Measurement of surface topography and area-specific nanohardness in the scanning force microscope

1995 ◽  
Vol 10 (10) ◽  
pp. 2503-2506 ◽  
Author(s):  
D. Scholl ◽  
M.P. Everson ◽  
R.C. Jaklevic

A Scanning Force Microscope (SFM) is employed to indent and image surfaces with sub-micron resolution. The SFM image shows the area and depth of each indentation as well as its location with respect to nearby topographic surface features. The image also reveals the surface roughness, which can set a lower limit on useful nanoindentation size. A cross section of a nitrided steel surface is measured to illustrate the method. The use of the SFM with separate tip-cantilever structures for indenting and imaging has significant advantages over other nanohardness methods for the study of samples with lateral inhomogeneities.

Metals ◽  
2021 ◽  
Vol 11 (9) ◽  
pp. 1445
Author(s):  
André Temmler ◽  
Magdalena Cortina ◽  
Ingo Ross ◽  
Moritz E. Küpper ◽  
Silja-Katharina Rittinghaus

Within the scope of this study, basic research was carried out on laser micro polishing of the tool steel 1.2379 (AISI D2) using a square, top-hat shaped intensity distribution. The influence of three different quadratic laser beam sizes (100 µm, 200 µm, 400 µm side length) and fluences up to 12 J/cm2 on the resulting surface topography and roughness were investigated. Surface topography was analyzed by microscopy, white light interferometry, spectral roughness analysis, and 1D fast Fourier transformation. Scanning electron microscopy and electrical discharge analyses indicate that chromium carbides are the source of undesired surface features such as craters and dimples, which were generated inherently to the remelting process. Particularly for high laser fluences, a noticeable stripe structure was observed, which is typically a characteristic of a continuous remelting process. Although the micro-roughness was significantly reduced, often, the macro-roughness was increased. The results show that smaller laser polishing fluences are required for larger laser beam dimensions. Additionally, the same or even a lower surface roughness and less undesired surface features were created for larger laser beam dimensions. This shows a potential path for industrial applications of laser micro polishing, where area rates of up to several m2/min might be achievable with commercially available laser beam sources.


2021 ◽  
Author(s):  
Roberta Pirazzini ◽  
Henna-Reetta Hannula ◽  
David Brus ◽  
Ruzica Dadic ◽  
Martin Scnheebeli

<p>Aerial albedo measurements and detailed surface topography of sea ice are needed to characterize the distribution of the various surface types (melt ponds of different depth and size, ice of different thicknesses, leads, ridges) and to determine how they contribute to the areal-averaged albedo on different horizontal scales. These measurements represent the bridge between the albedo measured from surface-based platforms, which typically have metre-to-tens-of-meters footprint, and satellite observations or large-grid model outputs.</p><p>Two drones were operated in synergy to measure the albedo and map the surface topography of the sea ice during the leg 5 of the MOSAiC expedition (August-September 2020), when concurrent albedo and surface roughness measurements were collected using surface-based instruments. The drone SPECTRA was equipped with paired Kipp and Zonen CM4 pyranometers measuring broadband albedo and paired Ocean Optics STS VIS (350 – 800 nm) and NIR (650-1100 nm) micro-radiometers measuring visible and near-infrared spectral albedo, and the drone Mavic 2 Pro was equipped with camera to perform photography mapping of the area measured by the SPECTRA drone.</p><p>Here we illustrate the collected data, which show a drastic change in sea ice albedo during the observing period, from the initial melting state to the freezing and snow accumulation state, and demonstrate how this change is related to the evolution of the different surface features, melt ponds and leads above all. From the data analysis we can conclude that the 30m albedo is not significantly affected by the individual surface features and, therefore, it is potentially representative of the sea ice albedo in satellite footprint and model grid areas.</p><p>The Digital Elevation Models (DEMs) of the sea ice surface obtained from UAV photogrammetry are combined with the DEMs based on Structure From Motion technique that apply photos manually taken close to the surface. This will enable us to derive the surface roughness from sub-millimeter to meter scales, which is critical to interpret the observed albedo and to develop correction methods to eliminate the artefacts caused by shadows.</p><p>The UAV-based albedo and surface roughness are highly complementary also to analogous helicopter-based observations, and will be relevant for the interpretation of all the physical and biochemical processes observed at and near the sea ice surface during the transition from melting to freezing and growing.</p>


2019 ◽  
Vol 12 (1) ◽  
pp. 9-14
Author(s):  
Isra Tariq, Fatima Maryum, Maheen Fazal, Hamza Shams, Muhammad Nauman Qureshi

PDF This paper investigates the use of chemical etching to develop repeating macro and micro geometric surface features on plain carbon steel. Important properties can be imparted in a material by the use of these surface features or textures leading to enhanced corrosion resistance in plain carbon steels. Maskant perforated with pinholes combined with standard chemical etching methods was used to create repeating features on the sample’s surface. Surface characterization was carried out using optical materials analysis microscopy and dynamic-mode imaging using an Atomic Force Microscope. Surface profiles were evaluated based on their center-to-center distance, surface topography and average surface roughness. Comparison with control sample revealed the effects of chemical etching in terms of changes in the average surface roughness and surface topography. Limitations were observed in the control of etchant flow to sample’s surface. However, the results were significant in refinement of the chemical etching methodology for this application.


Nanoscale ◽  
2020 ◽  
Author(s):  
Feifei ZHANG ◽  
Jérôme Plain ◽  
Davy Gerard ◽  
Jérôme Martin

The surface topography is known to play an important role on the near- and far- field optical properties of metallic nanoparticles. In particular, aluminum (Al) nanoparticles are commonly fabricated through...


1988 ◽  
Vol 13 (12) ◽  
pp. 1057 ◽  
Author(s):  
Dror Sarid ◽  
L. Stephen Bell ◽  
Doug Iams ◽  
Volker Weissenberger

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