scholarly journals Особенности деформирования круглых тонкопленочных мембран и экспериментальное определение их эффективных характеристик

2021 ◽  
Vol 91 (10) ◽  
pp. 1454
Author(s):  
А.А. Дедкова ◽  
П.Ю. Глаголев ◽  
Е.Э. Гусев ◽  
Н.А. Дюжев ◽  
В.Ю. Киреев ◽  
...  
Keyword(s):  
Mechanical Characteristics ◽  
Complex Shape ◽  
Membrane Surface ◽  
Initial Deflection ◽  
Silicon Substrates ◽  
Optical Profilometry ◽  
Spectral Ellipsometry ◽  
Entire Area ◽  
Spectroscopy Optical

The features of thin-film membranes, which are formed above round holes in silicon substrates using the Bosch-process are considered. The membrane has a complex shape due to the presence of the stress state of the initial films. The analysis of the dependence of the membrane deflection w on the supplied overpressure P is used to calculate the mechanical characteristics of the membranes. In this case, it is necessary to determine directly on the membrane its diameter, the thickness of the constituent layers, the change in the relief of the membrane surface over its entire area as the excess pressure P. Determination of the membrane diameter and the thicknesses of the constituent layers is shown by the example of p-Si*/SiNx/SiO2 and SiNх/SiО2/SiNх/SiО2 membranes. We used spectral ellipsometry, energy-dispersive X-ray spectroscopy, optical profilometry, optical microscopy. The influence of the peculiarities of the fixing conditions on the stress-strain state of membranes is shown, and the assessment is carried out by means of numerical modeling. A technique has been developed for measuring and calculating the mechanical characteristics of membranes that have an initial deflection. The calculation result is shown on the example of a membrane with an initial deflection of 2 µm – SiNх/SiО2/SiNх/SiО2 and a membrane with an initial deflection of 30 µm – Al/SiO2/Al.

scholarly journals Determination of platelet antigens and glycoproteins in the human fetus

Blood ◽  
1986 ◽  
Vol 68 (2) ◽  
pp. 488-492 ◽  
Author(s):  
Y Gruel ◽  
B Boizard ◽  
F Daffos ◽  
F Forestier ◽  
J Caen ◽  
...  
Keyword(s):  
Monoclonal Antibodies ◽  
Human Fetus ◽  
Antenatal Diagnosis ◽  
Polyclonal Antibodies ◽  
Umbilical Vein ◽  
Membrane Surface ◽  
Platelet Suspension ◽  
Direct Puncture ◽  
Normal Human

Abstract The autosomal recessive transmission of Glanzmann's thrombasthenia (GT) and Bernard-Soulier syndrome (BSS), together with requests of families who already had children with these diseases, prompted us to investigate the feasibility of their antenatal diagnosis. The preliminary step leading to the early detection of GT or BSS was to characterize, in the normal human fetus, the platelet antigens and glycoproteins (GPs) and to define their normal amounts on the membrane surface. Blood samples from 32 fetuses between 18 to 26 weeks of gestation were collected by direct puncture of the umbilical vein using an ultrasound-guided needle. Polyclonal antibodies from human origin directed against PLA1, Leka antigens, and the GPIIb IIIa complex (IgGL), or murine monoclonal antibodies specific for GPIb (AN51, 6D1), GPIIIa (AP-3), or GPIIb IIIa (AP-2) were studied using platelet suspension immunofluorescence tests. The binding of each antibody was quantified using a cytofluorograph (Ortho 50H). PLA1 and Leka antigens were expressed in normal amounts on fetal platelets as early as 16 weeks of intrauterine life. The GPIIb IIIa complex quantified by polyclonal or monoclonal antibodies was in the same range in fetuses (IgGL = 427 +/- 23 AUF, AP-2 = 459.5 +/- 8.5; AP-3 = 536 +/- 14) and in adults (IgGL = 420 +/- 30; AP-2 = 498 +/- 11; AP-3 = 515 +/- 13). The platelet binding of antibodies that recognized GPIb was higher in fetuses (AN51 = 491.5 +/- 14; 6D1 = 479 +/- 15) than in adults (AN51 = 426.5 +/- 9; 6D1 = 449 +/- 8.7). These results suggest that immunological techniques can be applied as early as 18 weeks of gestation for the antenatal diagnosis of GT and BSS.

Determination of Sub‐Parts per Billion Boron Contamination in N+ Czochralski Silicon Substrates by SIMS

1994 ◽  
Vol 141 (12) ◽  
pp. 3453-3456 ◽  
Author(s):  
Paul K. Chu ◽  
Roger J. Bleiler ◽  
Jenny M. Metz
Keyword(s):  
Silicon Substrates ◽  
Czochralski Silicon

The macrophage capacity for phagocytosis

1992 ◽  
Vol 101 (4) ◽  
pp. 907-913 ◽  
Author(s):  
G.J. Cannon ◽  
J.A. Swanson
Keyword(s):  
Surface Area ◽  
Membrane Surface ◽  
Fc Receptors ◽  
Phagocytic Capacity ◽  
Membrane Surface Area ◽  
Murine Bone Marrow ◽  
Latex Beads ◽  
Endocytic Compartments ◽  
Frustrated Phagocytosis

Murine bone marrow-derived macrophages, which measure 13.8 +/− 2.3 microns diameter in suspension, can ingest IgG-opsonized latex beads greater than 20 microns diameter. A precise assay has allowed the determination of the phagocytic capacity, and of physiological parameters that limit that capacity. Ingestion of beads larger than 15 microns diameter required IgG-opsonization, and took 30 minutes to reach completion. Despite the dependence on Fc-receptors for phagocytosis of larger beads, cells reached their limit before all cell surface Fc-receptors were occupied. The maximal membrane surface area after frustrated phagocytosis of opsonized coverslips was similar to the membrane surface area required to engulf particles at the limiting diameter, indicating that the capacity was independent of particle shape. Vacuolation of the lysosomal compartment with sucrose, which expanded endocytic compartments, lowered the phagocytic capacity. This decrease was reversed when sucrose vacuoles were collapsed by incubation of cells with invertase. These experiments indicate that the phagocytic capacity is limited by the amount of available membrane, rather than by the availability of Fc-receptors. The capacity was also reduced by depolymerization of cytoplasmic microtubules with nocodazole. Nocodazole did not affect the area of maximal cell spreading during frustrated phagocytosis, but did alter the shape of the spread cells. Thus, microtubules may coordinate cytoplasm for engulfment of the largest particles.

Combined determination of the mechanical characteristics of polymer films

1968 ◽  
Vol 1 (5) ◽  
pp. 84-87
Author(s):  
O. F. Shlenskii ◽  
N. N. Khovanskaya ◽  
V. V. Lavrent'ev
Keyword(s):  
Polymer Films ◽  
Mechanical Characteristics

scholarly journals Effect of type cement on the mechanical strength of copper slag mortars

2013 ◽  
Vol 66 (1) ◽  
pp. 85-90 ◽  
Author(s):  
Amin Nazer ◽  
Osvaldo Pavez ◽  
Ithamar Toledo
Keyword(s):  
Environmental Impact ◽  
Flexural Strength ◽  
Construction Industry ◽  
Mechanical Characteristics ◽  
Copper Slag ◽  
Cement Mortars ◽  
Alternative Material ◽  
Binder Type ◽  
Initial Resistance

Copper slag is a massive metallurgist waste. Annual production rises up to 24.6 million tons, approximately, and the main environmental impact derived from slag disposal is the usage of great soil extensions and the resulting visual contamination of the landscape. Along time, copper slag has been used in the manufacture of concrete and cement mortars. Thus, with the aim of verifying binder-type influence in the final hardness of mortars, two types of cement were used: regular cement and high initial resistance cement. Copper slag was characterized from the chemical, mineralogical and grading viewpoints. Official Chilean regulations were used in the applied methodology for the determination of some important slag parameters. Compression and flexural strength trials were carried out on cement mortars in specialized laboratories. The obtained results showed that mortars manufactured with copper slag presented a better resistance to compression and flexural strength than mortars manufactured with normal sand, and those made with high initial resistance cement were even better. It can be concluded from this work that copper slag offers optimal mechanical characteristics to be used in the manufacturing of cement mortars, becoming a sustainable and adequate alternative material for usage in the construction industry.

Kinetics of Pt Silicide Formation Studied by Spectral Ellipsometry

1997 ◽  
Vol 470 ◽  
Author(s):  
R. Schwarz ◽  
A. Dittrich ◽  
S. M. Zhou ◽  
M. Hundhausen ◽  
L. Ley ◽  
...  
Keyword(s):  
Activation Energy ◽  
Crystalline Silicon ◽  
Silicon Substrates ◽  
Silicide Formation ◽  
Spectral Ellipsometry ◽  
Step Process ◽  
Depth Profiles ◽  
Ellipsometric Angle ◽  
Kinetics Of

ABSTRACTSuicide formation during thermal annealing of thin Pt layers deposited by evaporation onto crystalline silicon substrates was studied by in-situ spectral ellipsometry. As was shown in an earlier study, Pt suicide is formed in a two-step process with intermediate stages of Pt2Si and PtSi at temperatures of about 190 and 240 °C, respectively. We observed a shift of about 15 °C of the di- and monosilicide formation, when the anneal rate was lowered from 3 to 1 K/min. The analysis of the reaction kinetics using the normalized ellipsometric angle δ yields a good fit to the data for different anneal rates with an activation energy of (1.6 ± 0.2) eV. The underlying model of suicide formation through a multilayer system was checked with depth profiles and compositional information obtained from Rutherford Backscattering.

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