebulized aerosols onto a hydrophilic surface

2020 ◽  
Vol 16 (3) ◽  
pp. 258-263
Author(s):  
Kusdianto Kusdianto ◽  
Masao Gen ◽  
Mitsuki Wada ◽  
Sugeng Winardi ◽  
I Wuled Lenggoro
Keyword(s):  
Raman Spectroscopy ◽  
Metallic Substrate ◽  
Hydrophilic Surface ◽  
Analysis Method ◽  
Model Surface ◽  
X Ray ◽  
Treated Area ◽  
Untreated Area ◽  
Electron Microscope Image ◽  
Pressure Analysis

The effect of chemical treatment of a metallic substrate on the deposition of aerosols generated by an ultrasonic nebulizer was investigated. A single substrate with areas having different “level” of hydrophilicity (or hydrophobicity) was used as a model surface. The treated (more hydrophilic) area became more negatively-charged based on a surface electric potential meter. A low-pressure analysis method (electron-microscope image) and ordinary pressure methods (Raman spectroscopy and X-ray fluorescence) analytical results indicated that in comparison with the untreated area, the treated area trapped more particles in the case of the deposition of “wet” aerosols. In the case of the deposition of more “dry” aerosols, the untreated area trapped more particles rather than that of the treated one. The efficiency of particles deposition not only depended on the degree of hydrophilicity (or hydrophobicity) of the surface but also due to the conditions (wet or dry) of incoming aerosols.

Raman spectroscopy and X-ray diffraction of lithium niobate at temperatures up to 1300○-4.80pt○C

2005 ◽  
Vol 126 ◽  
pp. 101-105 ◽  
Author(s):  
B. Moulin ◽  
L. Hennet ◽  
D. Thiaudière ◽  
P. Melin ◽  
P. Simon
Keyword(s):  
Raman Spectroscopy ◽  
Lithium Niobate ◽  
X Ray Diffraction ◽  
X Ray

Application of Cross-correlation Analysis Method for Measurement of the Fluid Flow Rate Based on X-ray Radiation

2019 ◽  
Vol 11 (1) ◽  
pp. 01025-1-01025-5 ◽  
Author(s):  
N. A. Borodulya ◽  
◽  
R. O. Rezaev ◽  
S. G. Chistyakov ◽  
E. I. Smirnova ◽  
...  
Keyword(s):  
Fluid Flow ◽  
Correlation Analysis ◽  
Flow Rate ◽  
Cross Correlation ◽  
Fluid Flow Rate ◽  
Analysis Method ◽  
X Ray ◽  
Cross Correlation Analysis ◽  
Correlation Analysis Method

The crystal and molecular structure of tris(pentamethylenedithiocarbamate) chromium(III)-chloroform (1 : 2)

1981 ◽  
Vol 46 (1) ◽  
pp. 6-19 ◽  
Author(s):  
Viktor Kettman ◽  
Ján Garaj ◽  
Jaroslav Majer
Keyword(s):  
Molecular Structure ◽  
Structural Analysis ◽  
Crystal And Molecular Structure ◽  
Analysis Method ◽  
Complex Molecules ◽  
Coordination Polyhedra ◽  
X Ray ◽  
Cell Dimensions ◽  
Crustal Density ◽  
Unit Cell Dimensions

The crystal and molecular structure of [Cr(S2CN(CH2)5)3].2 CHCl3 was found by the X-ray structural analysis method. The value R 0.090 was found for 1 131 observed independent reflections. The substance crystallizes in a space group of symmetry P212121 with the following unit cell dimensions: a = 0.8675 (6), b = 1.815(2), c = 2.155(3) nm. The experimentally observed crustal density was 1.48 Mgm-3 and the value calculated for Z = 4 was 1.51 Mgm-3. The CrS6 coordination polyhedron has the shape of a trigonally distorted octahedron, where the D3 symmetry is a approximately retained. The degree of trigonal distortion expressed as the projection of the chelate S-Cr-S angle onto the plane perpendicular to the C3 pseudo axis is Φ = 41.7° (Φ = 60° for an octahedron). The skeleton of the structure formed by the complex molecules contains channels filled with chloroform molecules. The specific type of complex-chloroform interaction consists of the formation of hydrogen bonds of the chloroform protons with the fully occupied pπ-orbitals of the sulphur atoms in the coordination polyhedra. The low stability and crystal decomposition can be explained by loss of chloroform from the channels.

scholarly journals Use of WetSEM® capsules for convenient multimodal scanning electron microscopy, energy dispersive X-ray analysis, and micro Raman spectroscopy characterisation of technetium oxides

2021 ◽  
Author(s):  
D. J. Bailey ◽  
M. C. Stennett ◽  
J. Heo ◽  
N. C. Hyatt
Keyword(s):  
Raman Spectroscopy ◽  
Low Cost ◽  
Powder Materials ◽  
Spectroscopy Analysis ◽  
X Ray ◽  
Micro Raman Spectroscopy ◽  
Hazard And Risk ◽  
Sem Imaging ◽  
General User ◽  
532 Nm

AbstractSEM–EDX and Raman spectroscopy analysis of radioactive compounds is often restricted to dedicated instrumentation, within radiological working areas, to manage the hazard and risk of contamination. Here, we demonstrate application of WetSEM® capsules for containment of technetium powder materials, enabling routine multimodal characterisation with general user instrumentation, outside of a controlled radiological working area. The electron transparent membrane of WetSEM® capsules enables SEM imaging of submicron non-conducting technetium powders and acquisition of Tc Lα X-ray emission, using a low cost desktop SEM–EDX system, as well as acquisition of good quality μ-Raman spectra using a 532 nm laser.

Silver oxide model surface improves computational simulation of surface-enhanced Raman spectroscopy on silver nanoparticles

2021 ◽  
Author(s):  
Scott G. Harroun ◽  
Yaoting Zhang ◽  
Tzu-Heng Chen ◽  
Huan-Tsung Chang ◽  
Alexis Vallée-Bélisle
Keyword(s):  
Raman Spectroscopy ◽  
Silver Nanoparticles ◽  
Silver Oxide ◽  
Accurate Result ◽  
Computational Simulation ◽  
Surface Enhanced Raman Spectroscopy ◽  
Model Surface ◽  
Surface Enhanced ◽  
Model Surfaces ◽  
Surface Enhanced Raman

For simulation of SERS on silver nanoparticles, Ag2O can provide a more accurate result than standard model surfaces such as Ag+, Ag, Ag4+ and Ag4.

scholarly journals Structural and Raman Vibrational Studies ofCeO2-Bi2O3Oxide System

2009 ◽  
Vol 2009 ◽  
pp. 1-4 ◽  
Author(s):  
L. Bourja ◽  
B. Bakiz ◽  
A. Benlhachemi ◽  
M. Ezahri ◽  
J. C. Valmalette ◽  
...  
Keyword(s):  
Solid Solution ◽  
Raman Spectroscopy ◽  
Phase Changes ◽  
Phase System ◽  
X Ray Diffraction ◽  
X Ray ◽  
Vibrational Studies ◽  
Coprecipitation Route

A series of ceramics samples belonging to theCeO2-Bi2O3phase system have been prepared via a coprecipitation route. The crystallized phases were obtained by heating the solid precursors at600∘Cfor 6 hours, then quenching the samples. X-ray diffraction analyses show that forx<0.20a solid solutionCe1−xBixO2−x/2with fluorine structure is formed. For x ranging between 0.25 and 0.7, a tetragonalβ′phase coexisting with the FCC solid solution is observed. For x ranging between 0.8 and 0.9, a new tetragonalβphase appears. Theβ′phase is postulated to be a superstructure of theβphase. Finally, close tox=1, the classical monoclinicα Bi2O3structure is observed. Raman spectroscopy confirms the existence of the phase changes as x varies between 0 and 1.

scholarly journals Plasma Fabrication and SERS Functionality of Gold Crowned Silicon Submicrometer Pillars

Materials ◽  
2020 ◽  
Vol 13 (5) ◽  
pp. 1244 ◽  
Author(s):  
Paola Pellacani ◽  
Carlo Morasso ◽  
Silvia Picciolini ◽  
Dario Gallach ◽  
Lucia Fornasari ◽  
...  
Keyword(s):  
Raman Spectroscopy ◽  
Surface Enhanced Raman Spectroscopy ◽  
Post Processing ◽  
Advanced Material ◽  
X Ray ◽  
Colloidal Monolayer ◽  
Surface Enhanced ◽  
Surface Enhanced Raman ◽  
Lift Off ◽  
X Ray Absorption

Sequential plasma processes combined with specific lithographic methods allow for the fabrication of advanced material structures. In the present work, we used self-assembled colloidal monolayers as lithographic structures for the conformation of ordered Si submicrometer pillars by reactive ion etching. We explored different discharge conditions to optimize the Si pillar geometry. Selected structures were further decorated with gold by conventional sputtering, prior to colloidal monolayer lift-off. The resulting structures consist of a gold crown, that is, a cylindrical coating on the edge of the Si pillar and a cavity on top. We analysed the Au structures in terms of electronic properties by using X-ray absorption spectroscopy (XAS) prior to and after post-processing with thermal annealing at 300 °C and/or interaction with a gold etchant solution (KI). The angular dependent analysis of the plasmonic properties was studied with Fourier transformed UV-vis measurements. Certain conditions were selected to perform a surface enhanced Raman spectroscopy (SERS) evaluation of these platforms with two model dyes, prior to confirming the potential interest for a well-resolved analysis of filtered blood plasma.

X-ray Raman Spectroscopy of Carbon in Asphaltene:  Light Element Characterization with Bulk Sensitivity

2000 ◽  
Vol 72 (11) ◽  
pp. 2609-2612 ◽  
Author(s):  
Uwe Bergmann ◽  
Oliver C. Mullins ◽  
S. P. Cramer
Keyword(s):  
Raman Spectroscopy ◽  
Light Element ◽  
X Ray
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