High-Flux X-Ray and Neutron Solution Scattering

Author(s):  
Stephen J. Perkins
Keyword(s):  
2009 ◽  
Vol 1203 ◽  
Author(s):  
Jen Bohon ◽  
John Smedley ◽  
Erik M. Muller ◽  
Jeffrey W. Keister

AbstractHigh quality single crystal and polycrystalline CVD diamond detectors with platinum contacts have been tested at the white beam X28C beamline at the National Synchrotron Light Source under high-flux conditions. The voltage dependence of these devices has been measured under DC and pulsed-bias conditions, establishing the presence or absence of photoconductive gain in each device. Linear response has been achieved over eleven orders of magnitude when combined with previous low flux studies. Temporal measurements with single crystal diamond detectors have resolved the ns scale pulse structure of the NSLS.


1998 ◽  
Vol 39 (4) ◽  
pp. 372-374 ◽  
Author(s):  
K. J. Berg ◽  
B. Rolfsen ◽  
G. Stake

Purpose, Material and Methods, and Results: The dialyzability of the high-molecular X-ray contrast medium iodixanol was examined in an in vitro hemo-dialysis model using two different hollow fiber membranes: one high-flux (polysulfone) membrane and one intermediate-flux (cellulose triacetate) membrane. Blood flow was 200 ml/min and membrane area 1.3 m2. The dialyzer clearance of iodixanol dissolved in a mixture of leukocyte-filtered SAG-M blood and compatible citrate plasma was 134.2±3.6 ml/min for the polysulfone membrane and 113.0±3.6 ml/min for the cellulose triacetate membrane. Conclusion: Iodixanol is readily dialyzed through commercial high-flux membranes.


2014 ◽  
Vol 70 (a1) ◽  
pp. C1330-C1330
Author(s):  
Joerg Wiesmann ◽  
Andreas Kleine ◽  
Christopher Umland ◽  
André Beerlink ◽  
Juergen Graf ◽  
...  

Parasitic scattering caused by apertures is a well-known problem in X-ray analytics, which forces users and manufacturers to adapt their experimental setup to this unwanted phenomenon. Increased measurement times due to lower photon fluxes, a lower resolution caused by an enlarged beam stop, a larger beam defining pinhole-to-sample distance due to the integration of an antiscatter guard and generally a lower signal-to-noise ratio leads to a loss in data quality. In this presentation we will explain how the lately developed scatterless pinholes called SCATEX overcome the aforementioned problems. SCATEX pinholes are either made of Germanium or of Tantalum and momentarily have a minimum diameter of 30µm. Thus, these novel apertures are applicable to a wide range of different applications and X-ray energies. We will show measurements which were performed either at home-lab small angle X-ray scattering (SAXS) systems such as the NANOSTAR of Bruker AXS or at synchrotron beamlines. At the PTB four-crystal monochromator beamline at BESSY II data was collected for a comparison of conventional pinholes, scatterless Germanium slit systems and SCATEX pinholes. At the Nanofocus Endstation P03 beamline at PETRA III we compared the performance of our SCATEX apertures with conventional Tungsten slit systems under high flux density conditions.


2001 ◽  
Vol 40 (Part 1, No. 2B) ◽  
pp. 1094-1096 ◽  
Author(s):  
Hiroshi Amekura ◽  
Vladimir Voitsenya ◽  
Thi Thi Lay ◽  
Yoshihiko Takeda ◽  
Naoki Kishimoto

2014 ◽  
Vol 39 (18) ◽  
pp. 5383 ◽  
Author(s):  
S. L. Cousin ◽  
F. Silva ◽  
S. Teichmann ◽  
M. Hemmer ◽  
B. Buades ◽  
...  
Keyword(s):  

2021 ◽  
Vol 92 (8) ◽  
pp. 083102
Author(s):  
M. Espy ◽  
M. Klasky ◽  
M. James ◽  
D. Moir ◽  
J. Mendez ◽  
...  

2020 ◽  
Vol 27 (2) ◽  
pp. 319-328 ◽  
Author(s):  
Leonardo Abbene ◽  
Fabio Principato ◽  
Gaetano Gerardi ◽  
Antonino Buttacavoli ◽  
Donato Cascio ◽  
...  

In this work, the spectroscopic performances of new cadmium–zinc–telluride (CZT) pixel detectors recently developed at IMEM-CNR of Parma (Italy) are presented. Sub-millimetre arrays with pixel pitch less than 500 µm, based on boron oxide encapsulated vertical Bridgman grown CZT crystals, were fabricated. Excellent room-temperature performance characterizes the detectors even at high-bias-voltage operation (9000 V cm−1), with energy resolutions (FWHM) of 4% (0.9 keV), 1.7% (1 keV) and 1.3% (1.6 keV) at 22.1, 59.5 and 122.1 keV, respectively. Charge-sharing investigations were performed with both uncollimated and collimated synchrotron X-ray beams with particular attention to the mitigation of the charge losses at the inter-pixel gap region. High-rate measurements demonstrated the absence of high-flux radiation-induced polarization phenomena up to 2 × 106 photons mm−2 s−1. These activities are in the framework of an international collaboration on the development of energy-resolved photon-counting systems for high-flux energy-resolved X-ray imaging.


2018 ◽  
Vol 4 (5) ◽  
pp. eaar3761 ◽  
Author(s):  
Allan S. Johnson ◽  
Dane R. Austin ◽  
David A. Wood ◽  
Christian Brahms ◽  
Andrew Gregory ◽  
...  

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