X-Ray Fractography of Stress Corrosion Cracking in Aisi 4340 Steel Under Controlled Electrode potential

1987 ◽  
Vol 31 ◽  
pp. 269-276 ◽  
Author(s):  
Masaaki Tsuda ◽  
Yukio Hirose ◽  
Zenjiro Yajima ◽  
Keisuke Tanaka
Keyword(s):  
Residual Stress ◽  
Fracture Surface ◽  
Stress Corrosion ◽  
Stress Corrosion Cracking ◽  
Electrode Potential ◽  
Diffraction Method ◽  
Corrosion Cracking ◽  
Fracture Mechanisms ◽  
X Ray ◽  
Electrode Potentials

The residual stress left on the fracture surface is one of the important parameters in X-ray fractography and has been used to analyze fracture mechanisms in fracture toughness and fatigue tests especially of high strength steels.In the present paper, the distribution of residual stress beneath the fracture surface made by stress corrosion cracking was measured by the X-ray diffraction method. Stress corrosion cracking tests were conducted by using compact tension specimens of 200°C tempered AISI steel in 3.5% NaCl solution environment under various electrode potentials. The effect of electrode potential on the growth kinetics of stress corrosion cracking is discussed on the basis of residual stress distribution.

X-ray Residual Stress Measurement on Fracture Surface of Stress Corrosion Cracking

1989 ◽  
Vol 33 ◽  
pp. 327-334 ◽  
Author(s):  
Masaaki Tsuda ◽  
Yukic Hirose ◽  
Zenjiro Yajima ◽  
Keisuke Tanaka
Keyword(s):  
Fracture Toughness ◽  
Residual Stress ◽  
Fracture Surface ◽  
Stress Corrosion ◽  
Stress Corrosion Cracking ◽  
Stress Measurement ◽  
High Strength Steels ◽  
High Strength ◽  
X Ray Diffraction ◽  
X Ray

X-ray fractography is a new method utilizing the X-ray diffraction technique to observe the fracture surface for the analysis of the micromechanisms and mechanics of fracture. The X-ray residual stress has been confirmed to be a particularly useful parameter when studying the fracture surfaces of high strength steels. The method has been applied to the fracture surface of fracture toughness and fatigue specimens.

scholarly journals Investigation of Stress Corrosion Cracking in Magnesium Alloys by Quantitative Fractography Methods

2017 ◽  
Vol 62 (2) ◽  
pp. 557-562 ◽  
Author(s):  
M. Sozańska ◽  
A. Mościcki ◽  
B. Chmiela
Keyword(s):  
Magnesium Alloy ◽  
Fracture Surface ◽  
Strain Rate ◽  
Stress Corrosion ◽  
Quantitative Evaluation ◽  
Stress Corrosion Cracking ◽  
Corrosion Cracking ◽  
Slow Strain Rate Test ◽  
Rate Test ◽  
We43 Magnesium Alloy

Abstract The article shows that the use of quantitative fracture description may lead to significant progress in research on the phenomenon of stress corrosion cracking of the WE43 magnesium alloy. Tests were carried out on samples in air, and after hydrogenation in 0.1 M Na2SO4 with cathodic polarization. Fracture surfaces were analyzed after different variants of the Slow Strain Rate Test. It was demonstrated that the parameters for quantitative evaluation of fracture surface microcracks can be closely linked with the susceptibility of the WE43 magnesium alloy operating under complex state of the mechanical load in corrosive environments. The final result of the study was the determination of the quantitative relationship between Slow Strain Rate Test parameters, the mechanical properties, and the parameters of the quantitative evaluation of fracture surface (microcracks).

Relationships Between Electrochemical Measurements and Stress Corrosion Cracking of Maraging Steel

CORROSION ◽  
1967 ◽  
Vol 23 (1) ◽  
pp. 5-10 ◽  
Author(s):  
J. A. S. GREEN ◽  
E. G. HANEY
Keyword(s):  
Yield Strength ◽  
Stress Corrosion ◽  
Maraging Steel ◽  
Stress Corrosion Cracking ◽  
Electrode Potential ◽  
Full Range ◽  
Corrosion Cracking ◽  
Deionized Water ◽  
Failure Times ◽  
Ph Values

Abstract Stress corrosion cracking of 18Ni maraging steel foil has been studied in deionized water solutions with the pH adjusted by NaOH additions over a range from 8 to 13. The full range of NaCl contents from saturated solutions to no addition was tested with specimens stressed to 75 percent of yield strength. For each variation in NaCl content, the specimen failure times go through a minimum with respect to pH. With increasing NaCl content, the minimum becomes more pronounced and its position shifts towards higher pH values. The position of each minimum is indicated by electrode potential measurements. Potentiostatic measurements as a function of pH confirm that maximum susceptibility to stress corrosion cracking occurs just prior to the onset of passivation.

NRC/EPRI Residual Stress Validation Program Phase I: Experimental Specimen Modeling and Measurement

2011 ◽  
Author(s):  
J. Broussard ◽  
P. Crooker
Keyword(s):  
Residual Stress ◽  
Residual Stresses ◽  
Stress Corrosion ◽  
Stress Corrosion Cracking ◽  
Phase 1 ◽  
Measurement Techniques ◽  
Corrosion Cracking ◽  
Welding Residual Stress ◽  
Hole Drilling ◽  
Pressurized Water

The US Nuclear Regulatory Commission (NRC) and the Electric Power Research Institute (EPRI) are working cooperatively under a memorandum of understanding to validate welding residual stress predictions in pressurized water reactor primary cooling loop components containing dissimilar metal welds. These stresses are of interest as DM welds in pressurized water reactors are susceptible to primary water stress corrosion cracking (PWSCC) and tensile weld residual stresses are one of the primary drivers of this stress corrosion cracking mechanism. The NRC/EPRI weld residual stress (WRS) program currently consists of four phases, with each phase increasing in complexity from lab size specimens to component mock-ups and ex-plant material. This paper describes the Phase 1 program, which comprised an initial period of learning and research for both FEA methods and measurement techniques using simple welded specimens. The Phase 1 specimens include a number of plate and cylinder geometries, each designed to provide a controlled configuration for maximum repeatability of measurements and modeling. A spectrum of surface and through-wall residual stress measurement techniques have been explored using the Phase 1 specimens, including incremental hole drilling, ring-core, and x-ray diffraction for surface stresses and neutron diffraction, deep-hole drilling, and contour method for through-wall stresses. The measured residual stresses are compared to the predicted stress results from a number of researchers employing a variety of modeling techniques. Comparisons between the various measurement techniques and among the modeling results have allowed for greater insight into the impact of various parameters on predicted versus measured residual stress. This paper will also discuss the technical challenges and lessons learned as part of the DM weld materials residual stress measurements.

Effects of Cold Working and Heat Treatment on Caustic Stress Corrosion Cracking of Alloy 800M

2005 ◽  
Vol 297-300 ◽  
pp. 993-998 ◽  
Author(s):  
Chun Bo Huang ◽  
Guang Fu Li ◽  
Zhan Peng Lu ◽  
Jian Min Zeng ◽  
Wu Yang
Keyword(s):  
Heat Treatment ◽  
Residual Stress ◽  
Stress Corrosion ◽  
Stress Corrosion Cracking ◽  
Cold Working ◽  
Corrosion Cracking ◽  
Caustic Solution ◽  
Surface Films ◽  
Microstructure Examination ◽  
Increasing Temperature

The effects of cold working and heat treatment on caustic stress corrosion cracking (SCC) of mill annealed (MA) alloy 800M in boiling solution of 50%NaOH+0.3%SiO2+0.3%Na2S2O3 were investigated by means of microstructure examination, tensile test, X-ray stress analysis, SCC testing of C-rings, Auger electron spectroscopy (AES), scanning electron microscopy (SEM) and metallography. The microstructure of alloy 800M under tested conditions was austenite. With a train of 25% by cold working, the grains of alloy 800M became longer, yield strength (YS) and ultimate tensile strength (UTS) increased, elongation (δ ) decreased, residual stress and the susceptibility to SCC increased. With increasing temperature of heat treatment of alloy 800M with cold working, the grains became bigger , residual stress, YS and UTS decreased and δ increased, the susceptibility to SCC of alloy 800M decreased. In boiling caustic solution, SCC cracks on the surfaces of C-ring specimens polarized potentiostatically at –20mV/SCE initiated from pitting and propagated along grain boundaries. AES analysis indicated that the surface films on MA alloy 800M were enriched in nickel and depleted in iron and chromium.

Effect of Ultrasonic Impact Treatment on the Stress Corrosion Cracking of 304 Stainless Steel Welded Joints

2008 ◽  
Author(s):  
Gang Ma ◽  
Xiang Ling
Keyword(s):  
Residual Stress ◽  
Finite Element ◽  
Stainless Steel ◽  
Stress Corrosion ◽  
Stress Corrosion Cracking ◽  
Welded Joints ◽  
Corrosion Cracking ◽  
Coarse Grained ◽  
304 Stainless Steel ◽  
Ultrasonic Impact Treatment

High tensile weld residual stress is an important factor contributing to stress corrosion cracking (SCC). Ultrasonic impact treatment (UIT) can produce compressive stresses on the surface of welded joints that negate the tensile stresses to enhance the SCC resistance of welded joints. In the present work, X-ray diffraction method was used to obtain the distribution of residual stress induced by UIT. The results showed that UIT could cause a large compressive residual stress up to 325.9MPa on the surface of the material. A 3D finite element model was established to simulate the UIT process by using a finite element software ABAQUS. The residual stress distribution of the AISI 304 stainless steel induced by UIT was predicted by finite element analysis. In order to demonstrate the improvement of the SCC resistance of the welded joints, the specimens were immersed in boiling 42% magnesium chloride solution during SCC testing, and untreated specimen cracked after immersion for 23 hours. In contrast, treated specimens with different coverage were tested for 1000 hours without visible stress corrosion cracks. The microstructure observation results revealed that a hardened layer was formed on the surface and the initial coarse-grained structure in the surface was refined into ultrafine grains. The above results indicate that UIT is an effective approach for protecting weldments against SCC.

Investigation of the Influence of Shot Peening on Stress Corrosion Cracking of Stainless Steel Welded Joints

2008 ◽  
Vol 575-578 ◽  
pp. 672-677 ◽  
Author(s):  
Xiang Ling ◽  
Hong Fang Ni ◽  
Gang Ma
Keyword(s):  
Stainless Steel ◽  
Stress Corrosion ◽  
Stress Corrosion Cracking ◽  
Welded Joints ◽  
Shot Peening ◽  
Corrosion Cracking ◽  
Glass Beads ◽  
Residual Tensile Stress ◽  
X Ray ◽  
Compressive Stresses

High residual tensile stress is an important factor contributing to stress corrosion cracking (SCC). Shot peening can impose compressive stresses on the surface of welded joints that negate the tensile stresses to enhance the SCC resistance of welded joints. In the present work, the distribution of residual stress caused by welding is measured by X-ray diffraction method. The maximum stress in the weld is close to the yield strength of AISI 304 stainless steel, and the stresses are negative at both ends of the weld and far from the weld. The X-ray method is also used to measure stress caused by shot-peening. The results show that the higher the peening coverage, the higher the residual compressive stresses in the surface of weldments. While under the same condition, the residual compressive stresses induced by glass beads shot-peening are larger than those by cast steel shots. Temperature and stress fields of welding are simulated by using ABAQUS codes. The 3-D solid elements are used in FEM. Temperature depending on material properties as well as the convection and radiation as boundary conditions are considered. The 3-D linear reduced-integration elements are used to simulate the shot peening process. The results of simulation have a good agreement with experimental data. All unpeened and peened weldments are immersed in boiling 42% magnesium chloride solution during SCC test. Unpeened specimens crack after immersion for 6 hours. The steel-peened specimens with 50% coverage crack after 310 hours, while the steel-peened specimens with 100% coverage crack for 3500 hours. However, steel-peened specimens with 200% coverage and glass-peened specimens with 50%, 100% and 200% coverage are tested for a total of 3500 hours without visible stress corrosion cracks in the peened surfaces. The experiment results indicate that shot peening is an effective method for protecting weldments against SCC and weldments peened by glass beads resist SCC better than those peened by steel shots.

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