scholarly journals GENERATION OF SYNTHETICAL MEDICAL DATA BY MDR-ANALYSIS

2021 ◽  
Vol 87 (2) ◽  
pp. 37-47
Author(s):  
Оlga Titova ◽  
Zoia Hrushak ◽  
Tetiana Kravchuk ◽  
Valerii Yefymenko ◽  
Mariia Maksumiuk

Purpose: The purpose of this article is to determine the dependence of the rate of gel formation on the type of reagent-inhibitor of the gel formation process, and to study the kinetic dependences of gel formation of silicate compositions in the presence of compounds that regulate the rate of gel formation. Research methods: Direct and reverse titration, potentiometric titration, pH-metry, determination of the dynamic viscosity on a rotational viscometer, axial compression method to determine the elastic modulus were used to study the possibility of using chemical reagents as gelation inhibitors. Results: The possibility of using inorganic and organic additives to slow down the gel formation process and the effect of these additives on the strength of the gel, their thermodynamic parameters have been researched. Discussion: The adding of organic acids into the silicate composition as "crosslinking agents" slows down the gel formation process, while replacing hydrochloric acid with other gel acids that slow down the gel formation process does not lead to a decrease in the strength characteristics of these systems compared to the standard. It was found that with an increase in the gelation time, the strength of the gels decreases, and the syneresis increases; the adding of inhibitor additives insignificantly worsens the filterability of silicate compositions, which in general have bad filterability, leading to an increase in resistance during filtration at the inlet section of the sample. Observations have shown that the addition of additives-inhibitors does not affect the thermal stability of gels, regardless of the additives' nature.

1988 ◽  
Vol 53 (8) ◽  
pp. 1735-1744 ◽  
Author(s):  
Jitka Horská ◽  
Jaroslav Stejskal ◽  
Pavel Kratochvíl ◽  
Aubrey D. Jenkins ◽  
Eugenia Tsartolia ◽  
...  

An attempt was made to prepare well-defined graft copolymers by the coupling reaction between acyl chloride groups located along the backbone chain and monohydroxy-terminated grafts prepared separately. The molecular weights and the parameters of heterogeneity in chemical composition of the products were determined by light scattering and osmometry. The determination of molecular characteristics revealed that the degree of grafting was low. The results therefore could not be confronted with a statistical model at this stage. The problems encountered in the synthesis, e.g., gel formation, and the data relating to the soluble products are discussed.


2017 ◽  
Vol 128 ◽  
pp. 130-139 ◽  
Author(s):  
Haigang Xiao ◽  
Wei Ye ◽  
Xiaoping Song ◽  
Yanmin Wang ◽  
Yuantai Ma ◽  
...  

1930 ◽  
Vol 20 (4) ◽  
pp. 511-516 ◽  
Author(s):  
A. Blenkinsop

1. A volumetric method for the determination of sodium which can be separated as a triple salt (uranium zinc sodium acetate) from mixed solutions is described. The reduction of the uranium with titanous chloride, upon which it depends is shown to be quantitative.2. Calcium, magnesium, and relatively large proportions of potash do not interfere. The procedure for the removal of iron, aluminium and phosphates by gentle ignition is simple and obviates the risk of error by the introduction of sodium as an impurity in the chemical reagents necessary for precipitation methods.3. 0.1 mg. of sodium can be determined accurately.


2017 ◽  
pp. 295-318
Author(s):  
Emanuela Borgia

This paper aims at the study of the Roman province of Cilicia, whose formation process was quite long (from the 1st century BC to 72 AD) and complicated by various events. Firstly, it will focus on a more precise determination of the geographic limits of the region, which are not clear and quite ambiguous in the ancient sources. Secondly, the author will thoroughly analyze the formation of the province itself and its progressive Romanization. Finally, political organization of Cilicia within the Roman empire in its different forms throughout time will be taken into account.


MICC 90 ◽  
1991 ◽  
pp. 401-411
Author(s):  
Andrey I. Koltakov ◽  
Pavel G. Kudryavtsev
Keyword(s):  

2017 ◽  
Vol 232 ◽  
pp. 369-378 ◽  
Author(s):  
Camila Sampaio Mangolim ◽  
Thamara Thaiane da Silva ◽  
Vanderson Carvalho Fenelon ◽  
Adriane do Nascimento ◽  
Francielle Sato ◽  
...  

2003 ◽  
Vol 70 (2) ◽  
pp. 139-148 ◽  
Author(s):  
Archie CA Clements ◽  
David J Taylor ◽  
Julie L Fitzpatrick

Samples of foremilk were collected from 261 clinically normal glands of 150 ewes, and tested using the California mastitis test (CMT). Further samples were collected from 195 of these glands for determination of automated somatic cell counts (SCC), and from 60 of these glands for bacteriological assessment. The sensitivity and specificity of CMT for detecting samples with SCC above different threshold levels and for CMT and SCC in determining bacteriological status were evaluated using two-graph receiver operating characteristics (TG-ROC). Milk samples were obtained subsequently from ten CMT positive, and five CMT negative first- and second-lactation ewes. Samples were cultured using a variety of media, incubation temperatures and atmospheric conditions, immediately after collection, and 1 week after storage at 4°C and −21°C. Results suggested that CMT is best used as a diagnostic test for ovine subclinical mastitis (SCM) with a cut-off of 3 (distinct gel formation), and that automated SCC thresholds of >1200×103 cells/ml are appropriate, especially where low prevalences are expected (e.g. <5%). Additionally, this study showed that routine bacteriological methods were appropriate for isolation of most species of pathogen responsible for ovine SCM, but storage of samples prior to culture, either at 4°C or −21°C, was detrimental to the isolation of several of these organisms.


2020 ◽  
Vol 834 ◽  
pp. 82-89
Author(s):  
Evgenii Igorevich Kurkin ◽  
Vladislava Olegovna Chertykovtseva ◽  
Yaroslav Vyacheslavovich Zakhvatkin

The Brookfield_to_MATLAB and ViscosityApproximation codes for processing of experiments results for determination of viscosity on a rotational Brookfield DV3T viscometer is developed in the MATLAB. The codes allow to carry out automatic capture data, to calculate the shear rate for standard spindles RV-1 ... RV-7, to sort the measurement results on temperatures, to combine the experimental data and to determine the coefficients of the Andrade type power-law model. Paper describes experiment results on determination of viscosity of the epoxy binder reinforced by short carbon fibers. The coefficients of the viscosity model are determined by the linear regression coefficients. The obtained determination coefficient shows a good agreement of the model with the experimental data. The results are used for study various contents of a mass fraction of fibers: 0%, 5%, 10%, and 15%.


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