The Effect of Precursors Concentration on the Structure and Micromagnetic Properties of Ultrafine Iron Oxides Obtained by Sol-Gel Route
2016 ◽
Vol 3
(1)
◽
pp. 38-45
Keyword(s):
Sol Gel
◽
Nanodispersed composite materials -Fe2O3/-Fe2O3 were obtained by thermaldecomposition of iron citrate xerogel hydrate synthesized by iron nitrate and citrate acid solutionswith different colloidal solutions of Fe(NO3)39H2O and С6Н8О7 Н2О for different molar ratiobetween precursors. The influence of the precursors molar concentration and calcinationtemperature on the material phase composition, crystalline and magnetic microstructure, surfacecondition was studied. Methods of X-ray diffraction, Mössbauer spectroscopy, electron microscopyand IR - spectroscopy were used.
2010 ◽
Vol 152-153
◽
pp. 1683-1686
2012 ◽
Vol 26
(26)
◽
pp. 1250141
◽
2014 ◽
Vol 789
◽
pp. 178-182
◽