scholarly journals Three-dimensional numerical simulation of crystal growth using TSM under g-jitter conditions

2021 ◽  
Author(s):  
Elalami Asmae

The goal of this thesis is to study the effect of residual gravity on crystal growth of Silicon Germanium GE0.98 Si0.02 using the Traveling Heater Method (THM). This method has proven to be one of the most efficient techniques to grow high-quality crystals because it can be grown at relatively low temperatures compared to existing crystal growth techniques. Yet, because of natural convection due to earth's gravity, imperfection in terms of silicon distribution along the growth interface occurs. By growing crystals in a space environment, residual gravity represented by a static microgravity component and a sinusoidal component would decrease the intensity of the convective flow, which in return would lead to a more uniform silicon distribution. However, g-jitter fluctuation has proven to have a noticeable effect on the silicon distribution. Therefore, as an initial step to understand the behavior of crystal growth in space, each component of the g-jitter force will be studied thoroughly. The momentum, mass and energy equations, representing the 3D TSM model, were solved using finite element means. The preliminary results indicate that the complexity and the intensity of the silicon distribution along the growth interface are proportional to the convective flow, that partially controls the migration of silicon. Therefore, the quality of the crystal growth is assessed based on the behavior of the flow along the solvent regime. Based on the imposed static gravity in the range of 10-6 go to 10-3 go, the flow was determined to be in a diffusion mode with a velocity ranging from 10-6 cm/sec to 10-3 cm/sec. As a matter of fact, the flow intensity was noted to be positively proportional to the dominant component of both the static and the amplitude of the imposed g-jitter and negatively proportional to the frequency of the sinusoidal g-jitter. Consequently, realistic space growth conditions have proven to be an effective way of producing a homogeneous crystal since a flawless crystal silicon distribution is obtained at the growth interface.

2021 ◽  
Author(s):  
Elalami Asmae

The goal of this thesis is to study the effect of residual gravity on crystal growth of Silicon Germanium GE0.98 Si0.02 using the Traveling Heater Method (THM). This method has proven to be one of the most efficient techniques to grow high-quality crystals because it can be grown at relatively low temperatures compared to existing crystal growth techniques. Yet, because of natural convection due to earth's gravity, imperfection in terms of silicon distribution along the growth interface occurs. By growing crystals in a space environment, residual gravity represented by a static microgravity component and a sinusoidal component would decrease the intensity of the convective flow, which in return would lead to a more uniform silicon distribution. However, g-jitter fluctuation has proven to have a noticeable effect on the silicon distribution. Therefore, as an initial step to understand the behavior of crystal growth in space, each component of the g-jitter force will be studied thoroughly. The momentum, mass and energy equations, representing the 3D TSM model, were solved using finite element means. The preliminary results indicate that the complexity and the intensity of the silicon distribution along the growth interface are proportional to the convective flow, that partially controls the migration of silicon. Therefore, the quality of the crystal growth is assessed based on the behavior of the flow along the solvent regime. Based on the imposed static gravity in the range of 10-6 go to 10-3 go, the flow was determined to be in a diffusion mode with a velocity ranging from 10-6 cm/sec to 10-3 cm/sec. As a matter of fact, the flow intensity was noted to be positively proportional to the dominant component of both the static and the amplitude of the imposed g-jitter and negatively proportional to the frequency of the sinusoidal g-jitter. Consequently, realistic space growth conditions have proven to be an effective way of producing a homogeneous crystal since a flawless crystal silicon distribution is obtained at the growth interface.


Materials ◽  
2019 ◽  
Vol 12 (19) ◽  
pp. 3272
Author(s):  
Ellefsen ◽  
Arzig ◽  
Steiner ◽  
Wellmann ◽  
Runde

We have studied the influence of different SiC powder size distributions and the sublimation behavior during physical vapor transport growth of SiC in a 75 mm and 100 mm crystal processing configuration. The evolution of the source material as well as of the crystal growth interface was carried out using in situ 3D X-ray computed tomography (75 mm crystals) and in situ 2D X-ray visualization (100 mm crystals). Beside the SiC powder size distribution, the source materials differed in the maximum packaging density and thermal properties. In this latter case of the highest packaging density, the in situ X-ray studies revealed an improved growth interface stability that enabled a much longer crystal growth process. During process time, the sublimation-recrystallization behavior showed a much smoother morphology change and slower materials consumption, as well as a much more stable shape of the growth interface than in the cases of the less dense SiC source. By adapting the size distribution of the SiC source material we achieved to significantly enhance stable growth conditions.


2004 ◽  
Vol 1 (4) ◽  
pp. 953-956 ◽  
Author(s):  
W. Szuszkiewicz ◽  
E. Dynowska ◽  
J. Z. Domagala ◽  
E. Janik ◽  
E. Łusakowska ◽  
...  

1994 ◽  
Author(s):  
Marina I. Kolybayeva ◽  
Igor M. Pritula ◽  
Viacheslav M. Puzikov ◽  
Vitaly I. Salo ◽  
Serge V. Garnov ◽  
...  

2000 ◽  
Vol 29 (9) ◽  
pp. 1074-1078 ◽  
Author(s):  
Richard H. Deitch ◽  
Stephen H. Jones ◽  
Thomas G. Digges

1985 ◽  
Vol 62 ◽  
Author(s):  
H. P. Strunk ◽  
A. Kessler ◽  
E. Bauser

ABSTRACTPlanar defects have been detected by transmission electron microscopy in silicon epitaxial layers that have been grown from Ga solutions below 500 °C. According to fringe contrast analysis, this defect can be modelled by a plane of Ga atoms within the Si lattice. This plane forms during crystal growth due to local preferential incorporation of Ga atoms at crystallographically defined sites, that occur repetitively in the trains of monomolecular growth steps at the liquid/solid growth interface.


1995 ◽  
Vol 398 ◽  
Author(s):  
A.V. Bune ◽  
D.C. Gillies ◽  
S.L. Lehoczky

ABSTRACTA numerical model of heat transfer by combined conduction, radiation and convection was developed using the FIDAP finite element code for NASA's Advanced Automated Directional Solidification Furnace (AADSF). The prediction of the temperature gradient in an ampoule with HgCdTe is a necessity for the evaluation of whether or not the temperature set points for furnace heaters and the details of cartridge design ensure optimal crystal growth conditions for this material and size of crystal. A prediction of crystal/melt interface shape and the flow patterns in HgCdTe are available using a separate complementary model.


2010 ◽  
Vol 645-648 ◽  
pp. 375-378 ◽  
Author(s):  
Valdas Jokubavicius ◽  
Justinas Palisaitis ◽  
Remigijus Vasiliauskas ◽  
Rositza Yakimova ◽  
Mikael Syväjärvi

Different sublimation growth conditions of 3C-SiC approaching a bulk process have been investigated with the focus on appearance of macrodefects. The growth rate of 3C-SiC crystals grown on 6H-SiC varied from 380 to 460 μm/h with the thickness of the crystals from 190 to 230 μm, respectively. The formation of macrodefects with void character was revealed at the early stage of 3C-SiC crystal growth. The highest concentration of macrodefects appears in the vicinity of the domain in samples grown under high temperature gradient and fastest temperature ramp up. The formation of macrodefects was related to carbon deficiency which appear due to high Si/C ratio which is used to enable formation of the 3C-SiC polytype.


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