Microstructural and surface residual stress development during low-temperature gaseous nitriding of Fe-3.07at.%Mo alloy

2011 ◽  
Vol 66 (2) ◽  
pp. 94-99 ◽  
Author(s):  
H. Selg ◽  
E. Bischoff ◽  
R. Schacherl ◽  
J. Schwarzer ◽  
E. J. Mittemeijer
Author(s):  
Yong Jiang ◽  
Peng-peng Zhang ◽  
Jianming Gong

In this present paper, the effect of specimen thickness on carburized layer thickness and surface residual stress of low temperature gaseous carburized AISI316L austenitic stainless steel was investigated by using specimen with thicknesses from ∼0.1 to ∼3 mm. After 15 and 30 hrs Low Temperature Gaseous Carburization (LTGC) treatment, the carburized layer thickness, surface residual stress and surface morphology were studied by optical microscope (OM), X-ray residual stress analyzer and scanning electron microscope (SEM). The results show that the specimen original thickness has no effect on the thickness of carburized layer. Surface compressive residual stresses are constant as about −1.6 and −2.1 GPa when the specimen thicknesses are not less than 0.485 mm for 15 hrs and 0.926 mm for 30 hrs LTGC treatment respectively. With the reduction of specimen thicknesses from 0.485 to 0.081 mm for 15 hrs LTGC treatment and 0.926 to 0.082 mm for 30 hrs LTGC treatment, the compressive residual stresses declined and finally reached about +0.4 and +1.0 GPa, respectively. Surface inter-granular cracking occurred on 0.082 mm specimen after 30 hrs LTGC treatment.


Author(s):  
J. Fang ◽  
H. M. Chan ◽  
M. P. Harmer

It was Niihara et al. who first discovered that the fracture strength of Al2O3 can be increased by incorporating as little as 5 vol.% of nano-size SiC particles (>1000 MPa), and that the strength would be improved further by a simple annealing procedure (>1500 MPa). This discovery has stimulated intense interest on Al2O3/SiC nanocomposites. Recent indentation studies by Fang et al. have shown that residual stress relief was more difficult in the nanocomposite than in pure Al2O3. In the present work, TEM was employed to investigate the microscopic mechanism(s) for the difference in the residual stress recovery in these two materials.Bulk samples of hot-pressed single phase Al2O3, and Al2O3 containing 5 vol.% 0.15 μm SiC particles were simultaneously polished with 15 μm diamond compound. Each sample was cut into two pieces, one of which was subsequently annealed at 1300° for 2 hours in flowing argon. Disks of 3 mm in diameter were cut from bulk samples.


Materials ◽  
2021 ◽  
Vol 14 (11) ◽  
pp. 2767
Author(s):  
Ki-Won Jeong ◽  
Jung-Suk Han ◽  
Gi-Uk Yang ◽  
Dae-Joon Kim

Yttria-stabilized zirconia (3Y-TZP) containing 0.25% Al2O3, which is resistant to low temperature degradation (LTD), was aged for 10 h at 130–220 °C in air. The aged specimens were subsequently indented at loads ranging from 9.8 to 490 N using a Vickers indenter. The influence of preaging temperature on the biaxial strength of the specimens was investigated to elucidate the relationship between the extent of LTD and the strength of zirconia restorations that underwent LTD. The indented strength of the specimens increased as the preaging temperature was increased higher than 160 °C, which was accompanied by extensive t-ZrO2 (t) to m-ZrO2 (m) and c-ZrO2 (c) to r-ZrO2 (r) phase transformations. The influence of preaging temperature on the indented strength was rationalized by the residual stresses raised by the t→m transformation and the reversal of tensile residual stress on the aged specimen surface due to the indentation. The results suggested that the longevity of restorations would not be deteriorated if the aged restorations retain compressive residual stress on the surface, which corresponds to the extent of t→m phase transformation less than 52% in ambient environment.


2014 ◽  
Vol 783-786 ◽  
pp. 692-697 ◽  
Author(s):  
Andrew Clark ◽  
Randy J. Bowers ◽  
Derek O. Northwood

The effects of heat treatment on distortion, residual stress, and retained austenite were compared for case-carburized 4320 steel, in both the austempered and quench-and-tempered condition. Navy C-ring samples were used to quantify both size and shape distortions, as well as residual stress. The austempering heat treatment produced less distortion and a higher surface residual stress. Both hoop and axial stresses were measured; the difference between them was less than seven percent in all cases. Depth profiles were obtained for residual stress and retained austenite from representative C-ring samples for the austempered and quench-and-tempered heat treatment conditions. Austempering maintained a compressive residual stress to greater depths than quench-and-tempering. Quench-and-tempering also resulted in lower retained austenite amounts immediately beneath the surface. However, for both heat treatments, the retained austenite content was approximately one percent at depths greater than 0.5 mm.


2013 ◽  
Vol 753-755 ◽  
pp. 277-280 ◽  
Author(s):  
Wei Xiang Liu

Nano-ceramic materials had high hardness and wear resistance. Combined with current technology and cost saving, nanostructured coatings technology were carried out, using HVOF ( high velocity oxygen fuel) or plasma spraying technique can obtain high quality ceramic coating on metal substrate. Ceramic coatings produced cracks in the grinding due to grinding surface residual stress. the coatings grinding surface residual stress of engineering ceramics have been researched, grinding surface residual stress in the nanostructured ceramic coatings are being researched. the researches in this field include grinding process modeling, abrasives and grinding parameters, grinding process monitoring and control and realization of the software, the grinding mechanism and grinding damage on the surface, grinding force prediction, on-line detection, grinding on nanocoating material is a multivariable complex process.


2009 ◽  
Vol 24 (S1) ◽  
pp. S22-S25
Author(s):  
Y. B. Guo ◽  
S. Anurag

Hard turning, i.e., turning hardened steels, may produce the unique “hook” shaped residual stress (RS) profile characterized by surface compressive RS and subsurface maximum compressive RS. However, the formation mechanism of the unique RS profile is not yet known. In this study, a novel hybrid finite element modeling approach based on thermal-mechanical coupling and internal state variable plasticity model has been developed to predict the unique RS profile patterns by hard turning AISI 52100 steel (62 HRc). The most important controlling factor for the unique characteristics of residual stress profiles has been identified. The transition of maximum residual stress at the surface to the subsurface has been recovered by controlling the plowed depth. The predicted characteristics of residual stress profiles favorably agree with the measured ones. In addition, friction coefficient only affects the magnitude of surface residual stress but not the basic shape of residual stress profiles.


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