scholarly journals Realization of Phase and Microstructure Control in Fe/Fe2SiO4-FeAl2O4 Metal-Ceramic by Alternative Microwave Susceptors

Author(s):  
Chen-bo Gao ◽  
Peng-fei Xu ◽  
Fei Ruan ◽  
Chen-yu Yang

This study provides a novel method to prepare metal-ceramic composites from magnetically selected iron ore using microwave heating. By introducing three different microwave susceptors (Activated Carbon, SiC, and a mixture of Activated Carbon and SiC) during the microwave process, effective control of the ratio of metallic and ceramic phases has been achieved easily. The effects of the three susceptors on the microstructure of the metal-ceramics and the related reaction mechanisms were also investigated in detail. The results show that the metal phase (Fe) and ceramic phase (Fe2SiO4, FeAl2O4) can be maintained, but the metal phase to ceramic phase changed significantly. In particular, the microstructures appeared as well-distributed nanosheet structures with diameters of ~400 nm and thicknesses of ~20 nm when SiC was used as the microwave susceptor.

Author(s):  
Brian Lester ◽  
Yves Chemisky ◽  
Dimitris Lagoudas

Metal-ceramic composites are being increasingly explored in an effort to find new materials for use in extreme environments. Via functional grading of of the volume fraction of the constituant phases and other techniques, the material can be optimized to incorporate the mechanical properties of the metal phase with the thermal properties of the ceramic phase. To get further benefit of the metal phase, a new area being investigated is the incorporation of Shape Memory Alloys (SMAs). In order to predict the phase transformation features of an SMA embedded in a stiff ceramic matrix, a micromechanical approach is developed to find the effective phase diagram of the ceramic-SMA composite. From this analysis, other composite characteristics such as stress in each phase and the evolution of tranformation strain in the SMA can be determined in order to improve the design of such new composite materials.


Nanomaterials ◽  
2021 ◽  
Vol 11 (10) ◽  
pp. 2499 ◽  
Author(s):  
Elena G. Zemtsova ◽  
Denis V. Yurchuk ◽  
Pavel E. Morozov ◽  
Petr M. Korusenko ◽  
Vladimir K. Kudymov ◽  
...  

The development of new composites with improved functional properties is the important task of modern materials science. The composites must be structurally organized to provide improved properties. For metal-ceramic composites, there is a need for a uniform distribution of the dispersed ceramic phase in the bulk metallic matrix The modification of the dispersed ceramic phase surface with a metal coating is one of the more effective ways to accomplish this. Particularly, in this work, the conditions of Ni nanolayer deposition on titanium carbide (TiC) particles were studied. The goal was to create core–shell particles with a thickness of the Ni coating on TiC not exceeding 90 nm. Preliminary work was also carried out to study the effect of the dispersed phase composition on the mechanical properties of the composite with an Al matrix.


Author(s):  
Jian-Shing Luo ◽  
Chia-Chi Huang ◽  
Jeremy D. Russell

Abstract Electron tomography includes four main steps: tomography data acquisition, image processing, 3D reconstruction, and visualization. After acquisition, tilt-series alignments are performed. Two methods are used to align the tilt-series: cross-correlation and feature tracking. Normally, about 10-20 nm of fiducial markers, such as gold beads, are deposited onto one side of 100 mesh carbon-coated grids during the feature-tracking process. This paper presents a novel method for preparing electron tomography samples with gold beads inside to improve the feature tracking process and quality of 3D reconstruction. Results show that the novel electron tomography sample preparation method improves image alignment, which is essential for successful tomography in many contemporary semiconductor device structures.


2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Erik Poloni ◽  
Florian Bouville ◽  
Christopher H. Dreimol ◽  
Tobias P. Niebel ◽  
Thomas Weber ◽  
...  

AbstractThe brick-and-mortar architecture of biological nacre has inspired the development of synthetic composites with enhanced fracture toughness and multiple functionalities. While the use of metals as the “mortar” phase is an attractive option to maximize fracture toughness of bulk composites, non-mechanical functionalities potentially enabled by the presence of a metal in the structure remain relatively limited and unexplored. Using iron as the mortar phase, we develop and investigate nacre-like composites with high fracture toughness and stiffness combined with unique magnetic, electrical and thermal functionalities. Such metal-ceramic composites are prepared through the sol–gel deposition of iron-based coatings on alumina platelets and the magnetically-driven assembly of the pre-coated platelets into nacre-like architectures, followed by pressure-assisted densification at 1450 °C. With the help of state-of-the-art characterization techniques, we show that this processing route leads to lightweight inorganic structures that display outstanding fracture resistance, show noticeable magnetization and are amenable to fast induction heating. Materials with this set of properties might find use in transport, aerospace and robotic applications that require weight minimization combined with magnetic, electrical or thermal functionalities.


2012 ◽  
Vol 95 (10) ◽  
pp. 3078-3083 ◽  
Author(s):  
Siddhartha Roy ◽  
Karl Günter Schell ◽  
Ethel Claudia Bucharsky ◽  
Pascal Hettich ◽  
Stefan Dietrich ◽  
...  

2013 ◽  
Vol 22 (08) ◽  
pp. 1350067 ◽  
Author(s):  
SEYYED AMIR ASGHARI ◽  
ATENA ABDI ◽  
OKYAY KAYNAK ◽  
HASSAN TAHERI ◽  
HOSSEIN PEDRAM

Electronic equipment used in harsh environments such as space has to cope with many threats. One major threat is the intensive radiation which gives rise to Single Event Upsets (SEU) that lead to control flow errors and data errors. In the design of embedded systems to be used in space, the use of radiation tolerant equipment may therefore be a necessity. However, even if the higher cost of such a choice is not a problem, the efficiency of such equipment is lower than the COTS equipment. Therefore, the use of COTS with appropriate measures to handle the threats may be the optimal solution, in which a simultaneous optimization is carried out for power, performance, reliability and cost. In this paper, a novel method is presented for control flow error detection in multitask environments with less memory and performance overheads as compared to other methods seen in the literature.


1998 ◽  
Vol 13 (4) ◽  
pp. 803-811 ◽  
Author(s):  
Philippe Colomban

The problems encountered to tailor simultaneously various specific chemical or physical properties are discussed. Selected polymeric precursors used in association with fine powders allow the control of the nano/microstructure of composites and hence the preparation of functional (FGM) and hierarchical reinforced (HRC) composites, making it possible to combine several kinds of fibers, interphases, and matrices in the same composite (hot microwave absorbent), to control the fiber/matrix interface (long life times composites), to achieve net-shape sintering of 3D composite matrices, and to prepare thick films of metal-ceramic composites with tailored microwave absorption (radar stealthiness).


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