scholarly journals Bond strength of resin cements to leucite-reinforced ceramics: part 2 – after one-year aging in water

RSBO ◽  
2017 ◽  
Vol 13 (3) ◽  
pp. 156
Author(s):  
Rubens Nazareno Garcia ◽  
Reinaldo Francisco do Nascimento ◽  
Ana Cristina Rocha Gomes ◽  
João Augusto Coutinho Garcia ◽  
Luiz Carlos Machado Miguel ◽  
...  

The aim of this study was to compare the shear bond strength (SBS) of two resin cements bonded to four leucite-reinforced ceramics after one week and one year of aging. Material and methods: Forty ceramic blocks (4 mm wide, 14 mm length, and 2 mm thick) were used (1 week) and reused at the back side (1 year). The blocks were abraded with aluminum oxide (90 µm) and randomly divided into eight groups for each time. Two dual resin cements (RelyX ARC and RelyX U200 self-adhesive, 3M ESPE) were bonded to ceramics Creapress (CRE – Creation / Klema), Finesse All-Ceramic (FIN – Dentsply / Ceramco), IPS Empress Esthetic (IEE – Ivoclar Vivadent) and Vita PM9 (PM9-Vita). For each resin, time, and ceramic block, after applications of the 10% hydrofluoric acid (for 1 min) and silane, 3 Tygon cut tubes were positioned over each block and filled in with the resin cements (light-cured for 40 s). The tubing molds were removed to expose the bond specimens as cylinders (area=0.38 mm2) stored in relative humidity at 24±2°C for one week and at 37±2°C for one year. All bonds were tested in an Instron in shear (applied of the base cylinder with a thin wire - 0.25 mm) at speed of 0.5 mm/min, until failure. Results: The results were analyzed by ANOVA (resin cements, ceramic systems, and time) and Tukey test (p<0.05) for rank ordering of SBS. The FIN and IEE ceramics did not show significant SBS decreasing on aging with U200. The mean SBS decreasing for all the ceramics was 36% with ARC and 14% with U200 cement. Conclusion: The SBS of ARC cement were significantly lower for all ceramics with aging than that of U200 cement. The SBS of ARC cement was also weakened by aging. FIN ceramic + U200 cement proved to be the most stable and strongest bond strength, and PM9+ARC cement proved to be the weakest bond strength with low stability.

Author(s):  
Hoseinali Mahgoli ◽  
Mahnaz Arshad ◽  
Kamran Rasouli ◽  
Ali Akbar Sobati ◽  
Ahmad Reza Shamshiri

  Objectives: This study aimed to assess the effect of application of two types of zirconia primers on repair bond strength of composite to zirconia ceramic. Materials and Methods: In this in vitro, experimental study, 60 zirconia blocks were divided into five groups and subjected to the application of Z-Prime Plus (ZPP), Monobond Plus (MBP), Porcelain Bonding Resin (PBR), ZPP followed by PBR (ZPP+PBR) and MBP followed by PBR (MBP+PBR). They were then bonded to Z100 composite. The samples were then immersed in water at 37°C for 24 hours, thermocycled for 1000 cycles between 5-55°C and subjected to shear bond strength (SBS) test. The mode of failure was determined under a stereomicroscope and a scanning electron microscope (SEM). Results: The mean bond strength was the highest in ZPP+PBR group followed by MBP+PBR, ZPP, PBR and MBP group (22.29±8.86, 15.75±2.81, 12.02±3.24, 3.60±2.92 and 2.92±1.78 MPa, respectively). The effects of type of zirconia primer and use/no use of PBR on SBS were significant (P<0.05). The frequency of adhesive failure in MBP and PBR groups was significantly higher than that in MBP+PBR and ZPP+PBR groups (P<0.05). The cohesive failure was significantly more frequent in ZPP+PBR group than in ZPP, MBP and PBR groups (P<0.05). Conclusion: Simultaneous application of zirconia primer and PBR is the most efficient technique for repair of all-ceramic zirconia restorations with composite resin.


2019 ◽  
Vol 22 (2) ◽  
pp. 275-280
Author(s):  
Beatriz Curvello de Mendonça ◽  
William Matthew Negreiros ◽  
Marcelo Giannini

Objective: to evaluate the effect of aluminum oxide sandblasting (AOS), argon plasma application (APL) and their combination (AOS+APL) on the shear bond strength (SBS) of dual-cure resin cement (Panavia F 2.0, Kuraray Noritake) to two zirconiabased ceramics (Lava, 3M ESPE and Katana, Kuraray Noritake). Material and Methods: One hundred twenty zirconia plates (13 mm in length X 5 mm in width X 1 mm in thickness) were prepared and treated according to the following treatments: 1- AOS, 2- APL,3- AOS+APL and 4- no treatment (control). After treatments, resin cement cylinders (1.4 mm in diameter x 1 mm in height) bonded to zirconia surface were obtained by filling up the silicon matrix. The shear bond test was performed following storage of the samples for 24 hours and one year. Bond strength values were recorded in MPa and the data were analyzed by three-way ANOVA and Tukey post-hoc test (preset alpha of 0.05). Results: In general, AOS and AOS+APL showed the higher SBS. After one-year storage, SBS of the resin cement to the Katana zirconia did not reduce, regardless of the zirconia surface treatment. Conclusion: AOS alone was able to increase the SBS of the resin cement to both zirconia ceramics compared to control and SBS remained stable after one year depending on type of zirconia ceramic.KeywordsAluminum Oxide; Ceramics; Plasma; Resin Cements


Author(s):  
Ronaldo Luís Almeida de CARVALHO ◽  
Jean Soares MIRANDA ◽  
Rodrigo Furtado de CARVALHO ◽  
Michelly Rocha DUARTE ◽  
Estevão Tomomitsu KIMPARA ◽  
...  

ABSTRACT Objective Evaluate the influence of silane heat treatment in bond durability between two resin cements and CAD/CAM feldspathic ceramic. Methods 40 feldspathic ceramic blocks were obtained, and were duplicated in microhybrid composite. All ceramic blocks were etched with 10% hydrofluoric acid for 20 s and received application of silane agent. The blocks were randomizedinto eight groups (n=5) according to the surface treatments and luting agents: P- Panavia F; PAg- Panavia F + Aging; HP- Heat Treatment + Panavia F; HPAg- Heat Treatment + Panavia F + Aging; R- RelyX ARC; Rag- RelyX ARC + Aging; HR- Heat Treatment + RelyX ARC; HRAg- Heat Treatment + RelyX ARC + Aging. The heat treatment was performed in furnace at 100 °C for 2 min. All blocks were cemented and cut to obtain samples with adhesive area of 1 mm2. Aging was performed with 10000 thermal cycles. The samples were subjected to microtensile bond strength test. Results The three-way ANOVA test revealed a significant interaction between cement versus heat treatment (p=0.001) and heat treatment versus thermal cycling (p=0.001) indicating that there was a change in bond strength due to surface treatment and aging. Conclusion Therefore, the heat treatment of the silane at 100 ºC for 2 minutes obtained higher values of bond strength between the resin cement and a feldspathic ceramicafter aging.


2012 ◽  
Vol 83 (1) ◽  
pp. 152-157 ◽  
Author(s):  
Erika L. Silva-Benítez ◽  
Veronica Zavala-Alonso ◽  
Gabriel A. Martinez-Castanon ◽  
Juan P. Loyola-Rodriguez ◽  
Nuria Patiño-Marin ◽  
...  

Abstract Objective: To study the shear bond strength (SBS), sites of failure, and micromorphology of bonded molar tubes used on teeth affected by dental fluorosis. Materials and Methods: This in vitro study included 140 first molars classified according to Dean's index for dental fluorosis. Samples were divided into seven groups: (1) healthy teeth etched for 15 seconds, (2) teeth with moderate fluorosis (MOF) etched for 15 seconds, (3) teeth with MOF etched for 150 seconds, (4) teeth with MOF microabrasion etched for 15 seconds, (5) teeth with severe fluorosis (SEF) etched for 15 seconds, (6) teeth with SEF etched for 150 seconds, and (7) teeth with SEF microabrasion etched for 15 seconds. All samples were incubated and were then submitted to the SBS test and evaluated with the modified adhesive remnant index (ARI) and analyzed by using a scanning electronic microscope. Results: The SBS mean value for healthy enamel was 20 ± 10.2 MPa. For the group with MOF, the etched 150-second mean value was the highest (19 ± 7.6 MPa); for the group with SEF treated with microabrasion and etched for 15 seconds, the mean value was (13 ± 4.1 MPa). Significant differences (P ≤ .05) were found in the ARI between healthy and fluorosed groups. Conclusions: Fluorotic enamel affects the adhesion of bonded molar tubes. The use of overetching in cases of MOF and the combination of microabrasion and etching in SEF provides a suitable adhesion for fixed appliance therapy.


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