scholarly journals Determination of microstructural changes by severely plastically deformed copper-aluminum alloy: Optical study

2014 ◽  
Vol 50 (1) ◽  
pp. 61-68 ◽  
Author(s):  
N. Romcevic ◽  
M. Gilic ◽  
I. Anzel ◽  
R. Rudolf ◽  
M. Mitric ◽  
...  

Our work deals with the problem of producing a complex metal-ceramic composite using the processes of internal oxidation (IO) and severe plastic deformation. For this purpose, Cu-Al alloy with 0.4wt.% of Al was used. IO of sample serves in the first step of the processing as a means for attaining a fine dispersion of nanosized oxide particles in the metal matrix. Production technology continues with repeated application of severe plastic deformation (SPD) of the resulting metalmatrix composite to produce the bulk nanoscaled structural material. SPD was carried out with equal channel angular pressing (ECAP), which allowed that the material could be subjected to an intense plastic strain through simple shear. Microstructural characteristics of one phase and multiphase material was studied on internally oxidized Cu with 0.4wt.% of Al sample composed of one phase copper-aluminum solid solution in the core and fine dispersed oxide particles in the same matrix in the mantle region. In this manner AFM, X-ray diffraction and Raman spectroscopy were used. Local structures in plastically deformed samples reflect presence of Cu, CuO, Cu2O, Cu4O3 or Al2O3 structural characteristics, depending on type of sample.

2006 ◽  
Vol 519-521 ◽  
pp. 1485-1492 ◽  
Author(s):  
Z. Horita

The process of severe plastic deformation (SPD) makes it possible to reduce the grain size to the submicrometer or nanometer range in many metallic materials. When the SPD process is applied to age hardenable alloys, it may also be possible to control aging behavior. In this study, a technique of equal-channel angular pressing (ECAP) is used as an SPD process and aging behavior is examined on the three selected Al alloy systems such as Al-Ag, Al-Mg-Si and Al-Si-Ge. The microstructures are observed using transmission electron microscopy and the mechanical properties including hardness are measured. It is shown that the SPD process introduces unusual phenomena in the precipitation process and there should be a potential for enhancement of strength over the conventional age-hardening process or for improvement of ductility while keeping the high strength.


2009 ◽  
Vol 67 ◽  
pp. 53-58
Author(s):  
V. Anil Kumar ◽  
M.K. Karthikeyan ◽  
Rohit Kumar Gupta ◽  
P. Ramkumar ◽  
P.P. Sinha

Severe plastic deformation processes (SPD) are gaining importance as advanced materials processing techniques and hold immense potential in obtaining ultra fine-grained high strength materials. Among the SPD techniques, Equal channel angular pressing (ECAP) has its own merits to produce materials with ultra fine grains in bulk with better mechanical properties. The material deforms with high level of plastic strain inside the channel resulting in grain refinement of the output material with improvement in mechanical properties. A very viable die configuration was conceptualized and die was made with 1200 channel angle. Processing of 25 mm dia. of Al alloy AA2219 at room temperature was successfully carried out and grain refinement was observed. The mechanism of grain refinement has been studied using optical and transmission electron microscopy (TEM). It was observed that low energy dislocation structure (LEDS) forms concurrently with sub-grain structure due to dislocation rearrangements, which provide stability to the evolving sub-grain structure. Dislocation mobility is hindered by the presence of precipitates and / or intermetallic dispersoids present in the matrix and results in presence of dislocations in grain interiors. The pile up of dislocations at intermetallic dispersoids was confirmed from the dark field TEM micrographs. Present paper describes the experimental procedure and followed to attain severe plastic deformation through ECAP. Increase in hardness as well as refinement in the grain size after 5-passes have been discussed in light of extensive optical and TEM. The mechanisms of grain refinement to achieve nano-grained structure and strengthening accrued from the grain refinement through ECAP has been discussed.


2006 ◽  
Vol 503-504 ◽  
pp. 515-520 ◽  
Author(s):  
Igor V. Alexandrov ◽  
V.V. Latysh ◽  
Sun Ig Hong ◽  
S.N. Faizova ◽  
V.M. Polovnikov

The current work presents new results of investigation of properties and structure of nanocrystalline and submicrocrystalline Cu-1%Cr-0.7%Al alloy. Two severe plastic deformation (SPD) techniques were applied to refine the structure: high pressure torsion and equal-channel angular pressing (ECAP). The first technique was applied to conduct preliminary studies of the alloy different thermal treatments as before SPD as well as after it. A new technological thermomechanical technique for processing of bulk billets of Cu-1%Cr-0.7%Al alloy possessing an ultrafine grained structure was developed on the basis of the obtained results. This technique comprises a combination of ECAP and other deformational processes with the thermal treatment. High values of the tensile strength and yield stress - 700 MPa and 16% accordingly – have been obtained as a result of such treatment, whereas these values after conventional treatment consisted 450 MPa and 20% respectively.


2017 ◽  
Vol 62 (1) ◽  
pp. 159-166 ◽  
Author(s):  
A. Fata ◽  
G. Faraji ◽  
M. M. Mashhadi ◽  
V. Tavakkoli

Abstract In the current study, severe plastic deformation (SPD) was applied on a commercial Mg-3Al-1Zn alloy tubes via parallel tubular channel angular pressing (PTCAP) route. Different passes of PTCAP process were applied, and microstructure, hardness and tensile properties at the room, and elevated temperatures were evaluated. The results showed that bimodal microstructure appeared and led to AZ31 alloy represented higher hardness, higher strength with a reasonable elongation at room temperature. Similarly, very high elongation to failure was achieved at a higher temperature. The increase in the number of SPD passes up to two, leads to increasing the ductility up to 263% at 400°C. Then, an increase in the number of PTCAP passes to three, leads to decrease in the ductility as the results of formation of microvoids when SPD processing at higher equivalent strains without a sufficient hydrostatic compressive stress. Relatively ductile fracture mode was also occurred in all samples.


2014 ◽  
Vol 783-786 ◽  
pp. 2647-2652 ◽  
Author(s):  
Megumi Kawasaki ◽  
Terence G. Langdon

Severe plastic deformation (SPD) is an attractive processing method for refining microstructures to have ultrafine grain sizes within the submicrometer or even the nanometer levels. In SPD, the most promising techniques are equal-channel angular pressing (ECAP) and high-pressure torsion (HPT). A conventional superplastic Zn-22% Al eutectoid alloy was processed by ECAP and HPT. Experiments were conducted to demonstrate the evolution of hardness and microstructure and the enhancement of superplastic properties of the Zn-Al alloy after processing by the SPD techniques. In addition, flow mechanisms of the Zn-22% Al alloy are discussed by utilizing a deformation mechanism map.


Author(s):  
Андрей Дмитриевич Бухтеев ◽  
Виктория Буянтуевна Бальжиева ◽  
Анна Романовна Тарасова ◽  
Фидан Гасанова ◽  
Светлана Викторовна Агасиева

В данной статье рассматривается применение и технологии получения наноструктурированных поверхностей. Рассмотрены такие методы как компактирование порошков (изостатическое прессование, метод Гляйтера), интенсивная пластическая деформация (угловое кручение, равноканальное угловое прессование, обработка давлением многослойных композитов) и модификация поверхности (лазерная обработка, ионная бомбардировка). This article discusses the application and technology for obtaining nano-structured surfaces. Methods such as compaction of powders (isostatic pressing, Gleiter method), severe plastic deformation (angular torsion, equal-channel angular pressing, pressure treatment of multilayer composites) and surface modification (laser treatment, ion bombardment) are considered.


2010 ◽  
Vol 667-669 ◽  
pp. 925-930
Author(s):  
S.V. Krymskiy ◽  
Elena Avtokratova ◽  
M.V. Markushev ◽  
Maxim Yu. Murashkin ◽  
O.S. Sitdikov

The effects of severe plastic deformation (SPD) by isothermal rolling at the temperature of liquid nitrogen combined with prior- and post-SPD heat treatment, on microstructure and hardness of Al-4.4%Cu-1.4%Mg-0.7%Mn (D16) alloy were investigated. It was found no nanostructuring even after straining to 75%. Сryodeformation leads to microshear banding and processing the high-density dislocation substructures with a cell size of ~ 100-200 nm. Such a structure remains almost stable under 1 hr annealing up to 200oC and with further temperature increase initially transforms to bimodal with a small fraction of nanograins and then to uniform coarse grained one. It is found the change in the alloy post–SPD aging response leading to more active decomposition of the preliminary supersaturated aluminum solid solution, and to the alloy extra hardening under aging with shorter times and at lower temperatures compared to T6 temper.


2009 ◽  
Vol 23 (06n07) ◽  
pp. 1621-1626
Author(s):  
HYOUNG SEOP KIM

The technique of severe plastic deformation (SPD) enables one to produce metals and alloys with an ultrafine grain size of about 100 nm and less. As the mechanical properties of such ultrafine grained materials are governed by the plastic deformation during the SPD process, the understanding of the stress and strain development in a workpiece is very important for optimizing the SPD process design and for microstructural control. The objectives of this work is to present a constitutive model based on the dislocation density and dislocation cell evolution for large plastic strains as applied to equal channel angular pressing (ECAP). This paper briefly introduces the constitutive model and presents the results obtained with this model for ECAP by the finite element method.


2011 ◽  
Vol 53 (12) ◽  
pp. 1325-1330
Author(s):  
Ya. A. Abzgildin ◽  
R. F. Al’mukhametov ◽  
N. G. Zaripov ◽  
H. Ya. Mulyukov

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