scholarly journals Study of the iron nanoparticles phase transformation during thermal annealing

Author(s):  
Artem Kozlovskiy ◽  
Jumat Kargin ◽  
Malik Kokarev ◽  
Daut Mukhambetov

Change in structural properties and phase composition of nanoparticles based on iron oxide was researched in the paper. As a result of conducted studies it was found that during heat treatment oxide phases of (γ-Fe2O3) and α-Fe2O3 maghemite were formed in oxygen atmosphere. Researches of powder array magnetization were showed that the hysteresis loop movement had the form characteristic for ferromagnetic materials. Additionally, loops obtained at different directions of the magnetic field have different characters, which indicate the magnetic anisotropy presence in the samples.

Author(s):  
Sheng Bao ◽  
Shengnan Hu ◽  
Yibin Gu

The objective of this research is to explore the correlation between the piezomagnetic response and ratcheting failure behavior under asymmetrical cyclic stressing in X80 pipeline steel. The magnetic field variations from cycle to cycle were recorded simultaneously during the whole-life ratcheting test. Analysis made in the present work shows that the piezomagnetic hysteresis loop evolves systematically with the number of cycles in terms of its shape and position. Corresponding to the three-stage process in the mechanical response, piezomagnetic response can also be divided into three principal stages, but the evolution of magnetic parameter is more complex. Furthermore, the loading branch and unloading branch of the magnetic field-stress hysteresis loop separate gradually from each other during ratcheting failure process, leading to the shape of hysteresis loop changes completely. Therefore, the progressive degradation of the steel under ratcheting can be tracked by following the evolution of the piezomagnetic field. And the shape transition of the hysteresis loop can be regarded as an early warning of the ratcheting failure.


1945 ◽  
Vol 18 (1) ◽  
pp. 8-9 ◽  
Author(s):  
Eugénie Cotton-Feytis

Abstract From the standpoint of its magnetic anisotropy, stretched rubber is comparable in a first approximation to a uniaxial crystal, in which the direction of the axis is the same as the direction of elongation. It is possible to measure this anisotropy by means of the oscillation method used by Krishnan, Guha and Banerjee in studying crystals. The sample to be examined is suspended in a uniform horizontal magnetic field in such a manner that its axis is horizontal. It is then so arranged that the torsion of the suspension wire is zero when the rubber sample is in a position of equilibrium in the field. The times of oscillation T′ and T for very small angular displacements around this position, in the presence and then in the absence of the magnetic field, are then recorded. In this way the difference between the specific susceptibilities in the direction of the axis and in the horizontal direction perpendicular to the axis is calculated by application of the equation:


1999 ◽  
Vol 32 (1-4) ◽  
pp. 289-294
Author(s):  
V. A. Lukshina ◽  
N. V. Dmitrieva ◽  
A. P. Potapov

For nanocrystalline alloy Fe73.5Cu1Nb3Si13.5B9 thermomechanical treatment was carried out simultaneously with nanocrystallizing annealing (1) or after it (2). It was shown that a change in magnetic properties for the case 1 is essentially greater than for the case 2. Complex effect of thermomagnetic and thermomechanical treatments on magnetic properties was studied in the above-mentioned nanocrystalline alloy as well as in the amorphous alloy Fe5Co70.6Si15B9.4., During the annealings both field and stress were aligned with the long side of the specimens. It was shown that the magnetic field, AC or DC, decreases an effect of loading. Moreover, the magnetic field, AC or DC, applied after stress-annealing can destroy the magnetic anisotropy already induced under load.


2008 ◽  
Vol 59 ◽  
pp. 1-10 ◽  
Author(s):  
Outi Söderberg ◽  
Ilkka Aaltio ◽  
Yan Ling Ge ◽  
Xu Wen Liu ◽  
Simo Pekka Hannula

In the shape memory alloys (SMAs) the thermal triggering induces reversible dimensional change by the phase transformation – these materials may also be ferrior ferromagnetic, however, here only the ferromagnetic SMAs are discussed. In certain SMAs the austenitemartensite phase transformation is influenced by the magnetic field as either austenite or martensite is promoted by the field and this is exploited for the dimensional changes. However, in the magnetic shape memory (MSM) alloys no phase transformation occurs as the remarkable dimensional changes take place by the twin variant changes in the martensitic phase activated by the external magnetic field at constant temperature. In addition to the phase transformation or magnetic shape memory effect, the applied magnetic field may also result in the conventional magnetostriction (MS), enhance the superelasticity (magneticfieldassisted superelasticity MFAS) or induce the giant magnetocaloric effect (GMCE). Certain alloys such as NiMnGa may even be multifunctional showing more than one of these effects. The present paper gives an overview of the different types of the magnetically activated SMA alloys, their properties as well as their potentials for applications in the frameworks of the recent studies.


2003 ◽  
Vol 45 (3) ◽  
pp. 503-507 ◽  
Author(s):  
V. V. Randoshkin ◽  
V. A. Polezhaev ◽  
N. N. Sysoev ◽  
Yu. N. Sazhin ◽  
V. N. Dudorov

1974 ◽  
Vol 52 (17) ◽  
pp. 1622-1627 ◽  
Author(s):  
A. J. Slavin ◽  
W. R. Datars

The de Haas–van Alphen effect and the h.c.p.–f.c.c. phase transformation of ytterbium were studied with the magnetic field along the [0001] direction in the h.c.p. phase, using pressures up to 4 kbar. Solid helium was used as the pressure medium. The pressure dependence of the three dHvA frequencies in the h.c.p. phase for the [0001] magnetic field direction was linear within experimental error with dF/dP = −1.2 ± 0.2 T/kbar for F(P = 0) of 35.4 T, dF/dP = 0.30 ± 0.03 T/kbar for F(P = 0) of 142.5 T, and dF/dP = −0.78 ± 0.10 T/kbar for F(P = 0) of 156.4 T. The dHvA amplitude in the h.c.p. phase was independent of pressure up to the phase transition and no dHvA effect was observed in the f.c.c. phase. The pressure of the phase transformation at 1.2 K was determined to be 2.15 ± 0.05 kbar.


2012 ◽  
Vol 511 (1) ◽  
pp. 63-69 ◽  
Author(s):  
Z. Orolínová ◽  
A. Mockovčiaková ◽  
V. Zeleňák ◽  
M. Myndyk

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