scholarly journals Влияние углеродных нанотрубок на электрические и механические свойства хитозановых пленок

2022 ◽  
Vol 92 (3) ◽  
pp. 435
Author(s):  
А.М. Камалов ◽  
В.В Kодолова-Чухонцева ◽  
E.Н Дресвянина ◽  
T.П Масленникова ◽  
И.П Добровольская ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Electrical Conductivity ◽  
Scanning Electron Microscopy ◽  
Composite Films ◽  
X Ray Diffraction ◽  
Electronic Components ◽  
Electrical Field ◽  
Field Frequency ◽  
X Ray ◽  
Scanning Electron

Using the methods of X-ray diffraction and scanning electron microscopy, the structure of composite films based on chitosan and single-wall carbon tubes has been studied. It is shown that the introduction of carbon nanotubes leads to the ordering of the chitosan structure. Increase in concentration of nanotubes (from 0 to 3%) causes rise in the value of storage modulus from 3 to 4 GPa (DMA data), increase in electrical conductivity of samples (from 10-11 to 102 S/m), and some changes in their dielectric permittivity (from 5.5. to 26 at an electrical field frequency of 1kHz). Data on the ionic and electronic components of the conductivity of the composite film are presented.

scholarly journals Synthesis, Crystal Structure Refinement, and Electrical Conductivity of Pb(8−x)Na2Smx(VO4)6O(x/2)

2014 ◽  
Vol 2014 ◽  
pp. 1-7
Author(s):  
Tatiana M. Savankova ◽  
Lev G. Akselrud ◽  
Lyudmyla I. Ardanova ◽  
Alexey V. Ignatov ◽  
Eugeni I. Get’man ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Electron Microscopy ◽  
Electrical Conductivity ◽  
Scanning Electron Microscopy ◽  
Solid Solutions ◽  
Structure Refinement ◽  
Crystal Structure Refinement ◽  
X Ray Diffraction ◽  
X Ray ◽  
Scanning Electron

Solid solutions of Pb(8−x)Na2Smx(VO4)6O(x/2)were studied using X-ray diffraction analysis including Rietveld refinement and scanning electron microscopy and by measuring their electrical conductivity. Crystal structure of the solid solutions was refined and the solubility region0≤x≤0.2was determined for samarium substitution for lead under the scheme2Pb2++□→2Sm3++O2-. The influence of degree of substitution on the electrical conductivity of solid solutions was established.

scholarly journals Impact of Pyrolysis Temperature on the Properties of Eucalyptus Wood-Derived Biochar

Materials ◽  
2020 ◽  
Vol 13 (24) ◽  
pp. 5841
Author(s):  
Bruno Caio Chaves Fernandes ◽  
Kassio Ferreira Mendes ◽  
Ananias Francisco Dias Júnior ◽  
Vinícius Patrício da Silva Caldeira ◽  
Taliane Maria da Silva Teófilo ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Electrical Conductivity ◽  
Scanning Electron Microscopy ◽  
Pyrolysis Temperature ◽  
Volatile Matter ◽  
Matter Content ◽  
X Ray Diffraction ◽  
X Ray ◽  
Eucalyptus Wood ◽  
Scanning Electron

Pyrolysis conditions directly influence biochar properties and, consequently, influence the potential use of biochar. In this study, we evaluated the effects of different pyrolysis temperatures (450, 550, 650, 750, 850, and 950 °C) on the hydrogen potential, electrical conductivity, ash content, yield, volatile matter content, elemental analysis, Fourier-transform infrared spectroscopy results, X-ray diffraction results, scanning electron microscopy results, specific surface area, and micropore volume of eucalyptus wood-derived biochar. The degree of linear association between pyrolysis temperatures and biochar properties was examined using the Pearson correlation coefficient. The results showed a positive correlation of the pyrolysis temperature with the hydrogen potential value, electrical conductivity, and elemental carbon. There was a negative correlation of the pyrolysis temperature with the yield, volatile matter content, elemental oxygen, elemental hydrogen, surface area, aromaticity, hydrophilicity, and polarity indexes. The Fourier-transform infrared spectroscopy data indicated an increase in aromaticity and a decrease in the polarity of high-temperature biochar. The increased pyrolysis temperature caused the loss of cellulose and crystalline mineral components, as indicated by X-ray diffraction analysis and scanning electron microscopy images. These results indicated that changing the pyrolysis temperature enables the production of biochar from the same raw material with a wide range of physicochemical properties, which allows its use in various types of agricultural and environmental activities.

scholarly journals Study on Comparative Analysis of Polymerization of Pyrrole Using Electrochemical Method and UV Photo Irradiation

2021 ◽  
Vol 04 (07) ◽  
Author(s):  
Dr. Hemant K. Chitte ◽  
Keyword(s):  
Electron Microscopy ◽  
Electrical Conductivity ◽  
Scanning Electron Microscopy ◽  
Fourier Transform ◽  
Electrochemical Method ◽  
Chemical Nature ◽  
X Ray Diffraction ◽  
X Ray ◽  
Xrd Techniques ◽  
Scanning Electron

Polymerization of pyrrole using various methods like pyrrole using electrochemical method and UV Photo irradiation has been investigated. Fourier transform infrared spectroscopy (FTIR), Scanning electron microscopy (SEM), X-ray diffraction (XRD) techniques were used to study the internal structure, material morphology, chemical nature of conducting polymers. The temperature dependence of the electrical conductivity of the Polypyrrole, Their behavior resemble the metallic conductors.

scholarly journals EFECTS OF CHEMICAL COMPOSITION ON THE MICROSTRUCTURE AND PROPERTIES OF THE CU-Ge-Sb ALLOYS

2017 ◽  
Vol 8 (1) ◽  
Author(s):  
Dejan Gurešić ◽  
Aleksandar Đorđević ◽  
Aleksandar Marković ◽  
Milica Tomović ◽  
Nadežda Talijan ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Electrical Conductivity ◽  
Scanning Electron Microscopy ◽  
Chemical Composition ◽  
Diffraction Analysis ◽  
Eddy Current ◽  
Energy Dispersive Spectroscopy ◽  
X Ray Diffraction ◽  
X Ray ◽  
Scanning Electron

In the current study a ternary Cu-Ge-Sb system has been experimentally assessed. Chemical andphase compositions of the alloy samples from three vertical sections Cu-GeSb, Ge-CuSb and Sb-CuGe were studied using scanning electron microscopy (SEM) and energy dispersive spectroscopy(EDS) and confirmed by X-ray diffraction analysis (XRD). Hardness of the alloys was measured byBrinell method while hardness of phases was measured using micro Vickers method. Electricalconductivity of the studied alloys was measured using eddy current instrument. Based onexperimentally determined values iso-lines of hardness and electrical conductivity for the wholeternary system were calculated using assumed mathematical models.

Identification of calcium oxalate crystals in dried or fixed tobacco leaf

1984 ◽  
Vol 42 ◽  
pp. 288-289
Author(s):  
Vicki L. Baliga ◽  
Mary Ellen Counts
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Calcium Oxalate ◽  
Growth And Development ◽  
Polarized Light ◽  
Calcium Oxalate Crystals ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Scanning Electron

Calcium is an important element in the growth and development of plants and one form of calcium is calcium oxalate. Calcium oxalate has been found in leaf seed, stem material plant tissue culture, fungi and lichen using one or more of the following methods—polarized light microscopy (PLM), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and x-ray diffraction.Two methods are presented here for qualitatively estimating calcium oxalate in dried or fixed tobacco (Nicotiana) leaf from different stalk positions using PLM. SEM, coupled with energy dispersive x-ray spectrometry (EDS), and powder x-ray diffraction were used to verify that the crystals observed in the dried leaf with PLM were calcium oxalate.

Environmental scanning electron microscopy of fresh human gallstones reveals new morphologies of precipitated calcium salts

1992 ◽  
Vol 50 (2) ◽  
pp. 1322-1323
Author(s):  
Howard S. Kaufman ◽  
Keith D. Lillemoe ◽  
John T. Mastovich ◽  
Henry A. Pitt
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Environmental Scanning Electron Microscopy ◽  
Environmental Scanning ◽  
X Ray Diffraction ◽  
Calcium Salts ◽  
Cholesterol Gallstones ◽  
X Ray ◽  
Ca Carbonate ◽  
Scanning Electron

Gallstones contain precipitated cholesterol, calcium salts, and proteins. Calcium (Ca) bilirubinate, palmitate, phosphate, and carbonate occurring in gallstones have variable morphologies but characteristic windowless energy dispersive x-ray (EDX) spectra. Previous studies of gallstone microstructure and composition using scanning electron microscopy (SEM) with EDX have been limited to dehydrated samples. In this state, Ca bilirubinates appear as either glassy masses, which predominate in black pigment stones, or as clusters, which are found mostly in cholesterol gallstones. The three polymorphs of Ca carbonate, calcite, vaterite, and aragonite, have been identified in gallstones by x-ray diffraction, however; the morphologies of these crystals vary in the literature. The purpose of this experiment was to study fresh gallstones by environmental SEM (ESEM) to determine if dehydration affects gallstone Ca salt morphology.Gallstones and bile were obtained fresh at cholecystectomy from 6 patients. To prevent dehydration, stones were stored in bile at 37°C. All samples were studied within 4 days of procurement.

PENINGKATAN LAJU DISOLUSI ACYCLOVIR DENGAN METODE SISTEM DISPERSI PADAT MENGGUNAKAN POLOXAMER 188

2016 ◽  
Vol 5 (1) ◽  
pp. 6
Author(s):  
Budi Setiawan ◽  
Erizal Zaini ◽  
Salman Umar
Keyword(s):  
Electron Microscopy ◽  
Thermal Analysis ◽  
Scanning Electron Microscopy ◽  
Fourier Transform ◽  
Differential Thermal Analysis ◽  
Fourier Transform Infrared ◽  
X Ray Diffraction ◽  
Poloxamer 188 ◽  
X Ray ◽  
Scanning Electron

Sebuah penelitian tentang sistem dispersi padat dari asiklovir dengan poloxamer 188 telah dilakukan formulasi dengan pencampuran secara fisika dengan rasio 1 : 1, 1 : 3, 1 : 5 dan dispersi padat 1 : 1, 1 : 3, 1 : 5 dan penggilingan 1:1 sebagai pembanding. Dispersi padat dibuat menggunakan metode pencairan (fusi), yang digabung dengan poloxamer 188 pada hotplate kemudian asiklovir dimasukkan ke dalam hasil poloxamer 188 lalu di kocok hingga membentuk masa homogen. Semua formula yang terbentuk termasuk asiklovir poloxamer 188 murni dianalisis karakterisasinya dengan Differential Thermal Analysis (DTA), X-ray Diffraction, Scanning Electron Microscopy (SEM), dan Fourier Transform Infrared (FTIR), kemudian pengambilan dilakukan  (penentuan kadar) mengunakan spektrofotometer UV pada panjang gelombang 257,08 nm dan uji laju disolusi dengan aquadest bebas CO2 menggunakan metode dayung. Hasil pengambilan  (penentuan kadar) menunjukkan bahwa semua formula memenuhi persyaratan farmakope Amerika edisi 30 dan farmakope Indonesia edisi 4 yaitu 95-110%. Sedangkan hasil uji laju disolusi untuk campuran fisik 1: 1, dan dispersi padat 1: 1, dan penggilingan 1: 1 menunjukkan peningkatan yang nyata dibandingkan asiklovir murni. Hal ini juga dapat dilihat dari hasil perhitungan statistik  menggunakan analisis varian satu arah  SPSS 17.

Structural Characterization of Gallbladder Stones Using Energy Dispersive X-ray Spectroscopy and X-ray Diffraction

2018 ◽  
Vol 21 (7) ◽  
pp. 495-500 ◽  
Author(s):  
Hassan A. Almarshad ◽  
Sayed M. Badawy ◽  
Abdalkarem F. Alsharari
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Energy Dispersive ◽  
Spectroscopic Techniques ◽  
X Ray Diffraction ◽  
Major Health Problem ◽  
X Ray ◽  
Gallbladder Stones ◽  
Pure Cholesterol ◽  
Scanning Electron

Aim and Objective: Formation of the gallbladder stones is a common disease and a major health problem. The present study aimed to identify the structures of the most common types of gallbladder stones using X-ray spectroscopic techniques, which provide information about the process of stone formation. Material and Method: Phase and elemental compositions of pure cholesterol and mixed gallstones removed from gallbladders of patients were studied using energy-dispersive X-ray spectroscopy combined with scanning electron microscopy analysis and X-ray diffraction. Results: The crystal structures of gallstones which coincide with standard patterns were confirmed by X-ray diffraction. Plate-like cholesterol crystals with laminar shaped and thin layered structures were clearly observed for gallstone of pure cholesterol by scanning electron microscopy; it also revealed different morphologies from mixed cholesterol stones. Elemental analysis of pure cholesterol and mixed gallstones using energy-dispersive X-ray spectroscopy confirmed the different formation processes of the different types of gallstones. Conclusion: The method of fast and reliable X-ray spectroscopic techniques has numerous advantages over the traditional chemical analysis and other analytical techniques. The results also revealed that the X-ray spectroscopy technique is a promising technique that can aid in understanding the pathogenesis of gallstone disease.

scholarly journals Analytical study of Buddha sculptures in Jingyin temple of Taiyuan, China

2021 ◽  
Vol 9 (1) ◽  
Author(s):  
Xiaojian Bai ◽  
Chen Jia ◽  
Zhigen Chen ◽  
Yuxuan Gong ◽  
Huwei Cheng ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Analytical Study ◽  
Energy Dispersive Spectrometry ◽  
Analytical Techniques ◽  
X Ray Diffraction ◽  
Ancient China ◽  
X Ray ◽  
Unique Style ◽  
Scanning Electron

AbstractWith exquisite design and unique style, the painted sculptures of Tutang Buddha and two attendants Buddha in Jingyin Temple are precious cultural heritages of China. The sculpture of Tutang Buddha, which was carved from a mound and painted by ancient craftsmen, was rarely found in ancient China. However, due to natural and human factors, the sculptures were severely damaged. Obviously, they require urgent and appropriate protection and restoration. In this study, samples taken from the sculptures were analysed through multiple analytical techniques, including scanning electron microscopy with energy dispersive spectrometry (SEM–EDS), Raman spectroscopy, X-ray diffraction (XRD), optical microscopy (OM) and granulometry. The analysis results enable us to infer the techniques used by the craftsmen in making the sculptures and provide a reliable evidence for the conservation and future protection of these and similar sculptures.

Preliminary Preparation and Characterization Studies of Cellulose from Merbau (Intsia bijuga)

2012 ◽  
Vol 620 ◽  
pp. 314-319
Author(s):  
Nur Amira Mamat Razali ◽  
Fauziah Abdul Aziz ◽  
Saadah Abdul Rahman
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Alkaline Treatment ◽  
Raw Material ◽  
X Ray Diffraction ◽  
X Ray ◽  
Preliminary Preparation ◽  
Characterization Studies ◽  
Scanning Electron

Hardwood is wood from angiosperm trees. The characteristic of hardwood include flowers, endosperm within seeds and the production of fruits that contain the seeds. This paper aims to discuss the preparation and characterization of cellulose obtained from hardwood. The hardwood Merbau (Intsia bijuga) was chosen as raw material in this study. Alkaline treatment and delignification methods were used for the preparation of cellulose. Acid hydrolysis was employed to produce cellulose nanocrystal (CNC). The treated and untreated samples were characterized using x-ray diffraction (XRD) and field emission scanning electron microscopy (FE-SEM). The final product, from both trated and untreated samples were then compared.

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