High Cycle Fatigue Properties of Modified 9Cr-1Mo Steel at Elevated Temperatures

Author(s):  
Yoshiaki Matsumori ◽  
Jumpei Nemoto ◽  
Yuji Ichikawa ◽  
Isamu Nonaka ◽  
Hideo Miura

Since high-cycle fatigue loads is applied to the pipes in various energy and chemical plants due to the vibration and frequent temperature change of fluid in the pipes, the high-cycle fatigue behavior of the alloys used for pipes should be understood quantitatively in the structural reliability design of the pipes. The purpose of this study, therefore, is to clarify the high-cycle fatigue strength and fracture mechanism of the modified 9Cr-1Mo steel at temperatures higher than 400°C. This material is one of the effective candidates for the pipes in fast breeder demonstration reactor systems. A rotating bending fatigue test was applied to samples at 50 Hz in air. The stress waveform was sinusoidal and the stress ratio was fixed at −1. The fatigue limit was observed at room temperature and it was about 420 MPa. This value was lower than the 0.2% proof stress of this alloy by about 60 MPa. This decrease can be attributed to the cyclic softening of this material. The limited cycles at knee point was about 8×105 cycles. All fracture was initiated from a single surface crack and no inclusion-induced fracture was observed in the fracture surface by SEM. Thus, the high-cycle fatigue design based on the fatigue limit may be applicable to the modified 9Cr-1Mo steel at room temperature. The fatigue limit of about 350 MPa was also observed at 400°C, and it appeared at about 107 cycles, while it appeared at around 106 cycles at room temperature. Thus, it was confirmed that the fatigue strength of this alloy decrease with temperature. However, the fatigue limit didn’t appear at 550°C up to 108 cycles. The fatigue limit may disappear in this alloy at 550°C. It is very important, therefore, to evaluate the ultra-high cycle fatigue strength of this alloy at temperatures higher than 400°C.

Author(s):  
Motoyuki Ochi ◽  
Ken Suzuki ◽  
Isamu Nonaka ◽  
Hideo Miura

In order to clarify the characteristics of high-cycle fatigue of the modified 9Cr-1Mo steel, a high temperature rotary bending test was carried out. As a result, the fatigue strength of this alloy decreased monotonically at elevated temperatures. It decreased from 440 MPa at room temperature to about 350 MPa at 400°C. This decrease of the fatigue strength was attributed to the temperature dependence of the yielding strength of this alloy. The fatigue limit appeared near 107 cycles at 400°C, whereas it appeared around 106 cycles at room temperature. The most important result is that the fatigue limit disappeared up to 108 cycles at temperatures higher than 500°C. Thus, the number of cycles at which the fatigue limit appeared shifted to higher cycles with increasing the testing temperature. Clear striation was observed in the stable crack growth region on the fracture surface of all the specimen tested at room temperature, 400°C, 500°C, 550°C, and 600°C. Intergranular cracking, which have been observed in creep-fatigue tests, was not observed. Since the estimated operating temperature of FBR is 550°C, it is very important to consider this fatigue strength in the structural and reliability design of the modified 9Cr-1Mo steel. In this study, the change of crystallinity of this alloy under fatigue loading was also analyzed by applying an EBSD method. The image quality (IQ) value obtained from the analysis was used for the quantitative evaluation of the crystallinity in the area where an electron beam of 20 nm in diameter was irradiated. The quality of the atomic alignment was found to degrade under the cyclic loading, and a crack started to occur on the surface of the alloy when the quality of the atomic alignment decreased to a certain critical value.


Author(s):  
Mohammad Bagher Limooei ◽  
Morteza Zandrahimi ◽  
Ramin Ebrahimi

In the present work, equal channel angular pressing of commercial pure aluminum 1070 was performed up to 4 passes using route Bc. For equal channel angular pressing operation, a suitable die set was designed and manufactured. X-ray diffraction analysis was used to determine the microstructure of the equal channel angular pressing-ed material. The fracture surface morphology and microstructure after fatigue were investigated by scanning electron microscopy. Mechanical properties of the equal channel angular pressing-ed material were evaluated by hardness and tension tests. Also, cyclic deformation behavior of severe plastic deformation Al1070 has been studied and results show a significant variation in hardness, ultimate strength and fatigue properties in high cycle fatigue life. Coefficient of fatigue strength σ′f and Bridgman correction factor have been obtained by S-N curve and tension test specimens, respectively, and compared before and after equal channel angular pressing process. Also an useful relation has been derived between fatigue life ( Nf) and stress amplitude ( σa) in high cycle fatigue region. Results indicated that there was not clear relation between fatigue strength coefficient and true corrected fracture stress in this case.


2008 ◽  
Vol 378-379 ◽  
pp. 131-146 ◽  
Author(s):  
Yoshiharu Mutoh ◽  
M. Shahnewaz Bhuiyan ◽  
Zainuddin Sajuri

The high cycle fatigue characteristics of magnesium alloys under low humidity, high humidity (80% RH) and sprayed 5%NaCl solution environments have been introduced. Fatigue limit of bulk magnesium alloy was significantly reduced even under high humidity condition, while other structural materials such as steel and aluminum alloy showed no influence of humidity on fatigue limit. The reduction of fatigue limit under 5% NaCl environments was much larger than that under high humidity environment. The remarkable reduction of fatigue limit under corrosive environments was attributed to the formation of corrosion pit, which was induced by simultaneous action of mechanical loading and corrosive environment. To improve the reduced fatigue strength under corrosive environment, coating used to apply on the surface. Non-chromium chemical conversion coating showed superior effect on the improvement of fatigue strength under corrosive environment compared to anodized coating. Fatigue strengths of the coated and painted AZ61 alloy under high humidity and 5%NaCl environments showed almost the same fatigue strength as bulk material under low humidity.


2011 ◽  
Vol 295-297 ◽  
pp. 2386-2389 ◽  
Author(s):  
Ren Hui Tian ◽  
Qiao Lin Ouyang ◽  
Qing Yuan Wang

In order to investigate the effect of plasma nitriding treatment on fatigue behavior of titanium alloys, very high cycle fatigue tests were carried out for Ti-6Al-4V alloy using an ultrasonic fatigue machine under load control conditions for stress ratios of R=-1 at frequency of ƒ=20KHz. Experiment results showed that plasma nitriding treatment played the principal role in the internal fatigue crack initiation. More importantly, plasma nitriding treatment had a detrimental effect on fatigue properties of the investigated Ti-6Al-4V alloy, and the fatigue strength of material after plasma nitriding treatment appeared to be significantly reduced about 17% over the untreated material.


Author(s):  
Huailin Li

A reduced-activation ferritic/martensitic (RAF/M) steel, JLF-1, is considered as one of the candidate structure material of the fusion reactors and supercritical water-cooled reactor (SCWR). Low cycle fatigue properties of JLF-1 steel at elevated temperature are the design base to provide adequate design margin against postulated mechanism that could experience during its design life, such as stress range, plastic deformation, and cyclic softening etc. However, the reduction in design margin is significant when the cyclic softening happens in cyclic deformation at RT, 673K, 873K. Thus, for the application as the structural materials, it is necessary to evaluate low cycle fatigue behavior and cyclic softening of JLF-1 steel at elevated temperature since those properties of material at elevated temperature are the key issue for design.


Author(s):  
Ming Zhang ◽  
Weiqiang Wang ◽  
Aiju Li

The authors researched the effects of specimen size on the very high cycle fatigue properties of FV520B-I through ultrasonic fatigue testing. The test results showed that the very high cycle fatigue mechanism was not changed and the fatigue properties declined as the specimen size increased. The S-N curve moved downward and the fatigue life decreased under the same stress level maybe due to the heat effects of large specimens in tests. The fatigue strength and the fatigue life were predicted by relevant models. The prediction of fatigue strength was close to test result, and the prediction of fatigue life was less effective compared with the previous prediction of small size specimen test results.


2013 ◽  
Vol 2013 (0) ◽  
pp. _OS1514-1_-_OS1514-3_
Author(s):  
Motoyuki OCHI ◽  
Ken SUZUKI ◽  
Isamu NONAKA ◽  
Hideo MIURA

2014 ◽  
Vol 217-218 ◽  
pp. 227-234 ◽  
Author(s):  
Alain Abou Antoun ◽  
Myriam Brochu ◽  
Heinrich Möller

Two objectives were targeted: 1) compare the high cycle fatigue behavior of rheocast aluminum alloy 357 prepared by the swirl enthalpy equilibration device (SEED) and by the Council for Scientific and Industrial Research (CSIR) process, and 2) study the effect of surface liquid segregation (SLS) on the fatigue behavior of the CSIR material. Rectangular hourglass specimens machined from rheocast plates were tested at four stress amplitudes in axial fatigue with a stress ratio of R = -1 and a frequency of 20 Hz. Results obtained for SLS free specimens show that the SEED and the CSIR processes produce rheocast materials with comparable high cycle fatigue properties, 115 MPa at 107 cycles. In order to study the influence of surface liquid segregation, slightly polished specimens with a remaining SLS of nearly 750 microns thick were also tested. According to the results, the SLS reduces the average fatigue strength by approximately 5% (110 MPa vs. 115 MPa at 107 cycles). For SLS free specimens, the fatigue crack initiated at shrinkage cavities, oxide films or in the alpha globules. On the other hand, for specimens with SLS, no crack initiation in the alpha globules was observed. The main crack initiation mechanism was identified to be a deformation incompatibility between regions characterized by higher silicon content compared to nominal eutectic regions. The originality of the work is provided by the rigorous comparative analysis of the fatigue performance of components produced in two different rheocasting facilities, but tested in a single laboratory. It is also the first fundamental research published on the mechanical effect of surface liquid segregation. It confirms that SLS should be removed in critical areas in order to optimize the fatigue resistance of rheocast components.


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