scholarly journals SYNTHESIS AND CHARACTERIZATION OF HEMATITE (Fe2O3) EXTRACTED FROM IRON ORE BY PRECIPITATION METHOD

2016 ◽  
Vol 16 (1) ◽  
pp. 15-17
Author(s):  
Andia Andia ◽  
Adi Rahwanto ◽  
Zulkarnanin Jalil
Keyword(s):  
Magnetic Separation ◽  
Steel Industry ◽  
Iron Ore ◽  
Precipitation Method ◽  
Synthesis And Characterization ◽  
X Ray Diffraction ◽  
Precipitation Mechanism ◽  
X Ray ◽  
Hematite Fe2o3

Indonesia has a lot of mining material of iron ore that could be used for various purposes in the steel industry or for other. This research, has synthesized and characterization of hematite from local iron ore from Lhoong area by precipitation mechanism. The iron ore powder was magnetic separation with magnet then mixed with HCl and NH4OH. Then, it was dried at temperature of 150 ºC and calcinated at 500º C for 2 hours. Characterizations were perfomed using X-ray Diffraction (XRD) and X-ray Fluorescence (XRF). As the results, it was found that the magnetic separation iron ore showed the composition of Fe2O3 (95.99%), SiO2 (2.10%). Then, by precipitation mechanism, the composition of Fe2O3 found around 96.58%. Next, the synthesis result are characterized with XRD show that the main phase is dominan in iron ore of Lhoong is hematit (Fe2O3). Scherrer calculations showed that precipitation mechanism to reducing grain size, the process of magnetic separation (58.009 µm) and the precipitation mechanism (20.950 µm.)

scholarly journals Synthesis and characterization of apatite silicated powders with wet precipitation method

2021 ◽  
Vol 234 ◽  
pp. 00106
Author(s):  
Houda Labjar ◽  
Hassan Chaair
Keyword(s):  
Electron Microscopy ◽  
Heat Treatment ◽  
Analytical Techniques ◽  
Precipitation Method ◽  
Synthesis And Characterization ◽  
X Ray Diffraction ◽  
X Ray ◽  
Wet Precipitation ◽  
Scanning Electron

The synthesis of apatite silicated Ca10(PO4)6-x(SiO4)x(OH)2-x (SiHA) with 0≤x≤2 was investigated using a wet precipitation method followed by heat treatment using calcium carbonate CaCO3 and phosphoric acid H3PO4 and silicon tetraacetate SiC8H20O4 (TEOS) in medium of water ethanol, with three different silicate concentrations. After drying, the samples are ground and then characterized by different analytical techniques like X-ray Diffraction (XRD), Fourier Transform Infrared Spectroscopy (FTIR) and Scanning electron Microscopy (SEM) and chemical analysis.

Synthesis and Characterization of Ag Doped Hydroxylapatite as an Antibacterial Scaffolds Material

2009 ◽  
Vol 283-286 ◽  
pp. 250-255 ◽  
Author(s):  
Abdurrahman Bahadir ◽  
Celaletdin Ergun ◽  
Murat Baydogan
Keyword(s):  
Fourier Transforms ◽  
Precipitation Method ◽  
Synthesis And Characterization ◽  
X Ray Diffraction ◽  
Scaffold Fabrication ◽  
Density Measurements ◽  
X Ray ◽  
Fourier Transforms Infrared Spectroscopy ◽  
And Behavior

Not many studies have been found in the literature on the effect of Ag ions on the structure and phase stability of hydroxylapatite which may be recognized as important information in the scaffold fabrication. The objective of the current study is to develop a better understanding on the structure and behavior of the antibacterial Ag incorporated hydroxylapatite. In order to do this, Ag doped hydroxylapatite was made by a precipitation method, and sintered in air at 1300oC. The materials were characterized by X-ray diffraction (XRD), Fourier transforms infrared spectroscopy (FTIR), density measurements and scanning electron microscopy (SEM).

scholarly journals SYNTHESIS AND CHARACTERIZATION OF HEMATITE (Fe2O3) OF IRON ORE AND MAGNETITE (Fe3O4) FROM IRON SAND THROUGH PRECIPITATION METHOD FOR INDUSTRIAL RAW MATERIALS

2020 ◽  
Vol 12 (2) ◽  
pp. 37-42
Author(s):  
Andia Fatmaliana ◽  
Maulinda Maulinda ◽  
Nirmala Sari
Keyword(s):  
Grain Size ◽  
Iron Ore ◽  
Extraction Process ◽  
Precipitation Method ◽  
Synthesis And Characterization ◽  
Size Difference ◽  
Precipitation Process ◽  
X Ray ◽  
Magnetite Fe3o4

Indonesia is a country that has enormous iron ore and iron sand mine that can be utilized for various industrial purposes. This research has been successfully conducted synthesis and characterization of hematite iron ore and magnetite from iron sand. Iron sand and iron ore that has been crushed manually repaired with a magnet was carried out with the HCl, and NH4OH then dried in the temperature of 150 oC and calcinated at a temperature of 500 oC. Characterization was carried out using X-ray diffraction (XRD) and X-ray fluorescence (XRF), where the preliminary information obtained from XRF results in an iron ore sample by manual separation have 95.99% of Fe2O3 and followed by compounds SiO2 (2.10%). While the iron sand contains 81.42% of Fe3O4 and 2.5% of SiO2. After the precipitation process, Fe2O3 compounds contained in iron ore has a content of 96.58% and Fe3O4 compounds contained in iron sand (86.73%).  The results of XRD indicate the dominant primary phase in iron ore is hematite or Fe2O3, and in iron, sand is magnetite Fe3O4, Before the extraction process, Fe2O3 was 58.009 μm in size and after the process of extracting the particles was reduced to 20.950 μm. While the Fe3O4, prior to the extract, has a grain size of 59.009 μm, and after an extraction process, the grain size reduced into 25.950 μm. The calculation results indicate there is a slight size difference between the grain size of iron sand and iron ore.

Synthesis and Characterization of Hexagonal Prismatic Ca10(PO4)6(OH)2 Prepared by Homogeneous Precipitation Method

2011 ◽  
Vol 391-392 ◽  
pp. 1239-1243
Author(s):  
Zhan Hui Zhang ◽  
Zhi Liang Huang ◽  
Jian Qiu Li ◽  
Ru An Chi ◽  
Yue Hua Hu ◽  
...  
Keyword(s):  
Growth Process ◽  
Crystal Morphology ◽  
Precipitation Method ◽  
Synthesis And Characterization ◽  
Hexagonal Prism ◽  
Homogeneous Precipitation ◽  
X Ray Diffraction ◽  
X Ray ◽  
Homogeneous Precipitation Method

Hexagonal prismatic hydroxyapatite (Ca10(PO4)6(OH)2, HAP) was successfully prepared by a homogeneous precipitation method. The products were characterized by X-ray diffraction, Fourier transform infrared spectrum, and scanning electron microscope. The growth process of the hexagonal prism was surveyed in detail based on the effects of the reaction time on the phase composition and the crystal morphology.

Synthesis and Characterization of Fe and Fe2O3 Nanoparticles

2013 ◽  
Vol 678 ◽  
pp. 46-49 ◽  
Author(s):  
Ponnaian Peula Kumari ◽  
Rachel Oommen ◽  
Chinna Kannaiyan Senthil Kumaran ◽  
Mariyappan Thambidurai ◽  
Natarajan Muthukumarasamy ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Secondary Phase ◽  
Chemical Precipitation ◽  
Precipitation Method ◽  
Synthesis And Characterization ◽  
Cubic Phase ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron

Fe and Fe2 O3 nanoparticle have been synthesized by chemical precipitation method. The x-ray diffraction studies indicate the formation of Fe and Fe2 O3 nanoparticles with cubic phase and no secondary phase was observed. Surface morphology of Fe and Fe2 O3 has been studied using scanning electron microscopy (SEM). Transmission electron microscopy (TEM) images reveal that Fe and Fe2 O3 nanoparticle have size ranging from 25-41 nm.

Synthesis and characterization of TiN / Ti / AISI 410 coatings

2018 ◽  
Vol 2 (1) ◽  
pp. 7
Author(s):  
S Chirino ◽  
Jaime Diaz ◽  
N Monteblanco ◽  
E Valderrama
Keyword(s):  
Synthesis And Characterization ◽  
Photoemission Spectroscopy ◽  
X Ray Diffraction ◽  
X Ray ◽  
Columnar Grains ◽  
Tin Thin Films ◽  
Steel Aisi ◽  
Interacting Surfaces ◽  
Stainless Steel Aisi

The synthesis and characterization of Ti and TiN thin films of different thicknesses was carried out on a martensitic stainless steel AISI 410 substrate used for tool manufacturing. The mechanical parameters between the interacting surfaces such as thickness, adhesion and hardness were measured. By means of the scanning electron microscope (SEM) the superficial morphology of the Ti/TiN interface was observed, finding that the growth was of columnar grains and by means of EDAX the existence of titanium was verified.  Using X-ray diffraction (XRD) it was possible to observe the presence of residual stresses (~ -3.1 GPa) due to the different crystalline phases in the coating. Under X-ray photoemission spectroscopy (XPS) it was possible to observe the molecular chemical composition of the coating surface, being Ti-N, Ti-N-O and Ti-O the predominant ones.

scholarly journals Synthesis and Characterization of Clay Polymer Nanocomposites of P(4VP-co-AAm) and Their Application for the Removal of Atrazine

Polymers ◽  
2019 ◽  
Vol 11 (4) ◽  
pp. 721 ◽  
Author(s):  
Jorge A. Ramírez-Gómez ◽  
Javier Illescas ◽  
María del Carmen Díaz-Nava ◽  
Claudia Muro-Urista ◽  
Sonia Martínez-Gallegos ◽  
...  
Keyword(s):  
Polymer Nanocomposites ◽  
Nanocomposite Materials ◽  
Synthesis And Characterization ◽  
Cross Linking ◽  
X Ray Diffraction ◽  
Numerous Species ◽  
X Ray ◽  
Different Types ◽  
Synthesized Materials

Atrazine (ATZ) is an herbicide which is applied to the soil, and its mechanism of action involves the inhibition of photosynthesis. One of its main functions is to control the appearance of weeds in crops, primarily in corn, sorghum, sugar cane, and wheat; however, it is very toxic for numerous species, including humans. Therefore, this work deals with the adsorption of ATZ from aqueous solutions using nanocomposite materials, synthesized with two different types of organo-modified clays. Those were obtained by the free radical polymerization of 4-vinylpyridine (4VP) and acrylamide (AAm) in different stoichiometric ratios, using tetrabutylphosphonium persulfate (TBPPS) as a radical initiator and N,N′-methylenebisacrylamide (BIS) as cross-linking agent. The structural, morphological, and textural characteristics of clays, copolymers, and nanocomposites were determined through different analytical and instrumental techniques, i.e., X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FTIR), and thermogravimetric analysis (TGA). Adsorption kinetics experiments of ATZ were determined with the modified and synthesized materials, and the effect of the ratio between 4VP and AAm moieties on the removal capacities of the obtained nanocomposites was evaluated. Finally, from these sets of experiments, it was demonstrated that the synthesized nanocomposites with higher molar fractions of 4VP obtained the highest removal percentages of ATZ.

scholarly journals High-pressure synthesis and characterization of the non-centrosymmetric scandium borate ScB6O9(OH)3

2020 ◽  
Vol 75 (6-7) ◽  
pp. 597-603
Author(s):  
Birgit Fuchs ◽  
Hubert Huppertz
Keyword(s):  
High Pressure ◽  
High Temperature ◽  
Synthesis And Characterization ◽  
X Ray Diffraction ◽  
X Ray ◽  
High Pressure High Temperature ◽  
Structure Solution ◽  
Temperature Experiment ◽  
Pressure Synthesis

AbstractThe non-centrosymmetric scandium borate ScB6O9(OH)3 was obtained through a high-pressure/high-temperature experiment at 6 GPa and 1473 K. Single-crystal X-ray diffraction revealed that the structure is isotypic to InB6O9(OH)3 containing borate triple layers separated by scandium layers. The compound crystallizes in the space group Fdd2 with the lattice parameters a = 38.935(4), b = 4.4136(4), and c = 7.6342(6) Å. Powder X-ray diffraction and vibrational spectroscopy were used to further characterize the compound and verify the proposed structure solution.

One Step Synthesis and Characterization of Zirconia-Graphene Composites

2012 ◽  
Vol 600 ◽  
pp. 174-177 ◽  
Author(s):  
Jian Fei Xia ◽  
Zong Hua Wang ◽  
Yan Zhi Xia ◽  
Fei Fei Zhang ◽  
Fu Qiang Zhu ◽  
...  
Keyword(s):  
Synthesis And Characterization ◽  
Two Dimensional ◽  
X Ray Diffraction ◽  
X Ray ◽  
Graphene Composite ◽  
Transmission Electron ◽  
One Step ◽  
Ft Ir ◽  
Xrd Techniques

Zirconia-graphene composite (ZrO2-G) has been successfully synthesized via decomposition of ZrOCl2•6H2O in a water-isopropanol system with dispersed graphene oxide (GO) utilizing Na2S as a precursor could enable the occurrence of the deposition of Zr4+ and the deoxygenation of GO at the same time. Transmission electron microscopy (TEM), Fourier transform infrared spectroscopy (FT-IR) and X-ray diffraction (XRD) techniques were used to characterize the samples. It was found that graphene were fully coated with ZrO2, and the ZrO2 existing in tetragonal phase, which resulted in the formation of two-dimensional composite.

Synthesis and Characterization of Multiferroic NiFe2O4/BiFeO3 Nanocomposites by Modified Pechini Method

2011 ◽  
Vol 197-198 ◽  
pp. 456-459
Author(s):  
Xian Ming Liu ◽  
Wen Liang Gao
Keyword(s):  
Pechini Method ◽  
Synthesis And Characterization ◽  
X Ray Diffraction ◽  
Magnetic Bias ◽  
Field Frequency ◽  
Magnetic Field Frequency ◽  
X Ray ◽  
Structure And Morphology ◽  
Modified Pechini Method

Spinel-perovskite multiferroics of NiFe2O4/BiFeO3 nanoparticles were prepared by modified Pechini method. The structure and morphology of the composites were examined by means of X-ray diffraction (XRD) and scanning electron microscopy (SEM). The results showed that the composites consisted of spinel NiFe2O4 and perovskite BiFeO3 after annealed at 700°C for 2h, and the particle size ranges from 40 to 100nm. VSM and ME results indicated that the nanocomposites exhibited both tuning magnetic properties and a ME effect. The ME effect of the nanocomposites strongly depended on the magnetic bias and magnetic field frequency.

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