Synthesis and characterization of new disilane -containing arylacetylene resin
AbstractA novel disilane-containing arylacetylene resin, abbreviated as DSA resin, was synthesized from diethynylbenzene and halogenated disilane by Grignard reaction. The obtained resin was a viscous liquid and soluble in a variety of common solvents. The structures and properties of the resin, cured resin and sintered resin were characterized by FT-IR, 1H-NMR, DSC, TGA and XRD techniques. The results showed that the DSA resin could cure at temperatures lower than 200°C and the cured resin exhibited high temperature resistance and good ceramic formability.
2012 ◽
Vol 560-561
◽
pp. 174-178
2010 ◽
Vol 119
(4)
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pp. 2339-2344
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