scholarly journals Nitrogen Tailored Activated Carbon via Microwave Synthesis Method for High Removal of Hydrogen Sulfide

2021 ◽  
Vol 17 (6) ◽  
pp. 794-604
Author(s):  
Norhusna Mohamad Nor ◽  
Lau Lee Chung ◽  
Abdul Rahman Mohamed

In this work, commercialized palm shell activated carbon was modified into nitrogen-functionalized carbon via urea impregnation method, followed by heat treatment via microwave irradiation at 950 °C.

2018 ◽  
Vol 280 ◽  
pp. 315-322
Author(s):  
N. Mohammad Nor ◽  
L. L. Chung ◽  
Bassim H. Hameed ◽  
S. Sethupathi ◽  
A. R. Mohamed

This research work is focuses on understanding the characteristics of modified nitrogen-enriched palm shell activated carbon (N-PSAC) that undergo different microwave (MW) operating parameters towards efficient H2S removal. The nitrogen functional groups were tailored onto PSAC micropore structures through impregnation of urea onto palm shell activated carbon (PSAC). The effect of MW heating variables (heating temperature, N2 flow rate, heating time and amount of adsorbent) on N-PSAC adsorbent was investigated and analyzed with respect to H2S adsorption capacity.One factor at a time (OFAT) approach was used to produce an efficient N-PSAC adsorbent, where theH2S breakthrough capacity (measured at 5% of H2S outlet concentration) attained was in the range of 98.71 – 211.35 mg/g.It was found that MW heating variables contribute a significant impactto the modification of N-PSAC adsorbent in catering the H2S emission.


2020 ◽  
Vol 10 (6) ◽  
pp. 849-859
Author(s):  
Radwa A. El-Salamony ◽  
Abeer A. Emam ◽  
Nagwa A. Badawy ◽  
Sara F. El-Morsi

Objective: ZnO nanoparticles were synthesized using wet impregnation method, and activated carbon from rice straw (RS) prepared through chemical route. Methods: The nano-composites ZnO-AC series were prepared with different ZnO:AC ratio of 10, 20, 50, and 70% to optimize the zinc oxide nanoparticles used. The obtained composites were characterized by FE-SEM, XRD, SBET, and optical techniques then used for the photo-degradation of Malachite green dye (MG) under visible light. Results: It was found that 10ZnO-AC exhibited excellent visible light photo-catalytic performance. The ·OH radicals’ formation is matching with photo-activity of the prepared composites. The photo-degradation efficiency of MG increased from 63% to 93%, when the 10ZnO-AC photocatalyst amount was increased from 0.5 to 6 g/L. Conclusion: The GC-MS technique was used to analyze the intermediates formed; up to 15 kinds of chemicals were identified as the degradation products.


2021 ◽  
pp. 125995
Author(s):  
So Yeon Yoon ◽  
Seok Byum Jang ◽  
Kien Tiek Wong ◽  
Hyeseong Kim ◽  
Min Ji Kim ◽  
...  

RSC Advances ◽  
2014 ◽  
Vol 4 (60) ◽  
pp. 31851-31854 ◽  
Author(s):  
Kaliyappan Karthikeyan ◽  
Yun Sung Lee

LiMnBO3 nanobeads (LMB-NB) prepared using a urea assisted microwave irradiation method delivered 67 mA h g−1 capacity at 0.6 C rate between 1.25 and 4.8 V, showing 88% cyclability after 100 cycles.


2011 ◽  
Vol 65 (9) ◽  
pp. 1423-1426 ◽  
Author(s):  
José Miguel González-Domínguez ◽  
Carmen Fernández-González ◽  
María Alexandre-Franco ◽  
Alejandro Ansón-Casaos ◽  
Vicente Gómez-Serrano

1960 ◽  
Vol 86 (6) ◽  
pp. 1-26
Author(s):  
R. S. Murphy ◽  
I. W. Santry

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