scholarly journals Characterizing Complex Mineral Structures in Thin Section of Geological Sample with a Scanning Hall Effect Microscope

Author(s):  
Jefferson F. D. F. Araujo ◽  
Andre L. A. dos Reis ◽  
Vanderlei C. Oliveia ◽  
Amanda F. Santos ◽  
Cleanio Luz-Lima ◽  
...  

We improved a magnetic scanning microscope for measuring the magnetic properties of minerals in thin sections of geological samples at submillimeter scales. The microscope is comprised of a 200 µm diameter Hall sensor that is 142 µm from the sample; an electromagnet capable of applying to the sample up to 500 mT dc magnetic fields over a 40 mm diameter region; a second Hall sensor arranged in a gradiometric configuration to cancel the background signal applied by the electromagnet and reduce overall noise in the system; a custom-designed electronics to bias the sensors and provide adjustment for background signal cancelation; and a scanning XY stage with micrometer resolution. Our system achieves a spatial resolution of  220 µm with noise at 6.0 Hz of »300 nTrms/(Hz)1/2 in an unshielded environment. The magnetic moment sensitivity is 1.3 × 10−11 Am2.1/2 We successfully measured the representative magnetization of a geological sample using an alternative model that takes into account the sample geometry and identified different micrometric characteristics in the sample slice.

Sensors ◽  
2019 ◽  
Vol 19 (7) ◽  
pp. 1636 ◽  
Author(s):  
Jefferson Araujo ◽  
Andre Reis ◽  
Vanderlei Oliveira ◽  
Amanda Santos ◽  
Cleanio Luz-Lima ◽  
...  

We improved a magnetic scanning microscope for measuring the magnetic properties of minerals in thin sections of geological samples at submillimeter scales. The microscope is comprised of a 200 µm diameter Hall sensor that is located at a distance of 142 µm from the sample; an electromagnet capable of applying up to 500 mT DC magnetic fields to the sample over a 40 mm diameter region; a second Hall sensor arranged in a gradiometric configuration to cancel the background signal applied by the electromagnet and reduce the overall noise in the system; a custom-designed electronics system to bias the sensors and allow adjustments to the background signal cancelation; and a scanning XY stage with micrometer resolution. Our system achieves a spatial resolution of 200 µm with a noise at 6.0 Hz of 300 nTrms/(Hz)1/2 in an unshielded environment. The magnetic moment sensitivity is 1.3 × 10−11 Am2. We successfully measured the representative magnetization of a geological sample using an alternative model that takes the sample geometry into account and identified different micrometric characteristics in the sample slice.


2018 ◽  
Vol 56 (1) ◽  
pp. 64
Author(s):  
Nguyen Thanh Tung ◽  
Nguyen Thi Mai ◽  
Ngo Tuan Cuong

The optimized geometries, stability, and magnetic properties of cationic clusters Si7+, Si6Mn+, and Si5Mn2+ have been determined by the method of density functional theory using the B3P86/6-311+G(d) functional/basis set. Their electronic configurations have been analyzed to understand the influence of substituting Si atoms by Mn atoms on the structural and magnetic aspects of Si7+. It is shown that the manganese dopant does not alter the structure of the silicon host but significantly changes its stability and magnetism. In particular, while the magnetic moment of Si7+ is 1 mB, Si5Mn2+ exhibits a strong magnetic moment of 9 mB and that of Si6Mn+ takes a relatively high value of 4 mB. Among studied clusters, the pentagonal bipyramid Si5Mn2+ is assigned as the most stable one.


RSC Advances ◽  
2014 ◽  
Vol 4 (85) ◽  
pp. 45598-45602 ◽  
Author(s):  
Palash Nath ◽  
Anirban Chakraborti ◽  
D. Sanyal

Effective magnetic moment for Zn54O53X (X = B, C, N, F, Al, Si, P, Cl, Ga, Ge, As) system.


2018 ◽  
Vol 185 ◽  
pp. 04021
Author(s):  
Alexander Inishev ◽  
Evgeny Gerasimov ◽  
Nikolay Mushnikov ◽  
Pavel Terentev ◽  
Vasily Gaviko

The magnetic and magnetothermal properties of the non-stoichiometric TbCo2Nix (0 ≤ x ≤ 0.2) alloys were studied. It was found that the concentration dependence of the Curie temperature and magnetic moment of the 3d-sublattice have a maximum at x = 0.025. The obtained experimental magnetic properties of the TbCo2Nix alloys were discussed under assumption that the Co magnetic moment in the compounds changes with increasing x. The magnetic entropy change was determined using the temperature dependences of the magnetization and Maxwell’s thermodynamic relation. The obtained results for TbCo2Nix were compared with those for the ErCo2Mnx alloys.


RSC Advances ◽  
2018 ◽  
Vol 8 (35) ◽  
pp. 19732-19738 ◽  
Author(s):  
Jinsen Han ◽  
Dongdong Kang ◽  
Jiayu Dai

The migration and magnetic properties of the bilayer graphene with intercalation compounds (BGICs) with magnetic elements are theoretically investigated based on first principles study.


2002 ◽  
Vol 57 (10) ◽  
pp. 1129-1132 ◽  
Author(s):  
A. Elmali ◽  
Y. Elerman ◽  
I. Svoboda

The mixed-ligand dinuclear complex (2,2'-dipyridyl)-(2-acetylphenolato)copper(II) perchlorate was synthesized and its crystal structures determined. The structure consists of a dimeric unit involving a planar Cu2O2 group. The coordination sphere of the Cu atom can be described as an alongated octahedron where the basal plane is formed by the two N atoms of the 2,2'-dipyridyl molecule and the two O atoms of the acetophenon anion. Two apical Cu - O contacts complete the 4+2 coordination of the Cu atoms. They correspond to one of the O atoms of the perchlorate anion and to the O atom of the second unit. Magnetic susceptibility data obey the Curie-Weiss law with θ = -8.1(2) K. The decreasing of the effective magnetic moment from 1.94(8) μB at 300 K to 1.86(8) μB at 70 K and the negative Weiss constant indicate weak antiferromagnetic interactions between the two copper atoms in the dimeric units.


2020 ◽  
Vol 35 (1) ◽  
pp. 145-154 ◽  
Author(s):  
Lanping Feng ◽  
Lian Zhou ◽  
Wenfeng Hu ◽  
Wen Zhang ◽  
Baichan Li ◽  
...  

Simple, fast and efficient column separation of Mo from geological sample matrices using the TRU resin.


2015 ◽  
pp. 173-177
Author(s):  
R. A. Dunlap ◽  
R. C. O’Handley ◽  
M. E. McHenry ◽  
V. Srinivas

1956 ◽  
Vol 2 (4) ◽  
pp. 163-170 ◽  
Author(s):  
Keith R. Porter

Electron microscopy of thin sections of muscle fibers in myotomes of Amblystoma larvae has revealed the presence of a complex, membrane-limited system of canaliculi and vesicles which form a lace-like reticulum around and among the myofibrils. This seems to correspond to the sarcoplasmic reticulum of the earlier light microscopists and the endoplasmic reticulum of other cell types. The elements constituting the reticulum are disposed in a pattern which bears a constant relation to the bands of the adjacent myofibrils and is therefore repeated in each sarcomere. At the H band the system is transversely continuous but not so at other levels. Longitudinally continuity is interrupted at the Z bands where large vesicles belonging to adjacent sarcomere segments of the system face off on opposite sides of the band. The opposing faces of these vesicles are flat and separated by a space of more or less constant width, in which are located small, finger-shaped vesicles. In view of these and other close structural relationships with the myofibrils it seems appropriate to assign to the system a role in the conduction of the excitatory impulse.


2017 ◽  
Vol 19 (23) ◽  
pp. 15021-15029 ◽  
Author(s):  
Yusheng Wang ◽  
Nahong Song ◽  
Min Jia ◽  
Dapeng Yang ◽  
Chikowore Panashe ◽  
...  

First principles calculations based on density functional theory were carried out to study the electronic and magnetic properties of C2N nanoribbons (C2NNRs).


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