scholarly journals Axial dispersion model in predictive mass transfer correlation for random pulsed packed column

2015 ◽  
Vol 21 (1-1) ◽  
pp. 77-83
Author(s):  
R. Teflanab ◽  
S.M. Ghoreishi ◽  
J. Safdari ◽  
M. Torab-Mostaedi

The continuous phase volumetric overall mass transfer coefficient in a ceramic intalox saddle pulsed packed extraction column using axial dispersion model was studied for two different liquid-liquid systems containing water/acetone/toluene and water/acetone/n-butyl acetate. The effects of pulsation intensity, continuous and dispersed phase flow rates on mass transfer coefficient were investigated. The experimental results indicated that the mass transfer coefficient was enhanced by increasing pulsation intensity and dispersed and continuous phase flow rates. The utilization of nonlinear least square method provided a new predictive correlation for the continuous phase overall mass transfer coefficient. The developed mass transfer model was validated via the comparison of the modeling data with experimental results with 18.7% average absolute relative error (AARE). Furthermore, one empirical correlation was developed for prediction of the continuous phase overall mass transfer coefficient as the function of the aforementioned operating variables.

Author(s):  
Hoang Nghia Vu ◽  
Xuan Linh Nguyen ◽  
Sangseok Yu

Abstract In a fuel cell vehicle, the water content of the gas supply within certain ranges plays a key role in improving the performance of a proton exchange membrane. The lower limit of water content in the air supply is to avoid the problem of drying-out, while the upper prevents flooding. Water management can be accomplished by a membrane humidifier which allows water vapor to permeate the mixture from the side having the higher water concentration, moving to the other side of the membrane. In this study, the variation in water content collected at the outlet of a membrane humidifier is investigated with a one-dimensional mass exchanger model and various operating variables. The vapor concentration of outlet flows is affected by operating temperature and relative humidity of the membrane humidifier. Relative humidity of the dry side at the point of outlet flow, to be supplied to the fuel cell module, is the key characteristic. The analogy of the effectiveness-NTU approach for heat transfer is used to analyze the characteristics of the mass exchanger. Mass flux through the membranes is estimated with an overall mass transfer coefficient which represents vapor transport characteristics moving through the membrane module. This coefficient has a similar role to the overall heat transfer coefficient in heat exchanger analysis. This parametric study is conducted to understand the effects of different variables. The Effectiveness-NTU methodology of mass transfer uses the overall mass transfer coefficient and the mass transfer rate, as evaluated experimentally. Simulink software is then employed to deliver outcomes of the model for different operating conditions.


2017 ◽  
Vol 114 ◽  
pp. 1665-1670 ◽  
Author(s):  
Xiaomei Wu ◽  
Min He ◽  
Yunsong Yu ◽  
Zhen Qin ◽  
Zaoxiao Zhang

2021 ◽  
Vol 7 (1) ◽  
pp. 25
Author(s):  
Pao-Chi Chen ◽  
Hsun-Huang Cho ◽  
Jyun-Hong Jhuang ◽  
Cheng-Hao Ku

In order to select the best mixed amines in the CO2 capture process, the absorption of CO2 in mixed amines was explored at the required concentrations by using monoethanolamine (MEA) as a basic solvent, mixed with diisopropanolamine (DIPA), triethanolamine (TEA), 2-amino-2-methyl-1-propanol (AMP), and piperazine (PZ). Here, a bubble column was used as the scrubber, and a continuous operation was adopted. The Taguchi method was used for the experimental design. The conditional factors included the type of mixed amine (A), the ratio of the mixed amines (B), the liquid feed flow (C), the gas-flow rate (D), and the concentration of mixed amines (E). There were four levels, respectively, and a total of 16 experiments. The absorption efficiency (EF), absorption rate (RA), overall mass transfer coefficient (KGa), and scrubbing factor (ϕ) were used as indicators and were determined in a steady-state by the mass balance and two-film models. According to the Taguchi analysis, the importance of the parameters and the optimum conditions were obtained. In terms of the absorption efficiency (EF), the absorption rate (absorption factor) (RA/ϕ), and the overall mass transfer coefficient (KGa), the order of importance is D > E > A > B > C, D > E > C > B > A, and D > E > C > A > B, respectively, and the optimum conditions are A1B4C4D3E3, A1B3C4D4E2, A4B2C3D4E4, and A1B1C1D4E1. The optimum condition validation results showed that the optimal values of EF, RA, and KGa are 100%, 30.69 × 10−4 mol/s·L, 1.540 l/s, and 0.269, respectively. With regard to the selection of mixed amine, it was found that the mixed amine (MEA + AMP) performed the best in the CO2 capture process.


2015 ◽  
Vol 31 (4) ◽  
Author(s):  
Reza Afshar Ghotli ◽  
Abdul Raman Abdul Aziz ◽  
Shaliza Ibrahim

AbstractA general review on correlations to evaluate mass transfer coefficients in liquid-liquid was conducted in this work. The mass transfer models can be classified into continuous and dispersed phase coefficients. The effects of drop size and interfacial area on mass transfer coefficient were investigated briefly. Published experimental results for both continuous and dispersed phase mass transfer coefficients through different hydrodynamic conditions were considered and the results were compared. The suitability and drawbacks of these correlations depend on the operating conditions and hydrodynamics. Although the results of these models are reasonably acceptable, they could not properly predict the experimental results over a wide range of designs and operating conditions. Therefore, proper understanding of various factors affecting mass transfer coefficient needs to be further extended.


2018 ◽  
Vol 7 (1) ◽  
pp. 731
Author(s):  
Panut Mulyono

Copper has been extracted by trtbuthyl phosphate-kerosene from a dilute aqueous solution with a double- stage mixer-settler extraction column. The extraction column used in this experiment was made of glass. The mixer diameter was equal to the diameter of settler was 13 cm. Both the mixer and settler heights were 8 cm. Drop coalescer was mounted in the middle of mixer and settler separator. The diameter of drop coalescer was 6 cm with the thickness of 1 cm. The hole diameter of drop coalescer was 1 mm The stirrer used in this experiment was cross flat blade with the diameter and width of the impeller was 6 cm and 8 mm, respectively. The overall volumetric coefficient of mass transfer (Kca) increased by increasing the flowrate of the continuous phase (Lc) at the constants stirring speed (N) and flowrate of the dispersed phase (Ld). The increase of Lc from 4.1634 cm3/second to 17.9436 cm3/second increased the Kca value from 6.6387x10-5/second to 23.1561x10-5/second or 248.8% The value of Kca was also increase by increasing N at the constant values of Lc and Ld Thie increase of N from 3.3333 rps to 8.3333 rps increased the Kca value from 6.0288x10-5/second to 6.6387x10-5/second or 10.1%.Keywords: Mass Transfer Coefficient, Extraction, Copper, Double-Stage Mixer-SettlerAbstrak Penelitian ini mempelajari perpindahan massa antar fasa pada ekstraksi Cu dart larutan CuSO4.5H2O dengan menggunakan pelarut tributyl phosphate dalam kerosin yang dilakukan dalam kolom ekstraksi double-stage mixer-settler yang dtsusun vertikal. Kolom ekstraksi mixer-settler dibuat darti gelas dengan diameter mixer sama dengan diameter sealer, yaitu 13 cm. Tinggi mixer juga sama dengan tinggt settler, yaitu 8 cm. Diameter drop coalescer 8 cm, tebal 1 cm, dan diameter lubangnya 1 mm. Pengaduk yang digunakan berbentuk flat blade dengan diameter 6 cm dan lebar blade 8 mm. Koeftsien perpindahan massa volumetris keseluruhan (Kca) naik dengan naiknya kecepatan alir fasa kontinyu (Lc) pada kecepatan putaran pengaduk (N) dan kecepatan alir fasa dispersi (Ld) tetap. Kenatkan nilai Lc dart 4,1634 cm3/detik menjadi 17,9436 cm3/detik meningkatkan nilai Kca dart 6,6387x10-5/detik menjadi 23,1561x10-5/detik atau 248,8% Kca juga naik dengan naiknya N pada Lc dan Ld yang tetap. Kenaikan nilai N dart 3,3333 rps menjadi 8,3333 rps meningkatkan nilai Kca dart 6,0288x10-5/detik menjadt 6,6387x10-5/detik atau 10,1%.Kata Kunci : Koefesien Perpindahan Massa, Ekstraksi, Tembaga, Double-Stage Mixer-Settler


2020 ◽  
Vol 13 (1) ◽  
pp. 67-73
Author(s):  
Elaf Thamera ◽  
Salih Abduljabbar Rushdi

In this work, an absorption technology   was used actually to investigation the  mass transfer coefficient of carbon dioxide from a gaseous mixture (air, carbon dioxide) in  blended solution Monoethanolamine (MEA) and Diethanolamine (DEA)  in a bubble column reactor (BCR) . The bubble column reactor(BCR) was made of Plexiglas with 1.5 m high and 0.1 m inside diameter. The overall mass transfer coefficient (  was evaluated at different operating conditions , gas flow rate, air Flow rate ,liquid flow rate .Where the gas flow rates were 10, 15 and 20 L /min ,  air flow rate 100,150 and 200 L/h ,and liquid flow rate 5 ,10,15 L /min . This experiment  by   using  continuous   process with helping centrifugal  pump  . High-performance gas chromatographic (GC) was performed to evaluate  loading during absorption experiment . The  experimental results have shown that the   loading in range of  0.581-1.367 (mol  /mole amine),and the maximum value of overall mass transfer coefficient ( KG) was 0.04 S-1 .


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