The state of metallurgical industry of the Russian empire at the end of XIX century is analyzed. The reasons of intensification of researches in technical sciences are determined. It is presented the information about creation of technological higher educational establishment in Kharkiv city; in particular, it is shown the help in this question given by authoritative residents of Kharkiv, public of other provinces, representatives of the South of Russian Empire mining industry. It is proven that in the Kharkiv practical technological institute the first in Ukraine specialized department from training of specialists in the field of metallurgy was created. It is given the information about the first scientifically pedagogical staff of KhPTI in the field of metallurgy and attention is accented, that teachers were experienced specialistspractitioners. Basic directions of leading scientists-metallurgists scientific work by A.F Mevius, V.S. Knabbe, T.M. Ber are illustrated. Main directions of scientific interests of these scientists are found out; value of their fundamental works is shown. Provision of course of metallurgy in KhPTI by equipment for realization of research work, and also by scientific and educational literature is illustrated. Using materials of Archives, the information about opening and financing of the first industrial metallurgical laboratory is given. It is shown that the material and technical base of institute allowed carrying out researches not only for scientific and educational purposes but also by the orders of industry. The conclusion is done, that staffing at the beginning of XX century was carried out due to the graduating students of institute, but not due to invitation of graduating students of West European establishments, as it was from the beginning of KhPTI activity.