EX SITU ATOMIC FORCE MICROSCOPY STUDIES OF SURFACE MORPHOLOGY ON {001} FACES OF MMTWD CRYSTALS

2006 ◽  
Vol 13 (05) ◽  
pp. 607-611
Author(s):  
X. J. LIU ◽  
X. Q. WANG ◽  
Z. Y. WANG ◽  
D. XU ◽  
G. W. YU ◽  
...  

Surface morphology of the {001} faces of MMTWD crystals grown from by the temperature-lowering method has been studied. Monolayer and multilayer steps elongate along the a direction, which is determined by the crystal structure. Apart from that, the elementary steps have narrower terraces than the bunched ones, which may be resulting from the faster growth rates of the former than the latter. The formation of the protuberances at the step fronts is primarily associated with the uneven growth rates. The hollow cavities also elongate along the a direction, which demonstrates that the formation of them is also restricted by the crystal structure. Cracks are supposed to occur during harvesting, handling, or temperature stress afterwards. Growth of the 3D hillocks in high density can probably cause large stress and induce structure mismatch and serious cracks at the later stage.

2005 ◽  
Vol 38 (4) ◽  
pp. 657-660 ◽  
Author(s):  
Y. L. Geng ◽  
D. Xu ◽  
X. Q. Wang ◽  
G. H. Zhang ◽  
G. W. Yu ◽  
...  

Surface morphology of {100} faces of LAP crystals was investigated by atomic force microscopy (AFM). Both the steps and the two-dimensional nuclei elongate along thebdirection, which is determined by the crystal structure. Fluctuations in the growth conditions could result in the formation of protuberances on the step fronts. Tree-like growth belts are initially observed on LAP crystals. It is assumed that the formation is caused by uneven liquid flow of the mother solution.


1992 ◽  
Author(s):  
Mark R. Kozlowski ◽  
Michael C. Staggs ◽  
Mehdi Balooch ◽  
Robert J. Tench ◽  
Wigbert J. Siekhaus

1999 ◽  
Vol 200 (3-4) ◽  
pp. 348-352 ◽  
Author(s):  
R.S Qhalid Fareed ◽  
S Tottori ◽  
K Nishino ◽  
S Sakai

Author(s):  
Pengcheng Chen ◽  
Jordan N. Metz ◽  
Adam S. Gross ◽  
Stuart E. Smith ◽  
Steven P. Rucker ◽  
...  

1995 ◽  
Vol 413 ◽  
Author(s):  
V. Shivshankar ◽  
C. Sung ◽  
J. Kumar ◽  
S. K. Tripathy ◽  
D. J. Sandman

ABSTRACTWe have studied the surface morphology of free standing single crystals of thermochromic polydiacetylenes (PDAs), namely, ETCD and IPUDO (respectively, the ethyl and isopropyl urethanes of 5,7-dodecadiyn-1,12-diol), by Atomic Force Microscopy (AFM) under ambient conditions. Micron scale as well as molecularly resolved images were obtained. The micron scale images indicate a variable surface, and the molecularly resolved images show a well defined 2-D lattice that is interpreted in terms of molecular models and known crystallographic data. Thereby information about surface morphology, which is crucial to potential optical device or chromic sensor performance is available. We also report the observation of a “macroscopic shattering” of the IPUDO monomer crystal during in-situ UV polymerization studies.


2002 ◽  
Vol 234 (2-3) ◽  
pp. 480-486 ◽  
Author(s):  
X.N. Jiang ◽  
D. Xu ◽  
D.L. Sun ◽  
D.R. Yuan ◽  
M.K. Lu ◽  
...  

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