Optimization of Vanillin Extraction from Biodegradation of Oil Palm Empty Fruit Bunches by Serpula lacrymans

Abstract This research aims to determine the combination of the ethyl acetate solvent volume and the extraction time that resulted in the optimum response of vanillin content and vanillin yield from the degradation of lignocellulose components from oil palm empty fruit bunches (OPEFB). First, OPEFB degraded using Serpula lacrymans to break down lignocellulosic components. The research design used a centralized composite design with two factors, the volume of ethyl acetate solvent (ml) and the extraction time (minutes). The responses of the experiment are vanillin content and vanillin yields. The optimization analysis results showed that the volume of ethyl acetate solvent and extraction time have a quadratic effect on the vanillin content and vanillin yields. The optimal solution was obtained by treatment with ethyl acetate volume 101.1 ml and extraction time 123.5 minutes. The optimal solution prediction results obtained vanillin content 0.014% and vanillin yield 7.302 μg/g with desirability of 92.8%. Validation based on the optimal solution’s prediction brought response vanillin content 0.013% and vanillin yield 6.950 μg/g. The vanillin content and yield validation results differed respectively by 4.081% and 4.826% lower when compared to predictions on the optimal solution. Keywords: ethyl acetate, vanillin content, vanillin yield

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EFFECTIVENESS OF SOME NITROGEN DOSE AND CELLULOLYTIC MICROORGANISM (MOS) TOWARD DECOMPOSITION RATE OF TAN AND EMPTY AEROBIC PALM

AgroTech Journal ◽

10.31327/atj.v1i1.203 ◽

2016 ◽

Vol 1 (1) ◽

pp. 33-36

Author(s):

Sakiah Sakiah ◽

Mariani Sembiring

Keyword(s):

Oil Palm ◽

Decomposition Rate ◽

Block Design ◽

Dry Weight ◽

Nitrogen Levels ◽

Empty Fruit Bunches ◽

Cellulolytic Microorganisms ◽

Randomized Block Design ◽

Two Factors ◽

Four Levels

This study aims to determine the effect of nitrogen levels, cellulolytic microorganisms and the interaction of both the aerobic decomposition rate of oil palm empty fruit bunches. The research was conducted at Home Compost STIP-AP Medan in April until July 2016. Research used a factorial randomized block design consisting of two factors and three replications. The first factor is the dose of nitrogen consisting of four levels i.e. N0 = without urea, N1 = dose of Nitrogen 2% of the dry weight of TKS which is 40% as much as 48 grams, N2 = dose of Nitrogen 4% of the dry weight of TKS which is 40% as much as 96 grams, N3 = Nitrogen dose of 6% of the dry weight of TKS which is 40% as much as 144 grams. The second factor is the cellulolytic microorganism isolates comprising four levels i.e. M0 = without cellulolytic microorganisms isolates, with isolates MOS M1 = 10 ml, M2 = isolate MOS 20 ml, isolate MOS M3 = 30 ml. From the research the effectiveness of multiple doses of nitrogen and cellulolytic microorganisms (MOS) on the rate of decomposition of oil palm empty fruit bunches can be deduced as follows, namely addition of nitrogen dose was able to reduce levels of C/N was 76.4% of the levels of C/N beginning. The best treatment is contained in N3 treatment. Addition of Microorganisms treatment cellulolytic (MOS) is able to reduce levels of C/N as much as 74.6% of the levels of C/N beginning. The best treatment is contained in M3 treatment. Interaction between giving treatment cellulolytic microorganisms Nitrogen and reducing levels of C/N as much as 79.4%. Interaction best treatment there in treatment N3M3.

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Sifat Fisik Dan Mekanik Papan Komposit Dari Serat Tandan Kosong Kelapa Sawit (TKKS) Hasil Penguraian Secara Mekanis Dengan Perekat Gambir

Jurnal Ilmiah Poli Rekayasa ◽

10.30630/jipr.15.2.165 ◽

2020 ◽

Vol 15 (2) ◽

pp. 38

Author(s):

Junaidi -

Keyword(s):

Water Content ◽

Oil Palm ◽

Waste Product ◽

Modulus Of Rupture ◽

Thickness Swelling ◽

Adhesive Properties ◽

Composite Board ◽

Empty Fruit Bunches ◽

Two Factors ◽

Oil Palm Industry

Oil palm empty fruit bunches (OPEFB) are a solid waste product from the oil palm industry that are about 70% fiber. Previous research has indicated that this fiber can be used to produce composite board. Gambier can be used in an adhesive to produce these boards as it has strong adhesive properties. This research investigates the suitability of four types of OPEFB fiber resulting from different mechanical separation speeds and three adhesive made from differing concentrations of Gambier (12%, 14%, 16%) to produce high quality composite board. The results of the research suggest the type of the fiber and the concentration of the gambier used significantly influence the density of the resulting board and that there are interactions between these two variables. The water content of the board is significantly influenced by the type of OPEFB fibre but not by the concentration of gambier or any interaction between these variables. Thickness swelling, modulus of rupture (MOR) and modulus of elasticity (MOE) are all influenced by type of fiber and concentration of gambier without any significant interaction between these two factors. The best types of fiber was those labeled A and B. The best performing composite board was produced from the longer B fibers and 16% gambier adhesive. This board a had density of 0.86 g/cm3, MOR 251.3 kg/cm2 and strength parallel to the grain of 145.6 kg/cm2. This data suggests that the density, water content and MOR of the boards made with this combination of material meets standard SNI 03-2105-2006 however the thickness swelling of the board fails this standard.

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Pengaruh Penambahan Nanoselulosa dari Tandan Kosong Kelapa Sawit (Elaeis guinensis Jacq) terhadap Karakteristik Polivinil Alkohol (PVA)

Jurnal Ilmiah Mahasiswa Pertanian ◽

10.17969/jimfp.v5i2.14837 ◽

2020 ◽

Vol 5 (2) ◽

pp. 203-209

Author(s):

Fathia Arami B Tou ◽

Eti Indarti ◽

Ismail Sulaiman

Keyword(s):

Oil Palm ◽

Water Vapor Permeability ◽

Vapor Permeability ◽

Cellulose Content ◽

Empty Fruit Bunches ◽

Descriptive Research ◽

Two Factors ◽

Ft Ir ◽

High Cellulose

Abstrak: Tandan kosong kelapa sawit merupakan limbah padat terbesar yang dihasilkan oleh perkebunan kelapa sawit. Kandungan utama tandan kosong kelapa sawit adalah selulosa. Tingginya kandungan selulosa pada tandan kosong kelapa sawit dapat dimanfaatkan sebagai bahan dasar pembuatan nanoselulosa. Nanoselulosa merupakan selulosa yang dihasilkan dalam skala nano dan memiliki sifat karakteristik yang jauh lebih baik dibandingkan dengan selulosa. Pada penelitian ini dilakukan isolasi selulosa yang berasal dari tandan kosong kelapa sawit untuk menghasilkan nanoselulosa yang dapat dimanfaatkan sebagai pencampur (filler) pada polimer polivinil alkohol (PVA), sehingga diharapkan dapat memperbaiki karakteristik pada PVA. Tujuan dari penelitian ini yaitu untuk mengkaji isolasi selulosa menjadi nanoselulosa dari tandan kosong kelapa sawit serta mempelajari karakteristik pada PVA dengan adanya penambahan nanoselulosa. Penelitian ini dilakukan menggunakan rancangan penelitian deskriptif yang terdiri dari jumlah penambahan nanoselulosa (N) dan jumlah PVA (P). Karakterisasi yang dilakukan adalah uji ketebalan, uji kuat tarik, uji FT-IR, uji WVP, dan uji UV-Vis Spectrophotometer. Hasil dari penelitian menunjukkan bahwa penambahan nanoselulosa berpengaruh terhadap karakteristik film PVA. The Effects of Adding Nanocellulose From Oil Palm Empty Fruit Bunch (Elaeis guinensis Jacq) For Characterization of Polyvinil Alcohol (PVA) Abstract: Oil palm empty fruit bunches (OPEFB) are the largest solid waste produced by oil palm plantations. The main content of oil palm empty fruit bunches is cellulose. High cellulose content in oil palm empty fruit bunches can be used for making nanocellulose. Nanocellulose is cellulose that produced in nanoscale and it has better characteristic properties compared to cellulose. In this study, cellulose from oil palm empty fruit bunches was isolated to produce nanocellulose that can be used as filler for characterization of polyvinil alcohol (PVA). The purpose of this study is to examined the isolation of cellulose into nanocellulose from oil palm empty fruit bunches and to investiage the characteristics of PVA with the addition of nanocellulose. This study was conducted using a descriptive research design consisting of 2 (two) factors. The first factor was the total addition of nanocellulose (N) and the second factor was the amount of polyvinyl alcohol (P). The characterization that carried out were a thickness test, tensile strength, Fourier Transform Infra-Red (FT-IR), Water Vapor Permeability (WVP), and UV-Vis Spectrophotometer. The results of the study showed that the addition of nanocellulose can effect the characteristics of PVA films.

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Thermal Decomposition Kinetics of Torrefied Oil Palm Empty Fruit Bunch Briquettes

Chemistry & Chemical Technology ◽

10.23939/chcht10.03.325 ◽

2016 ◽

Vol 10 (3) ◽

pp. 325-328 ◽

Cited By ~ 1

Author(s):

Bemgba Nyakuma ◽

◽

Arshad Ahmad ◽

Anwar Johari ◽

Tuan Abdullah ◽

...

Keyword(s):

Thermal Decomposition ◽

Oil Palm ◽

Decomposition Kinetics ◽

Thermal Decomposition Kinetics ◽

Kinetic Properties ◽

Tg Analysis ◽

Empty Fruit Bunches ◽

Thermal Lag ◽

Profile Characteristics ◽

Kinetics Of

The study is aimed at investigating the thermal behavior and decomposition kinetics of torrefied oil palm empty fruit bunches (OPEFB) briquettes using a thermogravimetric (TG) analysis and the Coats-Redfern model. The results revealed that thermal decomposition kinetics of OPEFB and torrefied OPEFB briquettes is significantly influenced by the severity of torrefaction temperature. Furthermore, the temperature profile characteristics; Tonset, Tpeak, and Tend increased consistently due to the thermal lag observed during TG analysis. In addition, the torrefied OPEFB briquettes were observed to possess superior thermal and kinetic properties over the untorrefied OPEFB briquettes. It can be inferred that torrefaction improves the fuel properties of pelletized OPEFB for potential utilization in bioenergy conversion systems.

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APPLICATION OF OIL PALM EMPTY FRUIT BUNCH FIBERS IN STRENGTH IMPROVEMENT AS A FIBER REINFORCED CONCRETE

Jurnal Penelitian Kelapa Sawit ◽

10.22302/iopri.jur.jpks.v25i3.33 ◽

2017 ◽

Vol 25 (3) ◽

pp. 161-170

Author(s):

Henny Lydiasari ◽

Ari Yusman Manalu ◽

Rahmi Karolina

Keyword(s):

Tensile Strength ◽

Compressive Strength ◽

Crack Length ◽

Oil Palm ◽

Fiber Reinforced Concrete ◽

Structural Concrete ◽

Empty Fruit Bunches ◽

Construction Products ◽

By Products ◽

Strength Improvement

The potency of oil palm empty fruit bunches (OPEFB) fibers as one of the by-products of processing oil palm is increasing significantly so that proper management is needed in reducing environmental impact. One of the utilization of OPEFB fibers is as a substitution material in construction which usually the material is derived from non-renewable mining materials so that the number is increasingly limited. Therefore, it is necessary to study to know the performance of OPEFB fiber in making construction products especially concrete. In this case, the experiment was conducted using experimental method with variation of fiber addition by 0%, 10%, 15%, 20%, 25%, and 30%. Each specimen was tested by weight, slump value, compressive strength, tensile strength, elasticity and crack length. As the results, the variation of fibers addition by 10%, decrease of slump value is 7%, concrete weight is 3% and crack length is 8% while increase of the compressive strength is 2.7% and the modulus of elasticity is 33.3% but its tensile strength decreased insignificantly by 0.05% . Furthermore, the addition of fibers above 10% to 30% decreased compressive strength is still below 10% and tensile strength below 2% while the weight of concrete, slump value and crack length decreased. Therefore, the addition of 10% can replace the performance of concrete without fiber but the addition of above 10% can still be used on non-structural concrete.

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Flammability, Tensile, and Morphological Properties of Oil Palm Empty Fruit Bunches Fiber/Pet Yarn-Reinforced Epoxy Fire Retardant Hybrid Polymer Composites

Polymers ◽

10.3390/polym13081282 ◽

2021 ◽

Vol 13 (8) ◽

pp. 1282

Author(s):

M.J. Suriani ◽

Fathin Sakinah Mohd Radzi ◽

R.A. Ilyas ◽

Michal Petrů ◽

S.M. Sapuan ◽

...

Keyword(s):

Tensile Properties ◽

Oil Palm ◽

Natural Fiber ◽

Fire Retardant ◽

Epoxy Composites ◽

Morphological Properties ◽

Hybrid Polymer ◽

Fiber Volume ◽

Fiber Loading ◽

Empty Fruit Bunches

Oil palm empty fruit bunches (OPEFB) fiber is a natural fiber that possesses many advantages, such as biodegradability, eco-friendly, and renewable nature. The effect of the OPEFB fiber loading reinforced fire retardant epoxy composites on flammability and tensile properties of the polymer biocomposites were investigated. The tests were carried out with four parameters, which were specimen A (constant), specimen B (20% of fiber), specimen C (35% of fiber), and specimen D (50% of fiber). The PET yarn and magnesium hydroxide were used as the reinforcement material and fire retardant agent, respectively. The results were obtained from several tests, which were the horizontal burning test, tensile test, and scanning electron microscopy (SEM). The result for the burning test showed that specimen B exhibited better flammability properties, which had the lowest average burning rate (11.47 mm/min). From the tensile strength, specimen A revealed the highest value of 10.79 N/mm2. For the SEM morphological test, increasing defects on the surface ruptured were observed that resulted in decreased tensile properties of the composites. It can be summarized that the flammability and tensile properties of OPEFB fiber reinforced fire retardant epoxy composites were reduced when the fiber volume contents were increased at the optimal loading of 20%, with the values of 11.47 mm/min and 4.29 KPa, respectively.

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