Deformation behavior and strain rate sensitivity of nanostructured materials at moderate temperatures

2005 ◽  
Vol 880 ◽  
Author(s):  
Cécilie Duhamel ◽  
Sandrine Guérin ◽  
Martin Hÿtch ◽  
Yannick Champion

AbstractStrain-rate jump tests in compression are carried out on nanostructured copper (grain size = 90 nm) at moderate temperatures (353K - 393K). Strain-rate sensitivity m is measured as a function of temperature, T, and strain rate, έ. Increasing temperature or decreasing strain rate induces an increase in the strain-rate sensitivity. For (έ, T) = (1×10-5 s-1, 393K), m is equal to 0.17 which is the highest value reported for nanocrystalline copper. These results of enhanced m are encouraging in terms of gain in ductility. The measurements emphasize the existence of a thermally activated mechanism different from the normal rate-controlling process observed for microcrystalline fcc metals.

2006 ◽  
Vol 503-504 ◽  
pp. 31-36 ◽  
Author(s):  
Johannes Mueller ◽  
Karsten Durst ◽  
Dorothea Amberger ◽  
Matthias Göken

The mechanical properties of ultrafine-grained metals processed by equal channel angular pressing is investigated by nanoindentations in comparison with measurements on nanocrystalline nickel with a grain size between 20 and 400 nm produced by pulsed electrodeposition. Besides hardness and Young’s modulus measurements, the nanoindentation method allows also controlled experiments on the strain rate sensitivity, which are discussed in detail in this paper. Nanoindentation measurements can be performed at indentation strain rates between 10-3 s-1 and 0.1 s-1. Nanocrystalline and ultrafine-grained fcc metals as Al and Ni show a significant strain rate sensitivity at room temperature in comparison with conventional grain sized materials. In ultrafine-grained bcc Fe the strain rate sensitivity does not change significantly after severe plastic deformation. Inelastic effects are found during repeated unloading-loading experiments in nanoindentations.


Metals ◽  
2020 ◽  
Vol 10 (9) ◽  
pp. 1153
Author(s):  
Ping Song ◽  
Wen-Bin Li ◽  
Yu Zheng ◽  
Jiu-Peng Song ◽  
Xiang-Cao Jiang ◽  
...  

This study investigated the deformation behavior of the Mo-10Ta alloy with a strain rate range of 102–105 s−1. The Split Hopkinson pressure bar (SHPB) experiments were conducted to investigate the influence of deformation conditions on the stress-strain relationship and strain rate sensitivity of the material within a strain rate range of 0.001–4500 s−1. The Shaped Charge Jet (SCJ) forming experiments under detonation loading was conducted to clarify the dynamic response and microstructure evolution of the material within an ultra-high strain rates range of 104–105 s−1. Based on the stress-strain relationship of Mo-10Ta alloy at high temperature (286–873 K) and high strain rate (460–4500 s−1), the influence of temperature and strain rate on the activation energy Q was analyzed. The results indicate that the material strain rate sensitivity increased with the increase in strain rate and strain. Meanwhile, the activation energy Q decreased as the temperature and strain rate increased. The plasticity of the Mo-10Ta alloy under the condition of SCJ forming was substantially enhanced compared with that under quasi-static deformation. The material grain was also refined under ultra-high strain rate, as reflected by the reduction in grain size from 232 μm to less than 10 μm.


Metals ◽  
2019 ◽  
Vol 9 (3) ◽  
pp. 344 ◽  
Author(s):  
Simon Sevsek ◽  
Christian Haase ◽  
Wolfgang Bleck

The strain-rate-dependent deformation behavior of an intercritically annealed X6MnAl12-3 medium-manganese steel was analyzed with respect to the mechanical properties, activation of deformation-induced martensitic phase transformation, and strain localization behavior. Intercritical annealing at 675 °C for 2 h led to an ultrafine-grained multi-phase microstructure with 45% of mostly equiaxed, recrystallized austenite and 55% ferrite or recovered, lamellar martensite. In-situ digital image correlation methods during tensile tests revealed strain localization behavior during the discontinuous elastic-plastic transition, which was due to the localization of strain in the softer austenite in the early stages of plastic deformation. The dependence of the macroscopic mechanical properties on the strain rate is due to the strain-rate sensitivity of the microscopic deformation behavior. On the one hand, the deformation-induced phase transformation of austenite to martensite showed a clear strain-rate dependency and was partially suppressed at very low and very high strain rates. On the other hand, the strain-rate-dependent relative strength of ferrite and martensite compared to austenite influenced the strain partitioning during plastic deformation, and subsequently, the work-hardening rate. As a result, the tested X6MnAl12-3 medium-manganese steel showed a negative strain-rate sensitivity at very low to medium strain rates and a positive strain-rate sensitivity at medium to high strain rates.


2010 ◽  
Vol 667-669 ◽  
pp. 707-712 ◽  
Author(s):  
Xiao Yan Liu ◽  
Xi Cheng Zhao ◽  
Xi Rong Yang

Ultrafine-grained (UFG) commercially pure (CP) Ti with a grain size of about 200 nm was produced by ECAP up to 8 passes using route BC at room temperature. For ECAP processing a proper die set was designed and constructed with an internal channel angle Φ of 120° and an outer arc of curvature Ψ of 20°. Strain rate sensitivity of UFG CP-Ti and CG CP-Ti were investigated by compression tests in the temperature range of 298~673K and strain rate range of 10-4~100s-1 using Gleeble simulator machine. Evolution of the microstructure during compression testing was observed using optical microscopy (OM) and transmission electron microscopy (TEM). Strain rate sensitivity value m of the UFG CP-Ti has been measured and is found to increase with increasing temperature and decreasing strain rate, and is enhanced compared to that of CG CP-Ti. Result of the deformation activation energy determination of UFG CP-Ti indicates that the deformation mechanism in UFG CP-Ti is correlated to the grain boundaries.


2013 ◽  
Vol 1513 ◽  
Author(s):  
Andrew C. Magee ◽  
Leila J. Ladani

ABSTRACTAn Al 5083 alloy with a bimodal grain size has been previously synthesized using a low-temperature milling process and consolidation via cold isostatic pressing (CIP). This material has been shown to exhibit greatly improved strength when compared to conventional aluminum alloys. Additionally, this material has shown sensitivity to test conditions. In this work, we studied the effects of temperature on the strain rate sensitivity of this material by examining its elastic and plastic properties though uniaxial tension tests conducted under a variety of conditions at temperatures up to 473 K. Serrated stress-strain curves were observed, indicating dynamic strain aging. Strain rate sensitivity was found to depend non-monotonically on the test temperature.


2015 ◽  
Vol 2015 ◽  
pp. 1-8 ◽  
Author(s):  
Ming-wei Guo ◽  
Zhen-hua Wang ◽  
Ze-an Zhou ◽  
Shu-hua Sun ◽  
Wan-tang Fu

316LN stainless steel with 0.08%N (08N) and 0.17%N (17N) was compressed at 1073–1473 K and 0.001–10 s−1. The hot deformation behavior was investigated using stress-strain curve analysis, processing maps, and so forth. The microstructure was analyzed through electron backscatter diffraction analysis. Under most conditions, the deformation resistance of 17N was higher than that of 08N. This difference became more pronounced at lower temperatures. The strain rate sensitivity increased with increasing temperature for types of steel. In addition, the higher the N content, the higher the strain rate sensitivity. Hot deformation activation energy increased from 487 kJ/mol to 549 kJ/mol as N concentration was increased from 0.08% to 0.17%. The critical strain for initiation of dynamic recrystallization was lowered with increasing N content. In the processing maps, both power dissipation ratio and unstable region increased with increasing N concentration. In terms of microstructure evolution, N promoted dynamic recrystallization kinetic and decreased dynamic recrystallization grain size. The grain growth rate was lower in 17N than in 08N during heat treatment. Finally, it was found that N favored twin boundary formation.


Author(s):  
B.O. Malomo ◽  
O.O. Fadodun ◽  
K.M. Oluwasegun ◽  
A.T. Ogunbodede ◽  
S.A. Ibitoye ◽  
...  

A framework based on the relationship between variations in cooling rates and volume fraction of reinforcements during solidification processing to enhance the deformation behavior of aluminum alloy AA6061 matrix composite produced with a hybrid system of reinforcements is investigated in this study. The aluminum matrix composite with 5 %, 10 % and 20 % volume fraction of reinforcements (Al2O3-SiC) was synthesized by infiltrating molten aluminum AA 6061 at a pouring temperature of 740 °C into prefabricated preforms of reinforcements at a pressure of 80 MPa, die preheat temperature of 300 °C and pressure holding time of 15 s using the squeeze casting method. By employing water jet spraying at the rate of 0.1, 0.2 and 0.3 kg/s and taking measurements using a K-type thermocouple, cooling rates were obtained in correspondence with varying volume fractions of reinforcements. The developed composites were sectioned and microstructural features were examined by optical microscopy. Tensile testing was conducted according to ASTM B557 standard using an MTS testing machine. It was observed that cooling rates decreased as the volume fraction of reinforcements was increased and the cooling time also increased accordingly during this process. With respect to deformation behavior, higher cooling rates are associated with an improvement in mechanical properties at 5 % and 10 % additions of hybrid reinforcement particles but this effect diminishes as the volume fraction of reinforcements was increased to 20 %. Also, the strain rate sensitivity (SRS) exponent increased considerably with strain rates and volume fraction of reinforcements, but the tensile elongation values decreased with increasing volume fraction of reinforcements; and the variations in these properties were most significant for samples containing 20% volume fraction of hybrid reinforcements.From the foregoing, it follows that an experimentally-determined optimal solidification range is critical to the enhancement of deformation parameters as the volume fraction of reinforcements is varied in a squeeze casting process.


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