Crystallographic texture of hot rolled uranium-molybdenum alloys

2021 ◽  
Vol 8 (3A) ◽  
Author(s):  
Guilherme Fernandes Nielsen ◽  
Nathanael Wagner Sales Morais ◽  
Nelson Batista de Lima

The uranium molybdenum (U-Mo) alloys have potential to be used as low enriched uranium nuclear fuel in research, test and power nuclear reactors. U-Mo alloy with composition between 7 and 10 wt% molybdenum shows excellent body centered cubic phase (γ phase) stabilization and presents a good nuclear fuel testing performance. Hot rolling is commonly utilized to produce parallel fuel plate where it promotes the cladding and the fuel alloy bonding. The mechanical deformation generates crystallographic preferential orientation, the texture, which influences the material properties. This work studied the texture evolution in hot rolled U-Mo alloys. The U7.4Mo and U9.5Mo alloys were melted in a vacuum induction furnace, homogenized at 1000°C for 5 h and then hot rolled at 650°C in three height reductions: 50, 65 and 80%. The crystalline phases and the texture were evaluated by X-ray diffraction (XRD). The as-cast and processed alloys microstructures were characterized by optical and electronic microscopies. The as-cast, homogenized and deformed alloys have γ phase. It was found microstructural differences between the U7.4Mo and U9.5Mo alloys. The homogenized treatment showed effective for microsegregation reduction and were not observed substantial grain size increasing. The deformed uranium molybdenum alloys presented α, γ, θ texture fibers. The intensity of these texture fibers changes with deformation step.

2015 ◽  
Vol 60 (3) ◽  
pp. 1789-1794 ◽  
Author(s):  
J. Kowalska ◽  
W. Ratuszek ◽  
M. Witkowska ◽  
A. Zielińska-Lipiec ◽  
M. Kowalski

Abstract Fe–23wt.%Mn–3wt.%Si–3wt.%Al alloy was cast, homogenized at 1150ºC, hot-rolled at temperatures between 1200ºC and 900ºC and next cold-rolled from 5% up to 40% reductions in thickness. Microstructure and texture of this alloy, which has a low stacking fault energy, were defined after cold-rolling. Investigation of transmission electron microscopy and X-ray diffraction showed that mechanical twinning and martensitic transformations (γfcc→εhcp and γfcc→εhcp→α′bcc) took place during cold-rolling. The crystallographic Shoji-Nishiyama (S-N) {00.2}ε║{111}γ, <11.0>ε ║ <110>γ and Kurdjumov-Sachs (K-S) {111}γ║{101}α’, <101>γ║<111>α’ relations between martensite (ε, α’) and austenite (γ), were found in the coldrolled material.


2018 ◽  
Vol 941 ◽  
pp. 1023-1028
Author(s):  
Krishna Kamlesh Verma ◽  
Subodh Kumar ◽  
Satyam Suwas

High-strength wrought magnesium alloys are one of the sought-after materials in the automotive sector owing to the demands for weight reduction in the automobiles due to fuel economy and CO2emission. However, because of low room temperature strength and formability of Mg alloys, only a few applications in wrought form have been explored with these materials. In the present investigation, a high strength, good ductility and low cost wrought magnesium alloy with Mg-Sn-Zn composition have been developed and subjected to conventional wrought processing. Hot rolling was carried out at 350°C without homogenization and after homogenization at 300°C and 330°C. The phase stability, microstructure and texture of the alloy has been investigated for as-cast, homogenized and hot rolled conditions. The compositional and microstructural characterization was carried out by Electron Probe Micro-analysis (EPMA) and optical microscopy respectively. Texture evolution was investigated by X-ray diffraction method. A strong (0002) basal texture develops after hot rolling without homogenization. The (0002) basal texture has been weekend by splitting of poles and double peak distribution when hot rolling was carried out after homogenization.


2020 ◽  
Author(s):  
Chi-Toan Nguyen ◽  
Alistair Garner ◽  
Javier Romero ◽  
Antoine Ambard ◽  
Michael Preuss ◽  
...  

JOM ◽  
2021 ◽  
Author(s):  
Chandra S. Perugu ◽  
Krishna Kamlesh Verma ◽  
H. C. Madhu ◽  
Padaikathan Pambannan

2021 ◽  
Vol 12 ◽  
pp. 63-73
Author(s):  
Ruifeng Dong ◽  
Xiaoyang Zhang ◽  
Hongchao Kou ◽  
Ling Yang ◽  
Yuhong Zhao ◽  
...  

Crystals ◽  
2021 ◽  
Vol 11 (3) ◽  
pp. 313
Author(s):  
Mohamad M. Ahmad ◽  
Hicham Mahfoz Kotb ◽  
Celin Joseph ◽  
Shalendra Kumar ◽  
Adil Alshoaibi

La2/3Cu3Ti4O12 (LCTO) powder has been synthesized by the mechanochemical milling technique. The pelletized powder was conventionally sintered for 10 h at a temperature range of 975–1025 °C, which is a lower temperature process compared to the standard solid-state reaction. X-ray diffraction analysis revealed a cubic phase for the current LCTO ceramics. The grain size of the sintered ceramics was found to increase from 1.5 ± 0.5 to 2.3 ± 0.5 μm with an increase in sintering temperature from 975 to 1025 °C. The impedance results show that the grain conductivity is more than three orders of magnitude larger than the grain boundary conductivity for LCTO ceramics. All the samples showed a giant dielectric constant (1.7 × 103–3.4 × 103) and dielectric loss (0.09–0.17) at 300 K and 10 kHz. The giant dielectric constant of the current samples was attributed to the effect of internal barrier layer capacitances due to their electrically inhomogeneous structure.


2008 ◽  
Vol 373-374 ◽  
pp. 318-321
Author(s):  
J. Liang ◽  
M.K. Lei

Effects of stacking faults in a high nitrogen face-centered-cubic phase (γΝ) formed on plasma source ion nitrided 1Cr18Ni9Ti (18-8 type) austenitic stainless steel on peak shift and peak asymmetry of x-ray diffraction were investigated based on Warren’s theory and Wagner’s method, respectively. The peak shift from peak position of the γΝ phase is ascribed to the deformation faults density α, while the peak asymmetry of the γΝ phase is characterized by deviation of the center of gravity of a peak from the peak maximum (Δ C.G.) due to the twin faults density β. The calculated peak positions of x-ray diffraction patterns are consistent with that measured for plasma source ion nitrided 1Cr18Ni9Ti stainless steel.


2009 ◽  
Vol 385 (2) ◽  
pp. 449-455 ◽  
Author(s):  
H. Palancher ◽  
N. Wieschalla ◽  
P. Martin ◽  
R. Tucoulou ◽  
C. Sabathier ◽  
...  

1996 ◽  
Vol 219 (1-2) ◽  
pp. 80-88 ◽  
Author(s):  
N. Gey ◽  
M. Humbert ◽  
M.J. Philippe ◽  
Y. Combres
Keyword(s):  

Sign in / Sign up

Export Citation Format

Share Document