Fabrication of Supports for Solid Oxide Fuel Cells by Powder Injection Molding

Author(s):  
Ali Keshavarz Panahi ◽  
Hadi Miyanaji ◽  
Moein Taheri ◽  
Milad Janbakhsh

In this paper the processing steps for producing SOFC (Solid Oxide Fuel Cell) supports by means of PIM (Powder Injection Molding) technique were investigated. Injection molding parameters in this study were divided into pressure-related (injection pressure and packing pressure), temperature-related (nozzle temperature and mold temperature), and time-related (injection rate and holding time) parameters. Keeping the other parameters (pressure-related, temperature-related and time-related parameters) constant at an optimized value, the effects of each of the molding parameters above were investigated. The results show that the short shot, warpage, weld line and void are the most common defects in molded parts. According to the results the short shot could be seen in low values of injection pressure, injection rate, nozzle and mold temperature. Also, warpage could be seen in high values of mold temperature, injection and packing pressure. Poor weld line was another defect that could be seen in low values of injection pressure, injection rate, nozzle and mold temperature. Also the void was one of the most common defects that could be seen in high values of injection rate and nozzle temperatures. Finally, using optimized molding parameters, the molded parts underwent debinding and sintering processes. Based on the results of thermal shock tests and the porosity measurements of the sintered parts, these molded parts possessed relatively desirable characteristics.

2010 ◽  
Vol 44-47 ◽  
pp. 2707-2711 ◽  
Author(s):  
Norhamidi Muhamad ◽  
Nor Hafiez Mohamad Nor ◽  
Sufizar Ahmad ◽  
Mohd Halim Irwan Ibrahim ◽  
Mohd Ruzi Harun

The L27 (313) Taguchi orthogonal array is used in the experiment while the injection pressure, injection temperature, powder loading, mold temperature, holding pressure and injection speed are optimized in this study. A grey relational grade (GRG) obtained from the grey relational analysis (GRA) is used to solve the titanium alloy powder injection molding operations with the multiple performance characteristics such as strength and density. From the analysis of variance (ANOVA), the injection temperature has the highest contribution at confidence level 90% to the quality of green part followed by powder loading. The others factor such as mold temperature, holding pressure, injection pressure and injection rate and all the interactions are not significant even though it give contribution during injection molding but the confidence level are less than 90%.


2012 ◽  
Vol 501 ◽  
pp. 294-299 ◽  
Author(s):  
Zhi Bian ◽  
Peng Cheng Xie ◽  
Yu Mei Ding ◽  
Wei Min Yang

This study was aimed at understanding how the process conditions affected the dimensional stability of glass fiber reinforced PP by microcellular injection molding. A design of experiments (DOE) was performed and plane test specimens were produced for the shrinkage and warpage analysis. Injection molding trials were performed by systematically adjusting six process parameters (i.e., Injection speed, Injection pressure, Shot temperature, SCF level, Mold temperature, and Cooling time). By analyzing the statistically significant main and two-factor interaction effects, the results showed that the supercritical fluid (SCF) level and the injection speed affected the shrinkage and warpage of microcellular injection molded parts the most.


2012 ◽  
Vol 184-185 ◽  
pp. 1651-1654
Author(s):  
Jeou Long Lee ◽  
Y. Lin ◽  
Y.K. Shen

This study characterizes warpage of a micro-injection molded micro electrical fan using the Michelson interference method. This study conducts experiments to analyze different polymers-polypropylene (PP), polyamide (PA), acrylonitrile-butadiene styrene (ABS), ABS+ polycarbonate (PC), and polyoxymethylene (POM)-process parameters, such as mold temperature, injection temperature, injection pressure, injection time, packing time, and packing pressure, for a micro electrical fan. To obtain the optimum result (minimum warpage), this study assesses the effect (warpage) of each material on micro-injection molding. PA plastic is the very suitable material for micro electrical fan with Michelson interference analysis on micro-injection molding.


Cerâmica ◽  
2018 ◽  
Vol 64 (369) ◽  
pp. 97-103 ◽  
Author(s):  
C. A. Costa ◽  
A. F. Michels ◽  
M. E. Kipper

Abstract This work presents a study to evaluate the process of producing internal holes in ceramic disks produced by low pressure injection molding (LPIM) process. Two process conditions defined as pre-injection and post-injection were used to test the proposition. In the first one the pin cores that produce the holes were positioned in the cavity before the injection of the feedstock; and in the second one, the pin cores were positioned in the cavity, just after the feeding phase of the injection mold. An experimental injection mold designed and manufactured to test both processes was developed to produce ceramic disk with Ø 50 x 2 mm with four holes of Ø 5 mm, equally and radially distributed through the disk. The feedstock was composed of 86 wt% alumina (Al2O3) and 14 wt% organic vehicle based on paraffin wax. Heating and cooling systems controlled by a data acquisition system were included in the mold. The results showed that there were no welding lines with the post-injection process, proving to be an option for creating holes in the ceramic parts produced by LPIM. It was observed that best results were obtained at 58 °C mold temperature. The pins extraction temperature was about 45 °C, and the injection pressure was 170 kPa.


2012 ◽  
Vol 59 (2) ◽  
Author(s):  
Azizah Wahi ◽  
Norhamidi Muhamad ◽  
Khairur R. Jamaludin ◽  
Javad Rajabi ◽  
Abbas Madraky

Data Mining is a method that can be used to analyze large amount of data and produce useful information. In this study, clustering which is one of data mining tasks is used to clustered machine based on the injection moulding data. This paper is the first documented results on the optimization of Injection Moulding via Data Mining. Powder injection moulding is a process to produce near net shape with intricate part in mass production. This work focus on the optimization of injection molding process with combination of fine, coarse and bimodal water atomized SS 316L powder particles. The parameters involved in the optimization are injection pressure, injection temperature, mould temperature, holding pressure, injection rate, holding time, powder loading, cooling time and particle size. These variables are based on the defect score, green density and green strength. The key influencer report shows that the most influencing factors are injection rate, holding pressure as well as mould temperature where defect score lower than 2.4 can be achieved. The density higher than 5.34g/cm3 is also influenced most by the mould temperature. The result also shows that the optimize condition can be achieved by using bimodal particle. Injection rate and mould temperature gives the highest impact on the defect score and green strength value. While highest green density is significantly affected by powder loading and injection pressure.


2017 ◽  
Vol 36 (2) ◽  
pp. 51-74 ◽  
Author(s):  
Ying-Guo Zhou ◽  
Bei Su ◽  
Lih-Sheng Turng

Water-foamed injection molding (WFIM) uses conventional injection molding (CIM) with water as a physical foaming agent. Compared to CIM, WFIM is a much more complicated process. As such, it is critical to determine the processing conditions for fabricating quality parts using WFIM. We used the design of experiment (DOE) method based on the Taguchi method to determine the influence of the processing conditions on the morphological structure and ductility of PP/LDPE WFIM parts, which were investigated by tensile testing and scanning electron microscopy (SEM). Our research suggests that fabricating PP/LDPE super-ductile parts using WFIM is indeed feasible. Our research also indicates that there is a close relationship between the ductility and the foamed structures, both of which are deeply influenced by the processing conditions. The analysis of variance results shows further that the water content had the greatest influence on the ductility, followed by the melt temperature, packing time, packing pressure, and PP/LDPE ratio. However, the ductility was only slightly influenced by the mold temperature, injection pressure, and injection time in WFIM. As to the number of cells, the order of influence was melt temperature, water content, packing time, packing pressure, mold temperature, injection pressure, PP/LDPE ratio, and injection time, in that order. In addition, applying DOE is a quite effective method for deducing the optimal set of effective factors in WFIM to produce super-ductile parts with a maximum number of cells. To our knowledge, this is the first time that the relationship among the processing conditions, ductility, and foamed structure of PP/LDPE WFIM super-ductile parts has been investigated and reported.


2011 ◽  
Vol 55-57 ◽  
pp. 1511-1517
Author(s):  
Xiao Hua Wei ◽  
Bai Yang Lou

According to the basic theory and process of conventional injection molding, using the CAE software, numerical simulation research of the injection molding characteristic for micro thin-wall plastic parts are put forward. The effects of process parameters (melt temperature, mold temperature, injection pressure, injection rate) on molding characteristic of micro thin-wall plastic parts are discussed by single factor method, compare the significance of each factors.The simulation results showed that volume could be improved with the increase of melt temperature ,molding temperature, injection pressure and injection rate.


Materials ◽  
2021 ◽  
Vol 14 (13) ◽  
pp. 3632
Author(s):  
Sylvain Badie ◽  
Rimy Gabriel ◽  
Doris Sebold ◽  
Robert Vaßen ◽  
Olivier Guillon ◽  
...  

Near-net shape components composed of monolithic Ti2AlC and composites thereof, containing up to 20 vol.% Al2O3 fibers, were fabricated by powder injection molding. Fibers were homogeneously dispersed and preferentially oriented, due to flow constriction and shear-induced velocity gradients. After a two-stage debinding procedure, the injection-molded parts were sintered by pressureless sintering at 1250 °C and 1400 °C under argon, leading to relative densities of up to 70% and 92%, respectively. In order to achieve near-complete densification, field assisted sintering technology/spark plasma sintering in a graphite powder bed was used, yielding final relative densities of up to 98.6% and 97.2% for monolithic and composite parts, respectively. While the monolithic parts shrank isotropically, composite assemblies underwent anisotropic densification due to constrained sintering, on account of the ceramic fibers and their specific orientation. No significant increase, either in hardness or in toughness, upon the incorporation of Al2O3 fibers was observed. The 20 vol.% Al2O3 fiber-reinforced specimen accommodated deformation by producing neat and well-defined pyramidal indents at every load up to a 30 kgf (~294 N).


2006 ◽  
Vol 505-507 ◽  
pp. 229-234 ◽  
Author(s):  
Yung Kang Shen ◽  
H.J. Chang ◽  
C.T. Lin

The purpose of this paper presents the optical properties of microstructure of lightguiding plate for micro injection molding (MIM) and micro injection-compression molding (MICM). The lightguiding plate is applied on LCD of two inch of digital camera. Its radius of microstructure is from 100μm to 300μm by linearity expansion. The material of lightguiding plate uses the PMMA plastic. This paper uses the luminance distribution to make a comparison between MIM and MICM for the optical properties of lightguiding plate. The important parameters of process for optical properties are the mold temperature, melt temperature and packing pressure in micro injection molding. The important parameters of process for optical properties are the compression distance, mold temperature and compression speed in micro injection-compression molding. The process of micro injection-compression molding is better than micro injection molding for optical properties.


2018 ◽  
Vol 2018 ◽  
pp. 1-9 ◽  
Author(s):  
Youmin Wang ◽  
Zhichao Yan ◽  
Xuejun Shan

In order to obtain the optimal combination of process parameters for vertical-faced polypropylene bottle injection molding, with UG, the model of the bottle was drawn, and then, one module and sixteen-cavity injection molding system was established and analyzed using Moldflow. For filling and maintaining pressure during the process of infusion bottle injection molding, the orthogonal test table L25 (56) using CAE was designed for injection molding of the bottle, with six parameters such as melt temperature, mold temperature, injection pressure, injection time, dwell pressure, and dwell time as orthogonal test factors. By finding the best combination of process parameters, the orthogonal experiment was completed, the results were analyzed by range analysis, and the order of influence of each process parameter on each direction of optimization was obtained. The prediction dates of the infusion bottle were gained under various parameters, a comprehensive quality evaluation index of the bottle was formulated, and the multiobjective optimization problem of injection molding process was transformed into a single-objective optimization problem by the integrated weighted score method. The bottle parameters were optimized by analyzing the range date of the weighted scoring method, and the best parameter combination such as melt temperature 200°C, mold temperature 80°C, injection pressure 40 MPa, injection time 2.1 S, dwell pressure 40 MPa, and dwell time 40 S was gained.


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