Effect of sports drinks on the surface properties of composite resins after prolonged exposure

Aim: Using dietary supplements may affect the properties of composite resins due to their acidic pH. The present in vitro study aimed to assess the surface roughness and color stability of two composite resins - nanohybrid (Empress Direct) and nanoparticulate (Filtek Z350) - after prolonged exposure to dietary supplements. Methods: We produced 30 specimens from each composite (8x2-mm discs) and divided them into six groups (n=10). After the initial measurement of the surface properties (roughness and color), we exposed the specimens to a degradation process in Maltodextrin and Whey Protein for 22.5 and 7.5 days, respectively, using deionized water as the control solution. At the end of 22.5 days, we reassessed the specimens. After verifying data normality with the Kolmogorov-Smirnov test, we performed ANOVA followed by Tukey’s test at 5%. Results: We found significant differences for materials immersed in the Whey Protein solution (p<0.05). The roughness of Empress Direct was higher (0.45+0.07) than Filtek Z350 (0.22+0.05). The composites tested also showed color change (ΔE>3.3) after the immersion period (p<0.001). In Maltodextrin, the Empress Direct group presented (4.52+1.23) and Filtek Z350 (4.04+0.66), while after immersion in Whey Protein, they showed (5.34+1.68) and (4.26+1.02), respectively. Conclusion: Sports drinks changed the surface roughness and color stability of the composite resins studied. The Filtek Z350 group showed lower color variation than the Empress Direct composite in both solutions evaluated.

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Surface properties of composite resins with and without fluorides for bracket bonding / Propriedades de superfície de resinas compostas com e sem fluoretos para colagem de suportes

Brazilian Journal of Development ◽

10.34117/bjdv7n7-145 ◽

2021 ◽

Vol 7 (7) ◽

pp. 67267-67276

Author(s):

Emillyn Jones Greijal Dias Holanda ◽

José Guilherme Neves ◽

Milton Santamaria-Jr ◽

Silvia Amélia Scudeler Vedovello ◽

Ana Rosa Costa ◽

...

Keyword(s):

Surface Roughness ◽

Surface Properties ◽

Color Change ◽

Composite Resins ◽

Hardness Tester ◽

Significant Difference ◽

Post Test ◽

Roughness Analysis ◽

Diamond Paste ◽

Penetration Time

The aim of this study was to evaluate the surface properties of orthodontic resins with and without fluoride. Forty disks, measuring 2 mm thick by 6 mm in diameter, were made of 4 bracket-bonding composite resins (n=10): Transbond Plus Color Change-3M/Unitek (TPCC); Transbond XT- 3M/Unitek (TXT), Orthocem -FGM (OC); Orthocem UV Trace-FGM (OCUV). The discs were photoactivated for 40 seconds with irradiance of 450 mW/cm2 and manually polished in sequence by silicon carbide sandpapers with 1200 and 2000 grain size and finished with diamond paste and felt disc. The surface microhardness analysis was performed using a Shimadzu Micro Hardness Tester HMV-2,000 (Shimadzu Corporation, Kyoto, Japan) with a load of 50 gF and a 5 second penetration time. Surface roughness readings were taken using a Surf Corder Roughness Meter (SE 1700- Kosaka, Lisboa-Portugal). For data analysis, ANOVA (one-way) was used, followed by Tukey's post-test (?=0.05). The microhardness results showed a difference (p?0.05) in the means of the orthodontic resins between TPCC and TXT with the other groups. After the surface roughness analysis, the averages showed that TPCC resin showed higher roughness compared to OC and OCUV (p?0.05), and there was no statistical difference with TXT. It was concluded that statistically the composite resins with fluoride showed significant difference regarding hardness and roughness.

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Color Stability and Surface Roughness of Hybrid and Nanofilled Composites Brushed with Abrasive Dentifrices

Journal of Health Sciences ◽

10.17921/2447-8938.2021v23n2p85-91 ◽

2021 ◽

Vol 23 (2) ◽

pp. 85-91

Author(s):

Guilherme Ortiz Pinto Cruz ◽

Larissa Martins Costa ◽

Cesar Penazzo Lepri ◽

Ruchele Dias Nogueira ◽

Regina Guenka Palma-Dibb ◽

...

Keyword(s):

Surface Roughness ◽

Laser Scanning ◽

Color Change ◽

Color Stability ◽

Composite Resins ◽

Laser Scanning Microscopy ◽

Confocal Laser ◽

Test Surface ◽

Initial Color ◽

Level Of Significance

AbstractThe aim of this study was to evaluate the color stability and the surface roughness of different composites brushed with toothpastes presenting different levels of abrasivity. Thirty discs of each material were obtained using michohybrid composites (Brilliant NG and Charisma Diamond) and a nanocomposite (Filtek Z350XT). The initial color (CIELab) and surface roughness (confocal laser scanning microscopy) of resin discs were evaluated. Afterwards, 10 specimens per group were brushed with the following dentifrices: Maximum Cavity Protection, Sensodyne Repair & Protect and Colgate Sensitive Pro-Relief. Brushing was performed with an electric toothbrush equipped with soft bristle head, with standard power and weight, for 30 minutes. Every 30 seconds, 1.0 ml of the slurry was injected between the bristles of the brush and the specimen. After abrasive challenge, the samples had their color and roughness reevaluated. Data were submitted to the Kruskal-Wallis test (color change) or the t-test (surface roughness). The level of significance was 5%. Results: Brushing did not significantly change the color of the composites tested in the study herein . On the other hand, the surface roughness of the composites was significantly affected by the abrasive challenge, regardless of the toothpaste used. The surface roughness change was similar for all the composites. The abrasive challenge with the toothpastes Maximum Cavity protection, Sensodyne Repair & Protect and Colgate Sensitive Pro-Relief was not able to significantly change the color of the composite resins. Nevertheless, the abrasive challenges significantly altered the surface roughness of all the evaluated composites. However, the changes in surface roughness were statistically similar in the microhybrid and nanofilled composites. Keywords: Composites Resins. Dentifrices. Color. ResumoO objetivo deste estudo foi avaliar a estabilidade de cor e a rugosidade superficial de diferentes resinas compostas escovadas com dentifrícios de diferentes níveis de abrasividade. Trinta discos de cada material foram obtidos utilizando compósitos micro-híbridos (Brilliant NG e Charisma Diamond) e um nanocompósito (Filtek Z350XT). A cor inicial (CIELab) e a rugosidade superficial (microscopia confocal de varredura a laser) dos discos de resina foram avaliadas. Em seguida, 10 amostras por grupo foram escovadas com os dentifrícios Máxima Proteção Anticáries, Sensodyne Repair & Protect e Colgate Sensitive Pro-Alívio. A escovação foi realizada com uma escova elétrica com cabeça de cerdas macias, com potência e peso padronizados, durante 30 minutos. A cada 30 segundos, 1,0 ml da pasta era injetada entre as cerdas da escova e a amostra. Após o desafio abrasivo, as amostras tiveram sua cor e rugosidade reavaliadas. Os dados foram submetidos ao teste de Kruskal-Wallis (alteração de cor) ou ao teste t (rugosidade da superfície) (α=5%). A escovação não alterou significativamente a cor dos compósitos. Por outro lado, a rugosidade superficial dos compósitos foi significativamente afetada pelo desafio abrasivo, independentemente do dentifrício utilizado. A alteração da rugosidade superficial foi semelhante para todos os compósitos. O desafio abrasivo com a Máxima Proteção Anticáries, o Sensodyne Repair & Protect e o Colgate Sensitive Pro-Alívio não foi capaz de alterar significativamente a cor das resinas. Diferentemente, os desafios abrasivos alteraram significativamente a rugosidade superficial de todos os compósitos avaliados. No entanto, as mudanças na rugosidade foram estatisticamente semelhantes nos compósitos micro-híbridos e nanoparticulado. Palavras-chave: Resinas Compostas. Dentifrícios. Cor.

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Varying the Polishing Protocol Influences the Color Stability and Surface Roughness of Bulk-Fill Resin-Based Composites

Journal of Functional Biomaterials ◽

10.3390/jfb12010001 ◽

2020 ◽

Vol 12 (1) ◽

pp. 1

Author(s):

Filipa Freitas ◽

Teresa Pinheiro de Melo ◽

António HS Delgado ◽

Paulo Monteiro ◽

João Rua ◽

...

Keyword(s):

Surface Roughness ◽

Surface Properties ◽

Color Change ◽

Resin Composite ◽

Color Stability ◽

Control Surface ◽

Significance Level ◽

Color Changes ◽

Atomic Force ◽

Polishing Procedures

Surface properties of composites such as roughness and color impact periodontal health and aesthetic outcomes. Novel bulk-fill composites with improved functionality are being introduced and, in light of the existing variety of finishing/polishing procedures, research of their surface properties is warranted. Sixty discs were prepared from bulk-fill composites (Filtek™ Bulk Fill Posterior Restorative and Fill-Up™) and incremental-fill Filtek™ Z250. They were further divided according to different polishing procedures (n = 5): three multi-step polishing procedures or finishing with a bur (control). Surface roughness (Ra) was measured using an atomic force microscope (The AFM Workshop TT-AFM). A spectrophotometer (Spectroshade Micro Optic) was used to determine color stability, after exposure to a coffee solution. Data were analyzed using two-way MANOVA (significance level of 5%). Resin composite type, polishing procedure, and their interaction had a statistically significant effect on surface roughness (p < 0.001) and color change (p < 0.001). Fill-Up™ exhibited the highest surface roughness and greatest color change. Differences in color change were statistically significant (p < 0.001). Filtek™ Bulk Fill registered the lowest surface roughness and color change, after the three-step polishing procedure. Both parameters were significantly correlated (ρ = 0.754, p < 0.001) and found to be material dependent and polishing-procedure dependent. Higher surface roughness relates to greater color changes.

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Influence of Different Staining Beverages on Color Stability, Surface Roughness and Microhardness of Silorane and Methacrylate-based Composite Resins

The Journal of Contemporary Dental Practice ◽

10.5005/jp-journals-10024-1536 ◽

2014 ◽

Vol 15 (3) ◽

pp. 319-325 ◽

Cited By ~ 15

Author(s):

Oguz Suleyman Özdemir ◽

Emel Karaman ◽

Duygu Tuncer ◽

Esra Firat ◽

Sevilay Karahan

Keyword(s):

Surface Roughness ◽

Statistical Analysis ◽

Aluminum Oxide ◽

Vickers Hardness ◽

Color Change ◽

Color Stability ◽

Composite Resins ◽

Distilled Water ◽

Resin Composites ◽

Water Control

ABSTRACT Aim To investigate the influence of different staining beverages on color stability, surface roughness and microhardness of silorane and methacrylate-based composite resins. Materials and methods Three different composite resins (Filtek Silorane, Filtek P60, Filtek Supreme XT) were tested. Thirty cylindrical specimens (10 × 2 mm) per material were prepared and polished with a series of aluminum-oxide polishing disks. Each group was then randomly subdivided into three groups according to the test beverages: distilled water (control), cola and coffee. The samples were immersed into different beverages for 15 days. Color, surface roughness and microhardness values were measured by a spectrophotometer, prophylometer and Vickers hardness device respectively, at baseline and after 15 days. The data were subjected to statistical analysis. Results Immersion in coffee resulted in a significant discoloration for all the composites tested, although the color change was lower in Filtek Silorane than that of MBCs (p < 0.05). All the composites tested showed similar surface roughness changes after immersion in different beverages (p > 0.05). Besides coffee caused more roughness change than others. Immersion in coffee caused highest microhardness change in Filtek Supreme XT (p < 0.05). Conclusion Cola and coffee altered, to some degree, the color, surface roughness and/or microhardness of the tested resin composites, depending on the characteristics of the materials. How to cite this article Karaman E, Tuncer D, Firat E, Ozdemir OS, Karahan S. Influence of Different Staining Beverages on Color Stability, Surface Roughness and Microhardness of Silorane and Methacrylate-based Composite Resins. J Contemp Dent Pract 2014;15(3):319-325.

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Effects of Commonly Consumed Beverages on Surface Roughness and Color Stability of the Nano, Microhybrid and Hybrid Composite Resins: An in vitro Study

The Journal of Contemporary Dental Practice ◽

10.5005/jp-journals-10024-1390 ◽

2013 ◽

Vol 14 (4) ◽

pp. 718-723 ◽

Cited By ~ 19

Author(s):

P Sarveshwar Reddy ◽

KL Sunil Tejaswi ◽

Suneeth Shetty ◽

BM Annapoorna ◽

Sudarshan C Pujari ◽

...

Keyword(s):

Surface Roughness ◽

Hybrid Composite ◽

Color Change ◽

Resin Composite ◽

Color Stability ◽

Composite Resins ◽

Resin Composites ◽

Hybrid Resin ◽

Color Changes

ABSTRACT Background Consumption of certain beverages may affect the esthetic and physical properties of the resin composite, thereby undermining the quality of restorations. Aim To analyze the effect of three beverages (cola, coffee, tea) on color stability and surface roughness of three different types of resin composites at various time intervals in vitro. Materials and methods Nano, microhybrid and hybrid resin composites were used. Each material was randomly divided into four equal subgroups of 10 samples each according to the beverages used (cola, coffee, tea, distilled water). The samples were immersed in each beverage for 1, 15 and 30 days. Surface roughness and color changes measurements were noted at the baseline—the first, fifteenth and thirteenth day. Results It was found that nanoresin composite followed by microhybrid and hybrid showed least surface roughness and color change. The Coke beverage subgroup showed more surface roughness and the subgroup coffee has shown more color changes with respect to other subgroups. Conclusion All specimens showed discoloration after completion of the test period which was visually perceptible and clinically unacceptable. At the end of 30th day, among the materials, nanofilled composite resin showed comparatively less surface roughness and color change than microhybrid and hybrid composite resins. How to cite this article Reddy PS, Tejaswi KLS, Shetty S, Annapoorna BM, Pujari SC, Thippeswamy HM. Effects of Commonly Consumed Beverages on Surface Roughness and Color Stability of the Nano, Microhybrid and Hybrid Composite Resins: An in vitro Study. J Contemp Dent Pract 2013;14(4): 718-723.

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Effect of an Optical Whitening Toothpaste on Color Stability of Tooth-Colored Restorative Materials

European Journal of Dentistry ◽

10.1055/s-0040-1705071 ◽

2020 ◽

Vol 14 (01) ◽

pp. 085-091

Author(s):

Sedighe Sadat Hashemikamangar ◽

Farnoosh Hoseinpour ◽

Nazanin Kiomarsi ◽

Mehrzad Gholampour Dehaki ◽

Mohammad Javad Kharazifard

Keyword(s):

Statistical Analysis ◽

Color Change ◽

Color Stability ◽

Composite Resins ◽

Time Points ◽

Color Changes ◽

Honestly Significant Difference ◽

Significant Difference ◽

Resin Modified Glass Ionomer ◽

Composite Samples

Abstract Objectives This study aimed to assess the effect of an optical whitening toothpaste on color stability of microhybrid, nanofilled, and microfilled composite resins and resin-modified glass ionomer (RMGI) cement in comparison of two other toothpastes. Materials and Methods In this experimental study, disc-shaped composite samples were fabricated. The samples were then polished using silicon carbide papers. Twenty-seven samples of each material were fabricated and subjected to colorimetry using a spectrophotometer. Each group of material was then divided into three subgroups for the application of conventional whitening and whitening containing blue covarine toothpastes. One operator brushed the samples with an electric soft toothbrush with circular motion twice a day, each time for 30 seconds. Colorimetry was performed at 0, 1, 7, 30, and 90 days. Statistical Analysis Two-way analysis of variance (ANOVA), one-way ANOVA, and Tukey’s honestly significant difference (HSD) test were used for statistical analysis. Results The interaction effect of type of restorative material and time on ∆E was not significant at baseline or 1 day (p > 0.05). The effect of type of toothpaste on ∆E was not significant at baseline or 1 day (p = 0.78) but the effect of type of material was significant (p < 0.05). The toothpastes had significantly different effects on ∆E of Z250 at all time points (p < 0.05) except for ∆E0–30 (p = 0.106). The toothpastes had significantly different effects on ∆E of Z350 and Gradia at all time points (p < 0.05). The same was true for RMGI except for ∆E0–7 (p = 0.43) and ∆E0–90 (p = 0.52). The majority of color changes caused by toothpastes were not clinically perceivable (∆E < 3.3), except for ∆E0–90 by the whitening toothpaste (∆E = 9), ∆E0–90 by the conventional toothpaste for Z350 (∆E = 3.9), and ∆E0–1 by the whitening toothpaste for RMGI (∆E = 3.7). Conclusion The color change of all composite samples was not clinically perceivable (<3.3) at all time points, which shows that the tested toothpastes do not cause a significant change in color of composite materials.

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Bioadhesive Curcumin-Mediated Photodynamic Inactivation and Its Potential to Cause Undesirable Effects on Dental and Restorative Surfaces

Pharmaceutics ◽

10.3390/pharmaceutics13091458 ◽

2021 ◽

Vol 13 (9) ◽

pp. 1458

Author(s):

Bárbara Donadon Reina ◽

Carolina Santezi Neto ◽

Patrícia Petromilli Nordi Sasso Garcia ◽

Marlus Chorilli ◽

Giovana Maria Fioramonti Calixto ◽

...

Keyword(s):

Surface Roughness ◽

Liquid Crystal ◽

Tooth Enamel ◽

Dental Enamel ◽

Color Stability ◽

Composite Resins ◽

Photodynamic Inactivation ◽

Restorative Material ◽

Negative Effects ◽

Restorative Materials

Curcumin-mediated Photodynamic Inactivation (PDI) has shown great potential to disinfect specific sites on tooth enamel but may involve contact with restorative materials. Thus, before use in dentistry, it is necessary to investigate whether the PDI protocol causes undesirable changes in the surfaces of aesthetic restorative materials and dental enamel. This study investigated the effect of PDI mediated by curcumin (CUR) in a liquid crystal precursor system on color stability (ΔE), surface roughness (Ra), and microhardness (kgf) of three different composite resins and bovine dental enamel specimens. The microhardness and roughness readings were performed 60 days after the treatments while the color readings were performed immediately, 24, 48, and 72 h, 7, 14, 21, 30, and 60 days after the treatments. Results showed that CUR mediated-PDI does not seem to have the potential to promote any esthetic or mechanical changes to the surface of tooth enamel and can be applied safely in clinical practice. However, the results on color, roughness, and hardness obtained for composite resins show that some negative effects can be produced, depending on the type of restorative material; more experiments must be performed with different formulations and, perhaps, with lower concentrations of CUR.

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Evaluation of color change in acrylic and bisacrylic resin resins in different solutions

Journal of Research in Dentistry ◽

10.19177/jrd.v5e4201776-84 ◽

2018 ◽

Vol 5 (4) ◽

pp. 76

Author(s):

Mone Laiz Bortoli ◽

Cristina Von Appen ◽

Camila Longoni ◽

Carmen Beatriz Borges Fortes ◽

Jefferson Tomio Sanada

Keyword(s):

Color Change ◽

Color Stability ◽

Acrylic Resin ◽

Color Variation ◽

Color Reading ◽

Control Group ◽

Color Changes ◽

Significant Difference ◽

Prosthesis Material ◽

Chlorhexidine Solution

Aim: This work aimed to evaluate the color stability of an acrylic resin chemically activated (ARCA) using different handling techniques, and a bisacrylic resin when exposed to different pigmentation solutions.Material and Methods: Silicon matrixes were confectioned (10x10x3mm) to be used as specimens. The groups were designed as follows: Group Pot, Group Brush, Group Manufacturer and Group Bisacrylic (n=18). Each group was exposed to three different pigmentation solutions: distilled water, coke and chlorhexidine digluconate 0.12%. Three readings were performed for each specimen using a spectrophotometer, and the evaluations were carried out in three different time. After the color reading, three averages and the standard deviation of variation were performed after 24 hours (T1), 7 days (T2) and 14 days (T3). Data were submitted to the ANOVA and 2 criteria and Tukey (P<0.05) in the statistical software SSPS 18 for Macintosh (SPSS Inc., Chicago, USA).Results: When compared the solutions in each group of material, there was no statistically significant difference, except for T3, where the group Dencor Brush and Bisacrylic demonstrated higher color variation in all the solutions, even in the control group, and the values in Chlorhexidine higher than the other, showing greater instability after 14 days.Conclusions: With the results, bisacrylic resin used as provisory prosthesis material presents greater color instability than the ARCA, when submitted to different solutions. Bisacrylic resin and Dencor Brush present significantly visible color changes in chlorhexidine solution after 14 days. All the materials in coke solution present homogeneity in the color change after 7 days exposition to the solution, with no visible color change.

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Evaluation of the color stability and surface roughness of dual-cure, bulk-fill composites

International Dental Research ◽

10.5577/intdentres.2021.vol11.suppl1.39 ◽

2021 ◽

Vol 11 (Suppl. 1) ◽

pp. 266-273

Author(s):

Zehra Şivgan Güner ◽

Behiye Bolgül ◽

Tacettin İnandı

Keyword(s):

Surface Roughness ◽

Color Stability ◽

Pediatric Dentistry ◽

Ease Of Use ◽

Composite Resins ◽

Distilled Water ◽

Significant Difference ◽

Cherry Juice ◽

Experimental Group ◽

Composite Samples

Aim: In recent years, tooth-colored, dual-cure, bulk-fill composite resins, which have attracted attention for their ease of use, constitute one of the latest developments in pediatric dentistry applications. This study aimed to evaluate the color stability and surface roughness properties of three different dual-cure, bulk-fill materials and one light-cure, bulk-fill composite material used in pediatric dentistry. Methodology: In this study, three different dual-cure, bulk-fill composites (Fill-Up, HyperFIL, Cention-N) and one light-polymerized bulk-fill composite (Reveal HD) were used. A total of 70 samples were obtained for surface roughness testing. The surface roughness testing was performed with a Hysitron TI 950 Triboindenter device. A total of 105 samples were obtained for the evaluation of color stability. Cherry juice, iced tea, and distilled water were used as solutions. Initial and final color measurements were made using a spectrophotometer. The color differences between measurements were recorded according to the CIEDE 2000 system. Results: The least surface roughness among the composite groups was observed in the light polymerized Cention-N composite samples in the experimental group. In the Fill-Up and Cention-N composite groups in the experimental group, the surface roughness of the samples left to self-polymerization and the samples polymerized with light showed a statistically significant difference (p < 0.05). Among the composite groups, the highest amount of coloring was observed in the Fill-Up composite samples, which were left to self-polymerization and kept in cherry juice in the experimental group. The least coloration among the composite groups was observed in the Cention-N composite samples polymerized with light and kept in distilled water. Conclusion: Based on this information, a decrease in surface roughness and an increase in color stability can be expected due to self-polymerization and the light polymerization of dual-cured, bulk-fill composites. How to cite this article: Şivgan Güner Z, Bolgül B, İnandı T. Evaluation of the color stability and surface roughness of dual-cure, bulk-fill composites. Int Dent Res 2021;11(Suppl.1):266-273. https://doi.org/10.5577/intdentres.2021.vol11.suppl.39 Linguistic Revision: The English in this manuscript has been checked by at least two professional editors, both native speakers of English.

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