Struktur und mechanische Eigenschaften dermatosparaktischen Kollagens / Structure and Mechanical Properties of Dermatosparactic Collagen

1977 ◽  
Vol 32 (9-10) ◽  
pp. 743-747 ◽  
Author(s):  
R. Jonak ◽  
Ch. M. Lapière ◽  
A. Meinel ◽  
H. Nemetschek-Gansler ◽  
Th. Nemetschek ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Tensile Strength ◽  
Cyclic Extension ◽  
X Ray Diffraction ◽  
Mechanische Eigenschaften ◽  
X Ray ◽  
Mechanical Measurements ◽  
Tail Tendon ◽  
Tendon Collagen

Abstract Dermatosparactic calf-tail-tendon-collagen was investigated by mechanical measurements, electron microscopy and x-ray diffraction. We suppose, that the tensile strength decrease of the fibres is due to the irregular aggregation of subfibrils to fibrils. The x-ray diagram of the fibre is not influenced by state of disorder. Cyclic extension of dermatosparactic collagen leads to a higher increase in tensile strength than in the case of normal calf tendon. The effect might be due to the increase of fibril-and area-density resulting in an augmentation of crosslinks.

Some observations on the fine structure of elastoidin

1977 ◽  
Vol 195 (1120) ◽  
pp. 355-364 ◽  
Keyword(s):  
Electron Microscopy ◽  
Fine Structure ◽  
Long Range ◽  
X Ray Diffraction ◽  
X Ray ◽  
Tail Tendon ◽  
Rat Tail ◽  
Tendon Collagen

Electron microscopy of positively stained elastoidin reveals a fine struc­ture apparently identical with that of the collagen of rat tail tendon. The negatively stained pattern is clearly related to that of the collagen but differs from it; it resembles that of artificially cross-linked collagens more. X-ray diffraction fails to find evidence of any long range lateral order in the arrangement of molecules within the elastoidin. The interest­ing splitting of the meridional pattern upon drying is re-reported and its possible origins discussed. Some discussion of fibrillogenesis is presented based on a comparison of rat tail tendon collagen and elastoidin.

scholarly journals Investigating the Effect of Counter Gravity Mold Filling on Microstructure and Mechanical Properties of Cast Aluminium

2020 ◽  
Vol 5 (3) ◽  
pp. 497-506
Author(s):  
Vineet Chak ◽  
Himadri Chattopadhyay ◽  
Md. Mahfooz Alam
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Tensile Strength ◽  
Mold Cavity ◽  
X Ray Diffraction ◽  
X Ray ◽  
Cast Aluminium ◽  
Cavity Filling ◽  
Scanning Electron

In present study an effort has been made to investigate the effect of changing the mode of mold cavity filling on mechanical properties and microstructure of cast aluminium. The pouring of the melt in mold cavity is avoided so as to check defects associated with it and instead of pouring, counter gravity filling of mold technique is utilized. The obtained properties and microstructure are compared with gravity poured (traditionally cast) aluminium. Characterization techniques like optical microscopy, scanning electron microscopy, X-Ray diffraction and mechanical testing like tensile and hardness of the cast samples is carried out. Hardness and tensile strength reported an increment of 22.37% and 26.71% respectively as compared to traditionally cast specimens. This enhancement in mechanical properties was attributed to improved microstructure obtained.

Study of Ageing Treatment on Spray Forming Al-Zn-Mg-Cu Alloy

2012 ◽  
Vol 217-219 ◽  
pp. 1835-1838 ◽  
Author(s):  
Rui Ming Su ◽  
Ying Dong Qu ◽  
Run Xia Li ◽  
Rong De Li
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Tensile Strength ◽  
Hot Extrusion ◽  
Spray Forming ◽  
X Ray Diffraction ◽  
X Ray ◽  
Cu Alloy ◽  
Scanning Electron ◽  
Peak Value

The Al-Zn-Mg-Cu (7A04) alloys were prepared by using the method of spraying forming and the hot extrusion. The changes of microstructure and mechanical properties of the spray deposited Al-Zn-Mg-Cu alloy underwent ageing, regression and reageing treatment (RRA) was studied by scanning electron microscopy, X-ray diffraction and other methods. The results show that the tensile strength of the alloy aged at 120°C for 24 hours can reach the peak value (760MPa), but the elongation is only 4.8 percent. The toughness of the alloy regression treated at 160°C for 2 hours can increase to 9.0 percent, but its tensile strength decreases greatly (680MPa). The reaging treatment at 120°C can make the tensile strength up to 740MPa, while the elongation which is 8.2 percent still keeps a higher level.

scholarly journals STRUCTURES AND PROPERTIES OF NATURAL RUBBER/ORGANOCLAY NANOCOMPOSITES

2011 ◽  
Vol 14 (1) ◽  
pp. 30-38
Author(s):  
Hien Quang Pham ◽  
Son Thanh Thanh Do ◽  
Nieu Huu Nguyen
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Tensile Strength ◽  
Natural Rubber ◽  
Abrasion Resistance ◽  
X Ray Diffraction ◽  
X Ray ◽  
Structures And Properties ◽  
Scanning Electron

Natural rubber (NR), 30% epoxidized natural rubber (ENR30) and organoclays (Nanomer I28E and I30E) are blended in Brabender. Dispersions of the organoclay in NR are investigated by X – ray diffraction (XRD) and scanning electron microscopy (SEM). The results revealed the increase of dispersion efficiency by the addition of ENR30 as a compatibilizer. The existence of organoclay I28E reduces the vulcanization time, while torque value increases slightly and mechanical properties (abrasion resistance, modulus M100, modulus M300, tensile strength, tear strength) are improved considerably.

Phase Transformations in Ti-7w/oMo-3w/oMe Alloy

1974 ◽  
Vol 32 ◽  
pp. 514-515
Author(s):  
S. Fujishiro
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Transmission Electron Microscopy ◽  
Tensile Strength ◽  
Mechanical Processing ◽  
Ray Method ◽  
X Ray ◽  
Transmission Electron ◽  
Water Quench ◽  
Alpha Beta

The mechanical properties of three titanium alloys (Ti-7Mo-3Al, Ti-7Mo- 3Cu and Ti-7Mo-3Ta) were evaluated as function of: 1) Solutionizing in the beta field and aging, 2) Thermal Mechanical Processing in the beta field and aging, 3) Solutionizing in the alpha + beta field and aging. The samples were isothermally aged in the temperature range 300° to 700*C for 4 to 24 hours, followed by a water quench. Transmission electron microscopy and X-ray method were used to identify the phase formed. All three alloys solutionized at 1050°C (beta field) transformed to martensitic alpha (alpha prime) upon being water quenched. Despite this heavily strained alpha prime, which is characterized by microtwins the tensile strength of the as-quenched alloys is relatively low and the elongation is as high as 30%.

scholarly journals Features of the hydration process of the modified blended cement for fiber cement panels

2018 ◽  
Vol 170 ◽  
pp. 03030 ◽  
Author(s):  
Rustem Mukhametrakhimov ◽  
Liliya Lukmanova
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Blended Cement ◽  
Physical And Mechanical Properties ◽  
Hydration Process ◽  
Cement Matrix ◽  
X Ray Diffraction ◽  
Structure Form ◽  
Silicate Phase ◽  
X Ray

The paper studies features of the hydration process of the modified blended cement for fiber cement panels (FCP) using differential thermal analysis, X-ray diffraction analysis, electron microscopy and infrared spectroscopy. It is found that deeper hydration process in silicate phase, denser and finer crystalline structure form in fiber cement matrix based on the modified blended cement. Generalization of this result to the case of fiber cement panels makes it possible to achieve formation of a denser and homogeneous structure with increased physical and mechanical properties.

Effect of Sintering Temperature on Microstructure and Mechanical Properties of Al2O3-TiC-ZrO2 Ceramic Composites

2012 ◽  
Vol 476-478 ◽  
pp. 1031-1035
Author(s):  
Wei Min Liu ◽  
Xing Ai ◽  
Jun Zhao ◽  
Yong Hui Zhou
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Fracture Toughness ◽  
Flexural Strength ◽  
Relative Density ◽  
Sintering Temperature ◽  
Ceramic Composites ◽  
X Ray Diffraction ◽  
X Ray ◽  
Scanning Electron

Al2O3-TiC-ZrO2ceramic composites (ATZ) were fabricated by hot-pressed sintering. The phases and microstructure of the composites were studied by X-ray diffraction (XRD) and scanning electron microscopy (SEM). The relative density and mechanical properties (flexural strength, fracture toughness and Vicker’s hardness) of the composites were tested. The results show that the microstructure of the composites was the gray core-white rim. With the increase of sintering temperature, the relative density and mechanical properties of the composites increased first and then decreased. The composite sintered at 1705°C has the highest synthetical properties, and its relative density, flexural strength, fracture toughness and Vickers hardness are 98.3%,970MPa,6.0 MPa•m1/2and 20.5GPa, respectively.

Research on compatibility and surface of high impact bio-based polyamide

2021 ◽  
pp. 095400832110055
Author(s):  
Yang Wang ◽  
Yuhui Zhang ◽  
Yuhan Xu ◽  
Xiucai Liu ◽  
Weihong Guo
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Differential Scanning Calorimetry ◽  
Crystallization Behavior ◽  
High Impact ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Scanning Electron

The super-tough bio-based nylon was prepared by melt extrusion. In order to improve the compatibility between bio-based nylon and elastomer, the elastomer POE was grafted with maleic anhydride. Scanning Electron Microscopy (SEM) and Thermogravimetric Analysis (TGA) were used to study the compatibility and micro-distribution between super-tough bio-based nylon and toughened elastomers. The results of mechanical strength experiments show that the 20% content of POE-g-MAH has the best toughening effect. After toughening, the toughness of the super-tough nylon was significantly improved. The notched impact strength was 88 kJ/m2 increasing by 1700%, which was in line with the industrial super-tough nylon. X-ray Diffraction (XRD) and Differential Scanning Calorimetry (DSC) were used to study the crystallization behavior of bio-based PA56, and the effect of bio-based PA56 with high crystallinity on mechanical properties was analyzed from the microstructure.

Study on Organic Montmorillonite Modified Recycled Optical-Grade Polycarbonate Nanocomposite

2012 ◽  
Vol 214 ◽  
pp. 31-34
Author(s):  
Fu Quan Guo ◽  
Ying Ying Li ◽  
Bin Guo ◽  
Hao Liang
Keyword(s):  
Electron Microscopy ◽  
Great Increase ◽  
X Ray Diffraction ◽  
X Ray ◽  
Organic Montmorillonite ◽  
Modified Montmorillonite ◽  
Mechanical Measurements ◽  
Transmission Electron ◽  
Izod Impact ◽  
Optical Disks

Optical–grade polycarbonate (PC) was separated from optical disks by a chemical approach and used to prepare nanocomposite to make full use of the wasted polymers. A quaternary ammonium-modified montmorillonite (organic montmorillonite, OMMT) was chosen as a modifier and an auxiliary functional resin (CBT160) was utilized to exfoliate the layers of montmorillonite. The characterization results of X-ray diffraction (XRD) and transmission electron microscopy (TEM) for PC/ OMMT (5wt %) revealed that an exfoliation structure of the nanocomposite was obtained. The mechanical measurements show a great increase in tensile strength and Izod impact strength of PC/ OMMT nanocomposite compared with the recycled optical–grade PC.

UTILIZATION OF FLY ASH AND CONCRETE RESIDUE IN THE PRODUCTION OF GEOPOLYMER BRICKS

2017 ◽  
Vol 12 (1) ◽  
pp. 63-77 ◽  
Author(s):  
Siriporn Sirikingkaew ◽  
Nuta Supakata
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Compressive Strength ◽  
Phase Composition ◽  
Fly Ash ◽  
Industrial Waste ◽  
X Ray Diffraction ◽  
X Ray ◽  
Scanning Electron

This study presents the development of geopolymer bricks synthetized from industrial waste, including fly ash mixed with concrete residue containing aluminosilicate compound. The above two ingredients are mixed according to five ratios: 100:0, 95:5, 90:10, 85:15, and 80:20. The mixture's physico-mechanical properties, in terms of water absorption and the compressive strength of the geopolymer bricks, are investigated according to the TIS 168-2546 standard. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) analyses are used to investigate the microstructure and the elemental and phase composition of the brick specimens. The results indicate that the combination of fly ash and concrete residue represents a suitable approach to brick production, as required by the TIS 168–2546 standard.

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