Effect of Mode-Mixity and Porosity on Interfacial Fracture of Low-k Dielectrics

2004 ◽  
Vol 812 ◽  
Author(s):  
Caroline C. Merrill ◽  
Paul S. Ho

AbstractIn this study, we developed a system allowing interfacial adhesion measurements as a function of mode-mixity, from pure tension to pure shear. Results show that the debonding energy increases, by a factor of 3 to 10, as the amount of shear stress increases, approaching mode II conditions. For low k dielectrics, the debonding energy was found to decrease with increasing porosity and increase with increasing plasticity. The crack propagation is also dependent on mode-mixity.

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Elsiddig Elmukashfi

AbstractA method for determining the critical tearing energy in rubber-like materials is proposed. In this method, the energy required for crack propagation in a rubber-like material is determined by the change of recovered elastic energy which is obtained by deducting the dissipated energy due to different inelastic processes from the total strain energy applied to the system. Hence, the classical method proposed by Rivlin and Thomas using the pure shear tear test is modified using the actual stored elastic energy. The total dissipated energy is evaluated using cyclic pure shear and simple shear dynamic experiments at the critical stretch level. To accurately estimate the total dissipated energy, the unloading rate is determined from the time the crack takes to grow an increment. A carbon-black-filled natural rubber is examined in this study. In cyclic pure shear experiment, the specimens were cyclically loaded under quasi-static loading rate of $$0.01~{\rm {s}}^{-1}$$ 0.01 s - 1 and for different unloading rates, i.e. $$0.01$$ 0.01 , $$0.1$$ 0.1 and $$1.0~{\rm {s}}^{-1}$$ 1.0 s - 1 . The simple shear dynamic experiment is used to obtain the total dissipated energy at higher frequencies, i.e. $$0.5$$ 0.5 -$$18~{\rm {Hz}}$$ 18 Hz which corresponds to unloading rates $$0.46$$ 0.46 -$$16.41~{\rm {s}}^{-1}$$ 16.41 s - 1 , using the similarities between simple and pure shear deformation. The relationship between dissipated energy and unloading stretch rate is found to follow a power-law such that cyclic pure shear and simple shear dynamic experiments yield similar result. At lower unloading rates (i.e. $${\dot{\lambda }}_{\rm {U}} < 1.0~{\rm {s}}^{-1}$$ λ ˙ U < 1.0 s - 1 ), Mullins effect dominates and the viscous dissipation is minor, whereas at higher unloading rates, viscous dissipation becomes significant. At the crack propagation unloading rate $$125.2~{\rm {s}}^{-1}$$ 125.2 s - 1 , the viscous dissipation is significant such that the amount of dissipated energy increases approximately by $$125.4\%$$ 125.4 % from the lowest unloading rate. The critical tearing energy is obtained to be $$7.04~{\rm {kJ}}/{\rm {m}}^{2}$$ 7.04 kJ / m 2 using classical method and $$5.12~{\rm {kJ}}/{\rm {m}}^{2}$$ 5.12 kJ / m 2 using the proposed method. Hence, the classical method overestimates the critical tearing energy by approximately $$37.5\%$$ 37.5 % .


2010 ◽  
Vol 25 (4) ◽  
pp. 641-647 ◽  
Author(s):  
Juan Meng ◽  
Argjenta Orana ◽  
Ting Tan ◽  
Kurt Wolf ◽  
Nima Rahbar ◽  
...  

This paper presents experimental and theoretical studies of the adhesion between the drug-eluting layer and a Parylene C primer layer in coatings present on a model drug-eluting stent. To quantify adhesion, Brazil nut sandwich specimens were prepared mimicking the layers of this coating. These samples were stressed to fracture, and the resulting initial cracks at the Parylene C/drug interface were used to measure the dependence of interfacial fracture energy of mode mixity. The mating fracture surfaces were then analyzed using scanning electron microscopy (SEM) and energy dispersive x-ray spectroscopy (EDX). The interfacial energy release rates were obtained over a wide variety of mode mixities. Adhesion and fracture mechanics models were then used to estimate the mode mixity dependency of interfacial fracture toughness. Fracture toughness was found to be larger under higher mode mixity than that under lower mixity and the analytical model showed close agreement with experimental results.


1992 ◽  
Vol 114 (4) ◽  
pp. 690-697 ◽  
Author(s):  
H. Salehizadeh ◽  
N. Saka

The stress intensity factors for short straight and branched subsurface cracks subjected to a Hertzian loading are calculated by the finite element method. The effect of crack face friction on stress intensity factors is considered for both straight and branched cracks. The calculations show that the straight crack is subjected to pure mode II loading, whereas the branched crack is subjected to both mode I and mode II, with ΔKI/ΔKII < 0.25. Although KI is small, it strongly influences KII by keeping the branched crack faces apart. Based on the ΔKII values and Paris’s crack growth model, the number of stress reversals required to grow a crack in a rolling component from an initial threshold length to the final spalling length was estimated. It was found that the crack propagation period is small compared with the expected bearing fatigue life. Therefore, crack propagation is not the rate controlling factor in the fatigue failure of bearings operating under normal loading levels.


2007 ◽  
Vol 348-349 ◽  
pp. 853-856
Author(s):  
Shan Suo Zheng ◽  
Lei Li ◽  
Guo Zhuan Deng ◽  
Liang Zhang

Steel reinforced high strength and high performance concrete (SRHSHPC) specimens were experimented to study the mechanical behaviors between steel and concrete interface. In experiment, interfacial bond softening process was observed, which can be explained in terms of damage along the interface, leading to progressive reduction of shear transfer capability between steel and high strength and high performance concrete (HSHPC). In this paper, bond softening process along the interface is considered in the analysis of crack-induced debonding. Interfacial bond-slip mechanism between steel and HSHPC is studied in detail based on fracture mechanics. With the help of acoustic emissions technology, the crack propagation in the interlayer was observed, thus the interfacial crack propagation and fracture model is set up. Under the assumption that the interlayer is weak concrete compared with concrete matrix, the stress field as well as displacement field around the crack tip is deduced. The characteristics of interfacial fracture process are discussed and a model for interfacial fracture process zone is built up. With this model, the size of fracture process zone can be derived. At last, the influence of the fracture process zone on interfacial fracture toughness is determined using critical fracture toughness. All these may contribute to improvement of theory for SRHSHPC composite structure.


2019 ◽  
Vol 29 (4) ◽  
pp. 646-666 ◽  
Author(s):  
M Moazzami ◽  
MR Ayatollahi ◽  
A Akhavan-Safar

This paper presents an experimental research on the length and shape of the fracture process zone of rocks under mode I, mixed mode (I + II) and mode II loading conditions for different geometries of cracked specimens made of two types of rocks, using the digital image correlation approach. Single edge notch bending (SENB) and semi-circular bend specimens are the two geometries considered. In order to investigate the effect of the specimen size on the fracture process zone length, rocks with three different sizes are produced and tested. To investigate the effect of the mode mixity on the fracture process zone length of marble and sandstone, the specimens are tested under different modes of loading. According to the experimental results, it is found that the fracture process zone length changes with mode ratio, specimen size, geometry and the material properties. The fracture process zone length increases when the mode of loading moves from mode I to mode II. Experimental results also show that fracture process zone becomes longer for specimens with larger sizes. The fracture process zone is also affected by the specimen geometry.


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