scholarly journals Mechanical Characterization of Graphene Nanoplatelets-Reinforced Mg-3Sn Alloy Synthesized by Powder Metallurgy

2020 ◽  
Author(s):  
Pravir Kumar ◽  
Katerina Skotnicova ◽  
Ashis Mallick ◽  
Manoj Gupta ◽  
Tomas Cegan ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Compressive Strength ◽  
Powder Metallurgy ◽  
Compressive Strain ◽  
Hot Extrusion ◽  
Diffraction Field ◽  
X Ray Diffraction ◽  
Microstructural Characteristics

The present study investigated the effects of alloying and nano-reinforcement on the mechanical properties (microhardness, tensile strength, and compressive strength) of Mg-based alloys and composites. Pure Mg, Mg-3Sn alloy, and Mg-3Sn+0.2GNP alloy-nanocomposite were synthesized by powder metallurgy followed by hot extrusion. The microstructural characteristics of the bulk extruded samples were explored using X-ray diffraction, field-emission scanning electron microscopy, and optical microscopy and their mechanical properties were compared. The microhardness, tensile strength, and compressive strength of the Mg-3Sn alloy improved when compared to those of monolithic Mg sample and further improvements were displayed by Mg-3Sn+0.2GNP alloy-nanocomposite. No significant change in the compressive strain to failure was observed in both the alloy and the alloy-nanocomposite with respect to that of the pure Mg sample. However, an enhanced tensile strain to failure was displayed by both the alloy and the alloy-nanocomposite.

scholarly journals Mechanical Characterization of Graphene Nanoplatelets-Reinforced Mg-3Sn Alloy Synthesized by Powder Metallurgy

Metals ◽  
2020 ◽  
Vol 11 (1) ◽  
pp. 62
Author(s):  
Pravir Kumar ◽  
Katerina Skotnicova ◽  
Ashis Mallick ◽  
Manoj Gupta ◽  
Tomas Cegan ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Compressive Strength ◽  
Powder Metallurgy ◽  
Compressive Strain ◽  
Hot Extrusion ◽  
Diffraction Field ◽  
X Ray Diffraction ◽  
Microstructural Characteristics

The present study investigated the effects of alloying and nano-reinforcement on the mechanical properties (microhardness, tensile strength, and compressive strength) of Mg-based alloys and composites. Pure Mg, Mg-3Sn alloy, and Mg-3Sn + 0.2 GNP alloy-nanocomposite were synthesized by powder metallurgy followed by hot extrusion. The microstructural characteristics of the bulk extruded samples were explored using X-ray diffraction, field-emission scanning electron microscopy, and optical microscopy and their mechanical properties were compared. The microhardness, tensile strength, and compressive strength of the Mg-3Sn alloy improved when compared to those of monolithic Mg sample and further improvements were displayed by Mg-3Sn + 0.2 GNP alloy-nanocomposite. No significant change in the compressive strain to failure was observed in both the alloy and the alloy-nanocomposite with respect to that of the pure Mg sample. However, an enhanced tensile strain to failure was displayed by both the alloy and the alloy-nanocomposite.

scholarly journals Fabrication and Characterization of Electrospun Polycaprolactone Blended with Chitosan-Gelatin Complex Nanofibrous Mats

2014 ◽  
Vol 2014 ◽  
pp. 1-7 ◽  
Author(s):  
Yongfang Qian ◽  
Zhen Zhang ◽  
Laijiu Zheng ◽  
Ruoyuan Song ◽  
Yuping Zhao
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Weight Ratio ◽  
Degree Of Crystallinity ◽  
X Ray Diffraction ◽  
Tissue Engineering Scaffolds ◽  
Elongation At Break ◽  
Nanofibrous Scaffolds ◽  
Two Peaks

Design and fabrication of nanofibrous scaffolds should mimic the native extracellular matrix. This study is aimed at investigating electrospinning of polycaprolactone (PCL) blended with chitosan-gelatin complex. The morphologies were observed from scanning electron microscope. As-spun blended mats had thinner fibers than pure PCL. X-ray diffraction was used to analyze the degree of crystallinity. The intensity at two peaks at 2θof 21° and 23.5° gradually decreased with the percentage of chitosan-gelatin complex increasing. Moreover, incorporation of the complex could obviously improve the hydrophilicity of as-spun blended mats. Mechanical properties of as-spun nanofibrous mats were also tested. The elongation at break of fibrous mats increased with the PCL content increasing and the ultimate tensile strength varied with different weight ratios. The as-spun mats had higher tensile strength when the weight ratio of PCL to CS-Gel was 75/25 compared to pure PCL. Both as-spun PCL scaffolds and PCL/CS-Gel scaffolds supported the proliferation of porcine iliac endothelial cells, and PCL/CS-Gel had better cell viability than pure PCL. Therefore, electrospun PCL/Chitosan-gelatin nanofibrous mats with weight ratio of 75/25 have better hydrophilicity mechanical properties, and cell proliferation and thus would be a promising candidate for tissue engineering scaffolds.

Improved Tensile Strength of Carbon Nanotube Reinforced Aluminum Composites Processed by Powder Metallurgy

2012 ◽  
Vol 500 ◽  
pp. 651-656 ◽  
Author(s):  
Jin Zhi Liao ◽  
Ming Jen Tan
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Carbon Nanotube ◽  
Powder Metallurgy ◽  
Hot Rolling ◽  
Hot Extrusion ◽  
Significant Enhancement ◽  
Aluminum Composites ◽  
Thermal Mismatch ◽  
Pure Matrix

Carbon nanotube (CNT) reinforced aluminum (Al) composites were synthesized using the powder metallurgy (P/M) technique, combined with hot extrusion and hot rolling. 0-2.0wt.% of CNTs were added as reinforcements. The effect of CNTs on the mechanical properties of Al was investigated and a significant enhancement in tensile strength was obtained compared with the pure matrix. The improved strength was analyzed based on (i) Orowan strengthening, (ii) thermal mismatch between CNTs and matrix, and (iii) load partition effect due to the CNTs.

Development and Characterization of Ductile Mg∕Y2O3 Nanocomposites

2007 ◽  
Vol 129 (3) ◽  
pp. 462-467 ◽  
Author(s):  
S. F. Hassan ◽  
M. Gupta
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Hot Extrusion ◽  
Microstructural Characterization ◽  
Powder Metallurgy Technique ◽  
Magnesium Matrix ◽  
Mechanical Properties Characterization ◽  
Reinforcement Distribution ◽  
Work Of Fracture

Nano-Y2O3 particulates containing ductile magnesium nanocomposites were synthesized using blend-press-sinter powder metallurgy technique followed by hot extrusion. Microstructural characterization of the nanocomposite samples showed fairly uniform reinforcement distribution, good reinforcement-matrix interfacial integrity, significant grain refinement of magnesium matrix with increasing presence of reinforcement, and the presence of minimal porosity. Mechanical properties characterization revealed that the presence of nano-Y2O3 reinforcement leads to marginal increases in hardness, 0.2% yield strength and ultimate tensile strength, but a significant increase in ductility and work of fracture of magnesium. The fracture mode was changed from brittle for pure Mg to mix ductile and intergranular in the case of nanocomposites.

scholarly journals Mechanical Characterization of Aluminium-Silicon-Titanium Diboride (Al-Si-TiB2) Reinforced by Scandium (Sc) and Strontium (Sr)

2019 ◽  
Vol 7 (4.14) ◽  
pp. 392
Author(s):  
N. N.A. Basir ◽  
N. H. Mustafa ◽  
R. E. Ibrahim ◽  
R. Rosmamuhamadani ◽  
M. M. Mahat ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Titanium Diboride ◽  
High Strength ◽  
Matrix Composites ◽  
Composite Alloy ◽  
X Ray Diffraction ◽  
Hardness Tester ◽  
And Performance

Aluminium based metal matrix composites (MMCs) have better properties and performance. They are commonly used in transport applications which require combinations of high strength and ductility. They are quite attractive due to their low density, capability to be strengthened by precipitation, good corrosion resistance, high thermal and electrical conductivity. Grain refinement plays a crucial role in improving characteristics and properties of aluminium-silicon (Al-Si) alloy. In this investigation, scandium (Sc) and strontium (Sr) elements were added to aluminium-silicon-titanium diboride (Al-Si-TiB2) alloy for refinement of grains. The compositions of 93 wt.% Al-Si, 6 wt.% TiB2, 0.5 wt.% Sc and 0.5 wt.% Sr were melted into induction furnace. Then the composites have been characterized on the mechanical properties and microstructure characterization. Instron tensile machine and vickers hardness tester were used to characterize the mechanical properties of the composite alloy. Microstructure and phase composition were characterized by Field Emission Scanning Electron Microscope (FESEM) and X-ray Diffraction (XRD). From the results obtained, addition of Sc and Sr, into Al-S-TiB2 improved the tensile strength and hardness of composite alloy. Results also showed that the inoculants addition able to enhance the refinement of grains and escalate the values of hardness and tensile strength of Al-Si-TiB2 composite. Mechanical properties related much on the microstructure as it can be seen that the addition of grain refiners produced much higher value of mechanical properties.  

Development and Characterization of AZ31B Mg Alloy Using Powder Metallurgy Technique Followed by Hot Extrusion

2014 ◽  
Vol 984-985 ◽  
pp. 124-128 ◽  
Author(s):  
R. Anish ◽  
M.S. Pragash ◽  
G. Robert Singh
Keyword(s):  
Powder Metallurgy ◽  
Hot Extrusion ◽  
Sem Analysis ◽  
Mg Alloy ◽  
Powder Metallurgy Technique ◽  
Micro Hardness ◽  
X Ray Diffraction ◽  
X Ray ◽  
Powder Metallurgy Route

In this study AZ31B Mg alloy is developed by powder metallurgy route followed by hot extrusion. The extruded materials were characterized for microstructure, X-ray diffraction (XRD), density, porosity and mechanical properties such as tensile, compression, impact and micro hardness. The SEM analysis of fractured surface of AZ31B Mg alloy showed quasi-cleavage fracture mode.

Studying Methylcellulose-Base Edible Films Properties by XRD, EDXRF and FTIR

2014 ◽  
Vol 979 ◽  
pp. 319-322 ◽  
Author(s):  
W. Siriprom ◽  
P. Kuha ◽  
S. Kongsriprapan ◽  
K. Teanchai
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Hydrogen Bonding ◽  
Fourier Transform ◽  
Amorphous Structure ◽  
Edible Films ◽  
X Ray Diffraction ◽  
Xrd Pattern ◽  
X Ray

The physicochemical of methylcellulose (MC) base edible films were investigated in this work. The characterization of MC used X-Ray Diffraction (XRD), Energy Dispersive X-Ray Fluorescence (EDXRF) and Fourier Transform Infrared Spectroscopy (FTIR) spectroscopy for investigated the crystalline, the composition element, and the intermolecular interaction, respectively. It was found that, the XRD pattern indicated MC has amorphous structure. The chemical composition by XRF reported that Silver (Ag) have been detect and the hydrogen bonding formation between MC investigated with FTIR spectra, which interpreted in terms of the symmetry distortion of hydroxyl stretch. Another that, the mechanical properties tensile strength (TS) elastic modulus (EM) and elongation (E) values were investigated.

Study of Ageing Treatment on Spray Forming Al-Zn-Mg-Cu Alloy

2012 ◽  
Vol 217-219 ◽  
pp. 1835-1838 ◽  
Author(s):  
Rui Ming Su ◽  
Ying Dong Qu ◽  
Run Xia Li ◽  
Rong De Li
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Tensile Strength ◽  
Hot Extrusion ◽  
Spray Forming ◽  
X Ray Diffraction ◽  
X Ray ◽  
Cu Alloy ◽  
Scanning Electron ◽  
Peak Value

The Al-Zn-Mg-Cu (7A04) alloys were prepared by using the method of spraying forming and the hot extrusion. The changes of microstructure and mechanical properties of the spray deposited Al-Zn-Mg-Cu alloy underwent ageing, regression and reageing treatment (RRA) was studied by scanning electron microscopy, X-ray diffraction and other methods. The results show that the tensile strength of the alloy aged at 120°C for 24 hours can reach the peak value (760MPa), but the elongation is only 4.8 percent. The toughness of the alloy regression treated at 160°C for 2 hours can increase to 9.0 percent, but its tensile strength decreases greatly (680MPa). The reaging treatment at 120°C can make the tensile strength up to 740MPa, while the elongation which is 8.2 percent still keeps a higher level.

Effect of Zn on Microstructure and Mechanical Properties of Al-Zn-Mg-Cu-Zr Alloy by Powder Metallurgy

2013 ◽  
Vol 710 ◽  
pp. 102-105
Author(s):  
Chuan Dong Wu ◽  
Cheng Zhang Li ◽  
Pan Fang ◽  
Guo Qiang Luo ◽  
Qiang Shen
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Powder Metallurgy ◽  
Full Density ◽  
Hot Press ◽  
X Ray Diffraction ◽  
Electron Probe Micro Analyzer ◽  
Microstructure And Mechanical Properties ◽  
Hot Press Sintering ◽  
Zr Alloy

In this paper, full-density Al-Zn-Mg-Cu-Zr powder metallurgy (P/M) alloy is prepared by hot-press sintering in vacuum at 600°C. Experiments are conducted to evaluate the effects of Zn additive in the range of 7.2-8.4 wt.% on the microstructure and mechanical properties of Al-Zn-Mg-Cu-Zr alloys. X-ray diffraction (XRD), scanning electron microstructure (SEM) and electron probe micro-analyzer (EPMA), and mechanical properties such as tensile strength are measured. The porosity decreases gradually with increasing of Zn and it achieves 0.01% with a density of 2.95 g/cm3 at 8.4% Zn. The tensile strength reaches the maximal value of 436 MPa at 8.4% Zn.

Un-Bundled Carbon Nanotubes Reinforced Light Metal Composites via Powder Metallurgy Route

2011 ◽  
Vol 690 ◽  
pp. 339-342
Author(s):  
Katsuyoshi Kondoh ◽  
Thotsaphon Threrujirapapong ◽  
Hiroyuki Fukuda ◽  
Junko Umeda
Keyword(s):  
Mechanical Properties ◽  
Carbon Nanotubes ◽  
Tensile Strength ◽  
Powder Metallurgy ◽  
Pure Titanium ◽  
Hot Extrusion ◽  
Light Metal ◽  
Dispersion Strengthening ◽  
Multi Wall Carbon Nanotubes

By using light metal (Mg, Al, Ti) powders coated with un-bundled multi-wall carbon nanotubes (MWCNTs) via wet process, powder metallurgy (P/M) light metal matrix composite reinforced with un-bundled nanotubes was prepared by spark plasma sintering (SPS) and subsequently hot extrusion process. The microstructure and mechanical properties of the composites were evaluated. In the case of pure titanium, the distribution of CNTs and in-situ formed titanium carbide (TiC) compounds during sintering was investigated by optical and scanning electron microscopy (SEM) equipped with EDS analyzer. The mechanical properties of TMC were significantly improved by the additive of CNTs. For example, when employing the pure titanium composite powder coated with CNTs of 0.35 mass%, the increase of tensile strength and yield stress of the extruded TMC was 157 MPa and 169 MPa, respectively, compared to those of extruded titanium materials with no CNT additive. Fractured surfaces of tensile specimens were analyzed by SEM, and the uniform distribution of CNTs and TiC particles, being effective for the dispersion strengthening, at the surface of the TMC were obviously observed. In the case of Mg-Al alloys, in-situ formation of Al2MgC2compounds at the interface between CNTs and Mg-matrix occurred and effective for the tensile transfer loading, and resulted in the increment of tensile strength of the composite material.

Sign in / Sign up

Export Citation Format

Share Document