Study on the effect of processing conditions on the mechanical properties of PP/PC/SEBS ternary blends using Taguchi experimental analysis

e-Polymers ◽  
2010 ◽  
Vol 10 (1) ◽  
Author(s):  
O. Moini Jazani ◽  
A. Arefazar ◽  
M.H. Beheshty

AbstractIn this study, nine ternary polymer blends based on polypropylene (PP)/polycarbonate (PC)/styrene-ethylene-butylene-styrene triblock copolymer (SEBS) with the same compositions (70%wt PP, 15%wt PC, 7.5%wt SEBS and 7.5%wt maleic-anhydride grafted SEBS (SEBS-g-MAH) as a compatibilizer) are prepared using twin screw extruder at different levels of die temperature (235-245- 255 °C), screw speed (70-100-130rpm) and blending sequence (M1-M2-M3) . In M1 procedure, all of the components are dry blended and extruded simultaneously using Brabender twin-screw extruder. In M2 procedure, PC, SEBS, and SEBS-g- MAH minor phases are first pre-blended in twin screw extruder and after granulating are added to PP continuous phase in twin screw extruder. Consequently, in M3 procedure, PP and SEBS-g-MAH are first pre-blended and then are extruded with other components. The influence of these parameters as processing conditions on mechanical properties of PP/PC/SEBS ternary blends is investigated using L9 Taghuchi experimental design. The responding variables are impact strength and tensile properties (young modulus and yield stress) which are influenced by the morphology of ternary blend and the results are used to perform the analysis of variance (ANOVA). It is shown that the resulted morphology, tensile and impact strength are influenced by extrusion variables. Additionally the optimum processing conditions of ternary PP/PC/SEBS blends from Taguchi analysis was achieved.

2006 ◽  
Vol 514-516 ◽  
pp. 838-842 ◽  
Author(s):  
Ana Vera Machado ◽  
Martin van Duin ◽  
José A. Covas

Dynamic vulcanisation of EPDM/PE blends using the resol/SnCl2 system was studied in a co-rotating twin screw extruder using a series of sampling devices. In order to study the effect of the processing conditions on chemical development along the extruder and on the mechanical properties of the extrudate material, the same recipe (having the same polyolefin/EPDM ratio) was compounded under different processing conditions. The results showed that both chemical evolution and mechanical properties depend on the processing conditions.


Polymers ◽  
2021 ◽  
Vol 13 (7) ◽  
pp. 1058
Author(s):  
Hikaru Okubo ◽  
Haruka Kaneyasu ◽  
Tetsuya Kimura ◽  
Patchiya Phanthong ◽  
Shigeru Yao

Each year, increasing amounts of plastic waste are generated, causing environmental pollution and resource loss. Recycling is a solution, but recycled plastics often have inferior mechanical properties to virgin plastics. However, studies have shown that holding polymers in the melt state before extrusion can restore the mechanical properties; thus, we propose a twin-screw extruder with a molten resin reservoir (MSR), a cavity between the screw zone and twin-screw extruder discharge, which retains molten polymer after mixing in the twin-screw zone, thus influencing the polymer properties. Re-extruded recycled polyethylene (RPE) pellets were produced, and the tensile properties and microstructure of virgin polyethylene (PE), unextruded RPE, and re-extruded RPE moldings prepared with and without the MSR were evaluated. Crucially, the elongation at break of the MSR-extruded RPE molding was seven times higher than that of the original RPE molding, and the Young’s modulus of the MSR-extruded RPE molding was comparable to that of the virgin PE molding. Both the MSR-extruded RPE and virgin PE moldings contained similar striped lamellae. Thus, MSR re-extrusion improved the mechanical performance of recycled polymers by optimizing the microstructure. The use of MSRs will facilitate the reuse of waste plastics as value-added materials having a wide range of industrial applications.


2011 ◽  
Vol 366 ◽  
pp. 310-313
Author(s):  
Ming Tao Run ◽  
Meng Yao ◽  
Bing Tao Xing ◽  
Wen Zhou

The rheology, morphology and mechanical properties of the PA6/PP-g-MAH/POE blends prepared by twin-screw extruder were studied by rheometer, scanning electron microscopy, universal tester and impact tester, respectively. The results suggest that the impact strength is improved by the POE acting as a toughening agent, while the compatibility of PA6 and POE is improved by the compatibilizer of PP-g-MAH. Furthermore, the PP-g-MAH component also acts as a reinforcing agent for decreasing the strength depression induced by the POE component. When POE content is about 9 wt% and PP-g-MAH content is about 10% in blends, the blend has the maximum tensile strength and impact strength. All melts of PA6/PP-g-MAH/POE blends are pseudo-plastic fluids. Both the POE and PP-g-MAH components can increase the apparent viscosity of the melt due to their facility of the linear molecular.


2015 ◽  
Vol 1119 ◽  
pp. 283-287
Author(s):  
Sarit Liprapan ◽  
Thumnoon Nhujak ◽  
Pranut Potiyaraj

The objective of this study is to prepare α-cellulose reinforced poly (butylene succinate) composites (PBS/α-cellulose). The effect of amount α-cellulose on the mechanical properties of the composites was investigated. To improve interfacial interaction between PBS and α-cellulose, glycidyl methacrylate grafted poly (butylene succinate) (PBS-g-GMA) was used as a compatibilizer. Mechanical properties of PBS composites prepared by using a twin-screw extruder were investigated. The mechanical properties of PBS/α-cellulose decreased due to the agglomeration of α-cellulose. Nevertheless, tensile strength, Young’s modulus and flexural strength of PBS composites were improved after the incorporation of PBS-g-GMA. The optimum loading of PBS-g-GMA and α-cellulose in the PBS was found to be 5 and 6 phr.


2013 ◽  
Vol 561 ◽  
pp. 326-330
Author(s):  
Lei Guo ◽  
Qing Kun Liu ◽  
Chuan Sheng Wang

This paper uses a new twin-screw extruder for regeneration of waste tire crumb rubber, discusses the influence of screw speed and reaction temperature on the physical and mechanical properties of reclaimed rubber. Experimental results show that different screw speed and reaction temperature has a great impact on the physical and mechanical properties of the reclaimed rubber. When controls screw speed in the 60 ~ 90 r / min, reaction temperature at 170 to 210°C,the regeneration effect is the best. At this time, the physical and mechanical properties of reclaimed rubber, such as tensile strength, tear strength and elongation at break rate, is the best.


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