Fracture Toughness of NiAl In-Situ Eutectic Composites.

1992 ◽  
Vol 273 ◽  
Author(s):  
F. E. Heredia ◽  
J. J. Valencia
Keyword(s):  
Fracture Toughness ◽  
Mechanical Tests ◽  
Layered Material ◽  
Induction Melting ◽  
Directionally Solidified ◽  
Ordered Intermetallic ◽  
Initiation Fracture Toughness ◽  
Resistance Curves ◽  
Intermetallic Compound Nial

ABSTRACTMechanical tests were performed on directionally solidified (DS) NiAl in-situ eutectic composites in order to evaluate the effect of ductile reinforcements on the fracture resistance of the B2 ordered intermetallic compound NiAl. Reinforcements consisted of i) Mo fibers, ii) Cr fibers, and iii) Cr(Mo) solid solution plates. Near stoichiometric NiAl ingots were prepared by induction melting as reference material to compare with the eutectic composites. Resistance curves were obtained for the NiAl/Mo fibrous eutectic alloy as well as for the NiAl/Cr(Mo) layered material. The initiation fracture toughness of the DS NiAl/Mo and NiAl/Cr(Mo) eutectic composites is larger than that of the stoichiometric NiAl, with the layered material. producing the better properties. The mechanisms for such increase in fracture toughness are discussed.

The Effects of in-Situ Processing Methods on the Microstructure and Fracture Toughness of V-V3Si Composites

1993 ◽  
Vol 322 ◽  
Author(s):  
M. J. Strum ◽  
G. A. Henshall ◽  
B. P. Bewlay ◽  
J. A. Sutliff ◽  
M. R. Jackson
Keyword(s):  
Fracture Toughness ◽  
Synthesis Method ◽  
Solid Solution Phase ◽  
Synthesis Methods ◽  
Induction Melting ◽  
Ductile Phase ◽  
Three Point Bending ◽  
Surface Profiling ◽  
Temperature Fracture

AbstractThe present paper describes ductile-phase toughening in V-V3Si in-situ composites that were produced by conventional arc melting (AM), cold-crucible induction melting (IM), and coldcrucible directional solidification (DS). Notched three-point bending tests were performed to determine the effects of synthesis method on the room temperature fracture toughness of eutectic compositions, which contain nearly equal volume fractions of V3Si and the V(Si) solid solution phase. Fracture toughness values ranged from 10 MPa√m for the AM eutectic to over 20 MPa√m for the IM and DS eutectic alloys. SEM fractography, fracture surface profiling, and chemical analyses were performed to correlate the toughness values with the microstructures and interstitial concentrations produced by the three synthesis methods.

Ti-Modified Niobium-Silicide Based Directionally Solidified in-situ Composites

1996 ◽  
Vol 460 ◽  
Author(s):  
B. P. Bewlay ◽  
M. R. Jackson ◽  
H. A. Lipsitt
Keyword(s):  
Solid Solution ◽  
Fracture Toughness ◽  
High Temperature ◽  
Cold Crucible ◽  
Directionally Solidified ◽  
In Situ Composites ◽  
Czochralski Crystal Growth ◽  
Three Phase ◽  
Binary Eutectic

ABSTRACTThis paper examines microstructure-property relationships in high-temperature directionally solidified (DS) in-situ composites based on Nb silicides, such as Nb3Si and Nb5Si3. These in-situ composites are based on the Nb3Si-Nb binary eutectic, and are alloyed with Ti. They were prepared using cold crucible Czochralski crystal growth. Ternary Nb-Ti-Si alloys with Ti concentrations from 9 to 45%, and Si concentrations from 10 to 25%, were directionally solidified to generate aligned two- and three-phase composites containing a Nb solid solution with Nb3Si and Nb5Si3 silicides. Fracture toughness values generally greater than 10 MPa√m were measured in these composites. For a given Si concentration, the fracture toughness of the Ti-containing composites was increased ∼ 6 MPa√m over that of the binary alloy composites. The effects of Si concentration, and a range of Nb:Ti ratios, on microstructure, phase equilibria, and fracture toughness were examined.

Microstructure and room temperature fracture toughness of directionally solidified NiAl–Mo eutectic in situ composites

2012 ◽  
Vol 21 (1) ◽  
pp. 18-25 ◽  
Author(s):  
Jian-Fei Zhang ◽  
Jun Shen ◽  
Zhao Shang ◽  
Zhou-Rong Feng ◽  
Ling-Shui Wang ◽  
...  
Keyword(s):  
Fracture Toughness ◽  
Room Temperature ◽  
Directionally Solidified ◽  
In Situ Composites ◽  
Temperature Fracture

Stretch-zone analysis by image processing for the evaluation of initiation fracture toughness of a HSLA steel

2005 ◽  
Vol 96 (8) ◽  
pp. 924-932
Author(s):  
M. Tarafder ◽  
Swati Dey ◽  
S. Sivaprasad ◽  
S. Tarafder ◽  
M. Nasipuri
Keyword(s):  
Image Processing ◽  
Fracture Toughness ◽  
Hsla Steel ◽  
Stretch Zone ◽  
Initiation Fracture Toughness

VASCOMAX T-300

Alloy Digest ◽  
1990 ◽  
Vol 39 (12) ◽  
Keyword(s):  
Heat Treatment ◽  
Fracture Toughness ◽  
Tensile Strength ◽  
High Temperature ◽  
Heat Treating ◽  
Vacuum Arc ◽  
Vacuum Induction Melting ◽  
Induction Melting ◽  
Vacuum Arc Remelting ◽  
Temperature Performance

Abstract VASCOMAX T-300 is an 18% nickel maraging steel in which titanium is the primary strengthening agent. It develops a tensile strength of about 300,000 psi with simple heat treatment. The alloy is produced by Vacuum Induction Melting/Vacuum Arc Remelting. This datasheet provides information on composition, physical properties, hardness, elasticity, and tensile properties as well as fracture toughness. It also includes information on high temperature performance as well as forming, heat treating, machining, and joining. Filing Code: SA-454. Producer or source: Teledyne Vasco.

Estimation of Fracture Toughness JIC by Miniature Specimen Hydraulic Bulge Test

2017 ◽  
Vol 898 ◽  
pp. 753-757
Author(s):  
Le Le Gui ◽  
Tong Xu ◽  
Bin An Shou ◽  
Han Kui Wang ◽  
Jing Xiang
Keyword(s):  
Fracture Toughness ◽  
Fracture Energy ◽  
Fracture Strain ◽  
Bulge Test ◽  
Miniature Specimen ◽  
Hydraulic Bulge Test ◽  
Hydraulic Bulge ◽  
Resistance Curves ◽  
Miniature Specimens ◽  
Load Deflection Curve

The fracture toughness tests and a new miniature specimen technology named hydraulic bulge test (HBT) of 3Cr1Mo1/4V at four service time were carried out. Four J-R resistance curves by single-specimen method with one inch CT specimens were obtained to compute the JIC. Different definitions of equivalent fracture strain according to the section morphologies of HBT testing specimens were compared, and fracture energy of miniature specimens with three different thicknesses (0.4mm, 0.5mm and 0.6mm) were also calculated. Results showed that the typical HBT load-deflection curve can be divided into four sections like SPT curve. Equivalent fracture strain and fracture energy EHB can be chosen as two fracture parameters for the HBT specimen. Ductile fracture toughness JIC can be related approximately linearly to both the equivalent fracture strain and fracture energy EHB.

scholarly journals Morphology and Mechanical Properties of Fossil Diatom Frustules from Genera of Ellerbeckia and Melosira

Nanomaterials ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 1615
Author(s):  
Qiong Li ◽  
Jürgen Gluch ◽  
Zhongquan Liao ◽  
Juliane Posseckardt ◽  
André Clausner ◽  
...  
Keyword(s):  
Fracture Behavior ◽  
Three Dimensional ◽  
Mechanical Tests ◽  
Fracture Force ◽  
Thickness Change ◽  
X Ray ◽  
Transmission Electron ◽  
Percentage Concentration ◽  
Morphology Characterization

Fossil frustules of Ellerbeckia and Melosira were studied using laboratory-based nano X-ray tomography (nano-XCT), transmission electron microscopy (TEM) and energy-dispersive X-ray spectroscopy (EDS). Three-dimensional (3D) morphology characterization using nondestructive nano-XCT reveals the continuous connection of fultoportulae, tube processes and protrusions. The study confirms that Ellerbeckia is different from Melosira. Both genera reveal heavily silicified frustules with valve faces linking together and forming cylindrical chains. For this cylindrical architecture of both genera, valve face thickness, mantle wall thickness and copulae thickness change with the cylindrical diameter. Furthermore, EDS reveals that these fossil frustules contain Si and O only, with no other elements in the percentage concentration range. Nanopores with a diameter of approximately 15 nm were detected inside the biosilica of both genera using TEM. In situ micromechanical experiments with uniaxial loading were carried out within the nano-XCT on these fossil frustules to determine the maximal loading force under compression and to describe the fracture behavior. The fracture force of both genera is correlated to the dimension of the fossil frustules. The results from in situ mechanical tests show that the crack initiation starts either at very thin features or at linking structures of the frustules.

scholarly journals Effect of Mechanical Pretreatments on Damage Mechanisms and Fracture Toughness in CFRP/Epoxy Joints

Materials ◽  
2021 ◽  
Vol 14 (6) ◽  
pp. 1512
Author(s):  
Chiara Morano ◽  
Ran Tao ◽  
Marco Alfano ◽  
Gilles Lubineau
Keyword(s):  
Fracture Toughness ◽  
Carbon Fiber ◽  
Carbon Fibers ◽  
Polymer Matrix ◽  
Mechanical Tests ◽  
Adhesive Joints ◽  
Fiber Reinforced Polymers ◽  
Composite Joints ◽  
Damage Mechanisms ◽  
Grit Blasting

Adhesive bonding of carbon-fiber-reinforced polymers (CFRPs) is a key enabling technology for the assembly of lightweight structures. Surface pretreatment is necessary to remove contaminants related to material manufacturing and ensure bond reliability. The present experimental study focuses on the effect of mechanical abrasion on the damage mechanisms and fracture toughness of CFRP/epoxy joints. The analyzed CFRP plates were provided with a thin layer of surface epoxy matrix and featured enhanced sensitivity to surface preparation. Various degrees of morphological modification and fairly controllable carbon fiber exposure were obtained using sanding with emery paper and grit-blasting with glass particles. In the sanding process, different grit sizes of SiC paper were used, while the grit blasting treatment was carried by varying the sample-to-gun distance and the number of passes. Detailed surveys of surface topography and wettability were carried out using various methods, including scanning electron microscopy (SEM), contact profilometry, and wettability measurements. Mechanical tests were performed using double cantilever beam (DCB) adhesive joints. Two surface conditions were selected for the experiments: sanded interfaces mostly made of a polymer matrix and grit-blasted interfaces featuring a significant degree of exposed carbon fibers. Despite the different topographies, the selected surfaces displayed similar wettability. Besides, the adhesive joints with sanded interfaces had a smooth fracture response (steady-state crack growth). In contrast, the exposed fibers at grit-blasted interfaces enabled large-scale bridging and a significant R-curve behavior. While it is often predicated that quality composite joints require surfaces with a high percentage of the polymer matrix, our mechanical tests show that the exposure of carbon fibers can facilitate a remarkable toughening effect. These results open up for additional interesting prospects for future works concerning toughening of composite joints in automotive and aerospace applications.

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