scholarly journals DAA, 1-BIZ and 5-ATZ as Vapour Phase Corrosion Inhibitors for Mild Steel under Different Aggressive Atmospheric Conditions at High Temperature

2014 ◽  
Vol 36 ◽  
pp. 174-192 ◽  
Author(s):  
Vishal Saini ◽  
Harish Kumar
Keyword(s):  
Electron Microscopy ◽  
Mild Steel ◽  
Atmospheric Corrosion ◽  
Corrosion Inhibitors ◽  
Daily Life ◽  
Salt Spray ◽  
Vapour Phase ◽  
Raw Material ◽  
Atmospheric Conditions ◽  
Scanning Electron

Mild Steel and their products are main raw material for a strong infrastructure for every country which is the main demand in the race of survival, stabilization, growth and competition. Industrialization and modernization in now a days has made a strong demand of steel and their maintenance but atmospheric corrosion can aggressively accelerate the degradation of steel during their manufacturing, processing, storage and transportation. In these cases, traditional methods to prevent corrosion are not suitable which provide the scope of Vapour Phase Corrosion Inhibitors (VPCI) in industries, defense and daily life. Three new VPCI namely Diallylamine (DAA), 1-Benzylimidazole (1-BIZ) and 5-Aminotetrazole (5-ATZ) were tested for mild steel in different aggressive atmospheric conditions by Weight Loss Test, Eschke Test, Salt Spray Test, Sulphur dioxide (SO2) Test at 50 °C and results of these tests were supported by Metallurgical Research Microscopy and Scanning Electron Microscopy (SEM).

scholarly journals BIA, DPA, MBTA and DMA as Vapour Phase Corrosion Inhibitors for Mild Steel under Different Atmospheric Conditions

2013 ◽  
Vol 20 ◽  
pp. 52-66
Author(s):  
Harish Kumar ◽  
Vikas Yadav
Keyword(s):  
Mild Steel ◽  
Corrosion Inhibitors ◽  
Inhibition Efficiency ◽  
Salt Spray ◽  
Vapour Phase ◽  
Raw Material ◽  
Atmospheric Conditions ◽  
Sem Images ◽  
Corrosion Inhibition Efficiency ◽  
Diphenyl Amine

Mild steel is widely used as main raw material in fabrication of equipment, chief material of construction and as weapons. During its storage and transportation conditions, it comes in contact with aggressive environment which leads to decrease in mechanical strength and loss in useful properties. Four different vapor phase corrosion inhibitors (VPCIs) i.e. Benzaimidazole (BIA), Diphenyl amine (DPA), 2-mercapto benzothiazole (MBTA) and N,N-dimethyl aniline (DMA) were tested under different atmospheric conditions at 40 °C by Weight Loss, Eschke test, Salt Spray, SO2 test and SEM techniques. All the four VPCIs show good corrosion inhibition efficiency i.e. 65-96 %. The results obtained from all the four corrosion experiments were supported by SEM images.

ELECTROCHEMICAL INVESTIGATION OF 2-THIOHYDANTOIN DERIVATIVES AS CORROSION INHIBITORS FOR MILD STEEL IN ACIDIC MEDIUM

2021 ◽  
Author(s):  
Petar Stanić ◽  
◽  
Nataša Vukićević ◽  
Vesna Cvetković ◽  
Miroslav Pavlović ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mild Steel ◽  
Acidic Medium ◽  
Corrosion Inhibitors ◽  
Electrochemical Impedance ◽  
Electrochemical Investigation ◽  
Force Microscopy ◽  
Atomic Force ◽  
Hcl Solution ◽  
Scanning Electron

Four 2-thiohydantoin derivatives were synthesized and their corrosion inhibition properties on mild steel (MS) in 0.5M HCl solution was evaluated using usual gravimetric and electrochemical methods (weight loss, potentiodynamic polarization, electrochemical impedance spectroscopy (EIS). Morphology of the metal surface was characterized by scanning electron microscopy (SEM) and atomic force microscopy (AFM). The study has shown that these compounds provide good protection for mild steel against corrosion in the acidic medium.

Preliminary Preparation and Characterization Studies of Cellulose from Merbau (Intsia bijuga)

2012 ◽  
Vol 620 ◽  
pp. 314-319
Author(s):  
Nur Amira Mamat Razali ◽  
Fauziah Abdul Aziz ◽  
Saadah Abdul Rahman
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Alkaline Treatment ◽  
Raw Material ◽  
X Ray Diffraction ◽  
X Ray ◽  
Preliminary Preparation ◽  
Characterization Studies ◽  
Scanning Electron

Hardwood is wood from angiosperm trees. The characteristic of hardwood include flowers, endosperm within seeds and the production of fruits that contain the seeds. This paper aims to discuss the preparation and characterization of cellulose obtained from hardwood. The hardwood Merbau (Intsia bijuga) was chosen as raw material in this study. Alkaline treatment and delignification methods were used for the preparation of cellulose. Acid hydrolysis was employed to produce cellulose nanocrystal (CNC). The treated and untreated samples were characterized using x-ray diffraction (XRD) and field emission scanning electron microscopy (FE-SEM). The final product, from both trated and untreated samples were then compared.

Synthesis of NPK fertilizer from low-grade phosphate raw material

2021 ◽  
Vol 0 (0) ◽  
Author(s):  
Anar Kareeva ◽  
Uilesbek Besterekov ◽  
Perizat Abdurazova ◽  
Ulzhalgas Nazarbek ◽  
Irina Pochitalkina ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Graphical Method ◽  
Raw Materials ◽  
Xrd Analysis ◽  
Raw Material ◽  
Low Grade ◽  
Phosphate Raw Material ◽  
Npk Fertilizer ◽  
Scanning Electron ◽  
Comprehensive Study

Abstract The article presents the results of studies of the process of obtaining NPK fertilizer from low-grade phosphate raw materials with P2O5 of about 18%. Phosphate raw materials were leached with a mixture of nitric-phosphoric acids with the addition of potassium carbonate, which serves as a source of potassium in the final product. The main parameters determined were the content of the main nutrients P2O5:N:K2O, temperature and time of the leaching process. According to the graphical method, the “apparent” activation energy of the heterogeneous process is found, which is equal to 3.8 kJ/mol indicates the intradiffusion nature of the process. Methods of chemical analysis, scanning electron microscopy and XRD analysis were used for a comprehensive study of raw materials and final products.

scholarly journals Nanocrystalline Nickel Electrodeposition on Carbon Steel Using Eco-Friendly Aqueous Ananas comosus Juice

2019 ◽  
Vol 31 (11) ◽  
pp. 2425-2429
Author(s):  
J. Felicita Florence ◽  
M. Lavanya ◽  
J. Amala Infant Joice ◽  
H. Asia Thabassoom ◽  
R. Kanmani
Keyword(s):  
Electron Microscopy ◽  
Mild Steel ◽  
Ananas Comosus ◽  
Bath Composition ◽  
Corrosion Performance ◽  
Applied Current ◽  
Nickel Electrodeposition ◽  
Ft Ir ◽  
Polarization Studies ◽  
Scanning Electron

The present study aims to investigate the effect of Ananas comosus juice on nickel electrodeposition on mild steel. The effect of this additive on electrodeposition behaviour, bath composition, surface morphology and corrosion performance of the nickel electrodeposited mild steel were investigated. The bath constitutents are optimized through Hull cell experiments. To investigate the nature of the deposits, FT-IR, scanning electron microscopy, EDAX, XRD and electrochemical methods are applied. Current efficiency and polarization studies were carried out. The results confirmed the influence of Ananas comosus juice on nickel electrodeposition.

Analysis of Inclusion Microstructure in Material Engineering of Steel

2012 ◽  
Vol 568 ◽  
pp. 324-327
Author(s):  
Ding Guo Zhao ◽  
Shu Huan Wang ◽  
Ming Jian Guo
Keyword(s):  
Electron Microscopy ◽  
High Carbon Steel ◽  
Oxide Inclusion ◽  
Raw Material ◽  
High Carbon ◽  
Silicate Inclusion ◽  
Calcium Aluminates ◽  
Material Requirement ◽  
Lf Refining ◽  
Scanning Electron

The sample of oxide inclusion was obtained in the different stage of steelmaking for the 65 steel. The microstructure was observed by using scanning electron microscopy (SEM) to analyze the composition and type of inclusions. It was shown that the microscopic inclusions in the high carbon steel were mainly massive and cluster Al2O3, spherical and slope silicate inclusion, calcium-aluminates inclusions and sulphide complex inclusions. The measures including raw material requirement, improving of the converter, LF refining and continuous casting operations were put forward to decrease inclusion.

scholarly journals Water-Soluble and Biodegradable Pectin-Grafted Polyacrylamide and Pectin-Grafted Polyacrylic Acid: Electrochemical Investigation of Corrosion-Inhibition Behaviour on Mild Steel in 3.5% NaCl Media

2014 ◽  
Vol 2014 ◽  
pp. 1-9 ◽  
Author(s):  
R. Geethanjali ◽  
A. Ali Fathima Sabirneeza ◽  
S. Subhashini
Keyword(s):  
Electron Microscopy ◽  
Mild Steel ◽  
Corrosion Inhibition ◽  
Polyacrylic Acid ◽  
Water Soluble ◽  
Electrochemical Investigation ◽  
Grafted Polymers ◽  
Tafel Polarization ◽  
Inhibition Performance ◽  
Scanning Electron

Pectin-g-polyacrylamide (denoted as Pec-g-PAAm) and pectin-g-polyacrylic acid (denoted as Pec-g-PAA) were synthesized using pectin, acrylamide, and acrylic acid as starting materials. The grafted polymers were characterized using Fourier transform infrared spectroscopy (FTIR), thermogravimetric analyser (TGA), and scanning electron microscopy (SEM). The corrosion inhibition behaviour of the grafted polymers on mild steel in 3.5% NaCl was evaluated electrochemically through Tafel polarization and impedance studies. The corrosion inhibition performance of both the polymers was found to be around 85%.

Preparation of Expanded Graphite Using Recycling Graphite Rods by Microwave Irradiation

2012 ◽  
Vol 610-613 ◽  
pp. 2356-2360
Author(s):  
Hong Liang Hua ◽  
Yun Wang ◽  
Yu Jia Wang ◽  
Shi Jun Ruan ◽  
Chao Zeng ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Potassium Dichromate ◽  
Expanded Graphite ◽  
Chemical Oxidation ◽  
Raw Material ◽  
Expandable Graphite ◽  
Graphite Rods ◽  
Scanning Electron

After washing, milling and calcining, the graphite rods recycled from waste dry batteries were used as raw material to prepare expandable graphite by chemical oxidation (using acetic anhydride as inserting and potassium dichromate as oxidant), the expanded graphite was prepared from the obtained expandable graphite by microwave radiation (MW) at 1000W for 60s.The characterization of infrared spectroscopy (IR) and scanning electron microscopy (SEM) of obtained expanded graphite have been discussed. The results show that it is feasible to prepare expanded graphite using graphite rods recycled from waste dry batteries.

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