scholarly journals Holdup and characteristic velocity in a pulsed packed extraction column

2020 ◽  
Vol 9 (8) ◽  
pp. e674982543
Author(s):  
Jarlon Conceição da Costa ◽  
Luiz Mário Nelson de Góis ◽  
Silvana Mattedi e Silva
Keyword(s):  
Flow Rate ◽  
Water System ◽  
Continuous Phase ◽  
Liquid System ◽  
Operating Conditions ◽  
Extraction Column ◽  
Dispersed Phase ◽  
Internal Diameter ◽  
Phase Flow ◽  
Characteristic Velocity

The present work aims to evaluate the hydrodynamics of a pulsed packed extractor, with an internal diameter of 0.026m and a length of 1.0m, using the liquid butanol-water system. Thus, the basic parameters obtained for the hydrodynamic study of the extraction column in question as dispersed phase, slip velocity, characteristic velocity and flooding point. The methodology used in the work consisted of determining the holdup fraction of the dispersed phase, obtained through tests of simultaneous interruptions in the column feedings. The effects of frequency pulsation, dispersed phase flow rate and continuous phase flow rate investigated in the analysis of these parameters. New empirical correlations derived from the predictions of the parameters studied obtained in terms of operating variables and physical properties of the liquid system involved. The average absolute value of the relative error (AARE) was always below 5.6%. Good agreement between calculated and experimental results observed for all investigated operating conditions.

scholarly journals Dispersed phase hold-up and characteristic velocity in a pulsed packed extraction column

2012 ◽  
Vol 18 (2) ◽  
pp. 255-262 ◽  
Author(s):  
Mehdi Asadollahzadeh ◽  
Jaber Safdari ◽  
Ali Haghighi-Asl ◽  
Meisam Torab-Mostaedi
Keyword(s):  
Physical Properties ◽  
Packed Column ◽  
Operating Conditions ◽  
Empirical Correlation ◽  
Extraction Column ◽  
Dispersed Phase ◽  
Characteristic Velocity ◽  
Operating Variables ◽  
Liquid Systems ◽  
Good Agreement

Dispersed phase hold-up has been measured in a 76.2 mm diameter pulsed packed column for four different liquid-liquid systems. The effects of pulsation intensity, phase ratio, and packing characteristic on the hold-up have been investigated under a variety of operating conditions. The dispersed phase axial hold-up shows a strong non-uniformity, depending on the operating conditions. The results indicated that the characteristic velocity approach is applicable to this type of extraction column for analysis of hold-up. An empirical correlation is derived for prediction of the hold-up in terms of operating variables, physical properties of the systems, and packing geometry. Good agreement between prediction and experiments was observed for all investigated operating conditions.

scholarly journals A Newly Developed Empirical Predictive Model for the Dispersed Phase (DP) Holdup in Rotating Disc Contactors

2021 ◽  
Vol 5 (4) ◽  
pp. 79
Author(s):  
Ayham M. I. Al-Rahawi ◽  
Wallaa A. Noori ◽  
Amer A. Abdulrahman ◽  
Hasan Sh. Majdi ◽  
Issam K. Salih ◽  
...  
Keyword(s):  
Physical Properties ◽  
Flow Rate ◽  
Production Capacity ◽  
Hole Diameter ◽  
Operating Conditions ◽  
Percentage Error ◽  
Extraction Column ◽  
Dispersed Phase ◽  
Rotating Disc ◽  
Average Percentage

Newly novel developed correlations were derived to predict the dispersed phase (DP) holdup in a rotating disc contactor (RDC) extraction column. DP holdup is one of the significant parameters in the design of liquid–liquid contactors and for calculating their production capacity. Despite the availability of quite a large number of holdup prediction correlations for the RDC, most of these correlations are either general in nature or valid for a limited range of operating conditions. This study conducted an experimental and theoretical investigation of the RDC holdup under the influence of varying geometries, including variations in the dispersed phase distributor, speed of the disc, flow rate, and physical characteristics of the system. The analysis revealed that the holdup decreased with an increasing distributor hole diameter and increased with an increasing disc speed and total flow rate. The effect of the physical properties on the holdup was larger than the effect of the disc speed. Using the measurements of over 150 runs, two RDC column holdup predictive models were proposed and evaluated. The first correlation was derived in terms of the distributor hole diameter, operating parameters, system physical properties, and column geometry. The second correlation excluded the column geometry. These correlations, which consider the distributor hole inlet diameter in predicting the DP holdup for an RDC column, were presented for the first time in this study. The predictive capability of these correlations was evaluated via their standard deviation (SD) and mean average percentage error (MAPE). The respective SD and MAPE of the two correlations were 1.7 and 5.2% for the first correlation and 1.6 and 11.4% for the second.

scholarly journals Hydrodynamics of a pilot plant spray extraction column

2018 ◽  
pp. 159-168 ◽  
Author(s):  
Milan Sovilj ◽  
Branislava Nikolovski ◽  
Momcilo Spasojevic
Keyword(s):  
Pilot Plant ◽  
Droplet Diameter ◽  
Great Influence ◽  
Continuous Phase ◽  
Liquid System ◽  
Superficial Velocity ◽  
Hydrodynamic Characteristics ◽  
Extraction Column ◽  
Dispersed Phase ◽  
Axial Dispersion Coefficient

The hydrodynamic characteristics of the liquid-liquid system of toluene-water in a pilot plant spray extraction column were experimentally determined. The experimental data for hydrodynamic characteristics such as the dispersed phase holdup, mean droplet size, and the axial dispersion coefficient were obtained. The dispersed phase superficial velocity had a great influence on toluene holdup. At the same time, a strong effect of the continuous phase superficial velocity on the dispersed phase holdup was evident. The dispersed phase holdup had a tendency to increase when the ratio of the dispersed phase superficial velocity and characteristic velocity increased. The Sauter mean droplet diameter decreased with increasing dispersed phase superficial velocity when the continuous phase superficial velocity remained constant. In contrast, it was not affected by the changes in the continuous phase superficial velocity while the dispersed phase superficial velocity remained constant. It was concluded that the Peclet number increased as a result of an increase of the Reynolds number.

Investigation on the Droplet Formation Time With Xanthan Gum Solutions at a T-Junction

2012 ◽  
Author(s):  
Zhipeng Gu ◽  
Jong-Leng Liow ◽  
Guofeng Zhu
Keyword(s):  
Flow Rate ◽  
Xanthan Gum ◽  
Critical Concentration ◽  
Droplet Diameter ◽  
Droplet Formation ◽  
Continuous Phase ◽  
Formation Time ◽  
Drop Formation ◽  
Dispersed Phase ◽  
Phase Flow

Xanthan gum solutions with various concentrations were used as the dispersed phase to study the formation time for drop formation at a T-junction. Two critical concentrations (0.05 and 0.2 wt%) of xanthan gum solutions were observed resulting in three distinct regimes. The droplet diameter increased with increasing xanthan gum concentration within each regime but the transition through each critical concentration was accompanied by a significant reduction in the droplet size. Experimental results showed that the droplet formation time decreased exponentially with increasing continuous phase flow rate. It was also found that the formation time was reduced with increasing dispersed phase flow rate. Xanthan gum solutions with a higher concentration within each regime resulted in a longer formation time, and there was a decrease in the formation time at each critical concentration. The formation time consists of growth and breakup stages and the effect of xanthan gum concentration on each stage was examined.

Computational Investigation of Microdroplet Formation in a Crossflow Membrane Emulsification Process

2011 ◽  
Author(s):  
Manabendra Pathak
Keyword(s):  
Surface Tension ◽  
Flow Rate ◽  
Viscosity Ratio ◽  
Period Doubling ◽  
Continuous Phase ◽  
Inertia Force ◽  
Dispersed Phase ◽  
Phase Flow ◽  
Membrane Emulsification ◽  
Emulsification Process

Monodisperse microdroplets are formed, when a liquid is injected through a micropore into another immiscible liquid. Depending on the relative flow between the two phases, droplets may form in quiescent, coflowing and crossflowing environment. The dispersions of one phase liquid in another crossflowing liquid are observed in liquid emulsification process and the system has been used extensively in microfluidic devices to produce monodisperse microdroplets with controllable size. Liquid emulsions are widely used in food, cosmetics, pharmaceutics and polymer industries. In the present work, microdroplet formation in a crossflow membrane emulsification process has been investigated computationally using VOF/finite volume method. The full transient simulation has been carried out starting from the injection of dispersed phase to breakup into drops for different values of dispersed phase and continuous phase flow rate, surface tension and viscosity ratio of both the phases. Depending upon the values of the both phases, the droplet formation process shows the dripping and jetting behavior. The qualitative features of the two regimes and their transition have been correlated with different non-dimensional numbers such as Capillary number, Weber number and viscosity ratio of the two phase liquids. Some interesting nonlinear behavior such as period doubling been observed near the transition between the dripping and jetting regimes has. The topological characteristics of dripping, jetting and transition regimes in membrane emulsification have been observed different than in the cases of T-junction emulsification and flow focusing emulsification. Two ways of dripping to jetting transition have been observed, one with the increasing dispersed phase flow rate at constant continuous phase flow rate and other way is reducing the surface tension at constant dispersed phase flow rate. The effect of inertia force has been observed negligible for high value of surface tension and significant for lower surface tension value.

scholarly journals Prediction Models of Droplet Characteristics Based on the Locally Convergent Configurations in PMMA Microchips

2021 ◽  
Vol 2097 (1) ◽  
pp. 012027
Author(s):  
Zhongxin Liu ◽  
Zhiliang Wang ◽  
Chao Wang ◽  
Jinsong Zhang
Keyword(s):  
Flow Rate ◽  
Relative Position ◽  
Prediction Models ◽  
Continuous Phase ◽  
Lubricating Oil ◽  
Flow Rate Ratio ◽  
Phase Flow ◽  
Exponential Relationship ◽  
Two Phase ◽  
Relationship Of

Abstract This paper novel designed the local convergence configuration in the coaxial channels to study the two-phase flow (lubricating oil (continuous phase, flow rate Q c)/deionized water (dispersed phase, flow rate Q d)). Two geometric control variables, the relative position (x) and tapering characteristics (α), had the different effects on the droplet formation. The increase of relative position x caused the higher frequency and finer droplets, and the increase of convergence angle α, took the opposite effects. The results indicated that the equivalent dimensionless droplet length Ld/Wout and the flow rate ratio Qd/Qc had an exponential relationship of about 1/2. Similarly, it was found that the dispersed droplets generating frequency and the two-phase capillary number, CaTP = uTPμc/σ, had an exponential relationship. The advantage of the convergent configurations in micro-channel was the size and efficiency of droplet generation was very favorable to be controlled by α and x.

scholarly journals Experimental Study on the Effect of Locally Convergent Configurations on the Flow Pattern in PMMA Microchips

2021 ◽  
Vol 2097 (1) ◽  
pp. 012006
Author(s):  
Jinsong Zhang ◽  
Zhongxin Liu ◽  
Chao Wang ◽  
Zhiliang Wang
Keyword(s):  
Flow Rate ◽  
Rectangular Cross Section ◽  
Continuous Phase ◽  
Lubricating Oil ◽  
Phase Flow ◽  
Two Phase ◽  
Convergence Angle ◽  
Syringe Needle ◽  
Micro Flow ◽  
Two Parameters

Abstract The geometries of micro-channel play a key role in forming of digital droplets, and can be real-time or effective controlling methodologies. Local convergence regions are designed in the rectangular cross-section channels on PMMA microchips, in which two-phase coaxial jets are introduced by inserting a syringe needle. The two-phase flow (lubricating oil (continuous phase, flow rate Q c)/deionized water (dispersed phase, flow rate Q d)) is considered. Two geometric control variables, the relative position (needle displacement x) and tapering characteristics (convergence angle α), are naturally adopted to discribe such geometry configurations. The micro-flow under the change of these two parameters is mainly studied in this paper. Four kinds of characteristic flow patterns, namely, sausages, slug, dripping and jetting, are found in the experiment, and their occurring parameters and developing dynamic characteristics are discussed. The experiment shows that the increase of inner needle displacement x can produce higher frequency and finer droplets, which is in consistent with our previous results obtained in round tube experiments and simulations. While increasing the convergence angle α, contrarily, takes opposite effects.

scholarly journals KOEFISIEN PERPINDAHAN MASSA VOLUMETRIS KESELURUHAN PADA EKSTRAKSI Cu DARI LARUTAN CuSO4.5H2O DENGAN TRIRUTYL PHOSPHATE-KEROSIN DALAM DOUBLE-STAGE MIXER-SETTLER

2018 ◽  
Vol 7 (1) ◽  
pp. 731
Author(s):  
Panut Mulyono
Keyword(s):  
Aqueous Solution ◽  
Mass Transfer ◽  
Transfer Coefficient ◽  
Mass Transfer Coefficient ◽  
Tributyl Phosphate ◽  
Continuous Phase ◽  
Hole Diameter ◽  
Extraction Column ◽  
Dispersed Phase ◽  
Dilute Aqueous Solution

Copper has been extracted by trtbuthyl phosphate-kerosene from a dilute aqueous solution with a double- stage mixer-settler extraction column. The extraction column used in this experiment was made of glass. The mixer diameter was equal to the diameter of settler was 13 cm. Both the mixer and settler heights were 8 cm. Drop coalescer was mounted in the middle of mixer and settler separator. The diameter of drop coalescer was 6 cm with the thickness of 1 cm. The hole diameter of drop coalescer was 1 mm The stirrer used in this experiment was cross flat blade with the diameter and width of the impeller was 6 cm and 8 mm, respectively. The overall volumetric coefficient of mass transfer (Kca) increased by increasing the flowrate of the continuous phase (Lc) at the constants stirring speed (N) and flowrate of the dispersed phase (Ld). The increase of Lc from 4.1634 cm3/second to 17.9436 cm3/second increased the Kca value from 6.6387x10-5/second to 23.1561x10-5/second or 248.8% The value of Kca was also increase by increasing N at the constant values of Lc and Ld Thie increase of N from 3.3333 rps to 8.3333 rps increased the Kca value from 6.0288x10-5/second to 6.6387x10-5/second or 10.1%.Keywords: Mass Transfer Coefficient, Extraction, Copper, Double-Stage Mixer-SettlerAbstrak Penelitian ini mempelajari perpindahan massa antar fasa pada ekstraksi Cu dart larutan CuSO4.5H2O dengan menggunakan pelarut tributyl phosphate dalam kerosin yang dilakukan dalam kolom ekstraksi double-stage mixer-settler yang dtsusun vertikal. Kolom ekstraksi mixer-settler dibuat darti gelas dengan diameter mixer sama dengan diameter sealer, yaitu 13 cm. Tinggi mixer juga sama dengan tinggt settler, yaitu 8 cm. Diameter drop coalescer 8 cm, tebal 1 cm, dan diameter lubangnya 1 mm. Pengaduk yang digunakan berbentuk flat blade dengan diameter 6 cm dan lebar blade 8 mm. Koeftsien perpindahan massa volumetris keseluruhan (Kca) naik dengan naiknya kecepatan alir fasa kontinyu (Lc) pada kecepatan putaran pengaduk (N) dan kecepatan alir fasa dispersi (Ld) tetap. Kenatkan nilai Lc dart 4,1634 cm3/detik menjadi 17,9436 cm3/detik meningkatkan nilai Kca dart 6,6387x10-5/detik menjadi 23,1561x10-5/detik atau 248,8% Kca juga naik dengan naiknya N pada Lc dan Ld yang tetap. Kenaikan nilai N dart 3,3333 rps menjadi 8,3333 rps meningkatkan nilai Kca dart 6,0288x10-5/detik menjadt 6,6387x10-5/detik atau 10,1%.Kata Kunci : Koefesien Perpindahan Massa, Ekstraksi, Tembaga, Double-Stage Mixer-Settler

scholarly journals Hydrodynamics of pulsed sieve-plate extraction columns

2020 ◽  
Vol 74 (1) ◽  
pp. 1-14
Author(s):  
Milan Sovilj ◽  
Momcilo Spasojevic
Keyword(s):  
Continuous Phase ◽  
Liquid System ◽  
Axial Dispersion ◽  
Superficial Velocity ◽  
Dispersed Phase ◽  
Geometrical Parameters ◽  
Drop Diameter ◽  
Sieve Plate ◽  
Axial Dispersion Coefficient ◽  
Hydrodynamic Parameters

This paper presents a review of some hydrodynamic parameters in pulsed sieve-plate extraction columns. The hydrodynamic parameters in liquid-liquid systems in these columns were analyzed regarding the effects of operating and geometrical parameters. The values of Sauter mean drop diameter were function of the existing work flow regimes in the column device defined as mixer-settler, emulsion and dispersion regimes. It was concluded that the dispersed-phase holdup was a function of the mean drop diameter and dispersed-phase superficial velocity. An increase in the dispersed-phase holdup induced an increase in the interface area in the liquid-liquid system. Knowledge of the value of the dispersed-phase holdup can be used for calculation of the volumetric mass transfer coefficient, one of the important factor in the design of the column extractor. It was concluded that the increase in the dispersed-phase superficial velocity is causing a decrease in axial dispersion. On the other hand, an increase in the continuous-phase superficial velocity is causing the increase in the axial dispersion coefficient. Some of the empirical equations proposed in literature for calculations of the hydrodynamic parameters were presented. These correlations, derived for determination of the hydrodynamic parameters in pulsed sieve-plate extraction columns, can be used for the design of these liquid-liquid extraction columns.

Axial Dispersion in a Three-Phase Gas-Agitated Spray Extraction Column

1998 ◽  
Vol 63 (2) ◽  
pp. 283-292 ◽  
Author(s):  
Milan Sovilj
Keyword(s):  
Gas Phase ◽  
Dispersion Coefficient ◽  
Continuous Phase ◽  
Axial Dispersion ◽  
Superficial Velocity ◽  
Extraction Column ◽  
Dispersed Phase ◽  
Dispersion Coefficients ◽  
Axial Dispersion Coefficient ◽  
Three Phase

The continuous-phase axial dispersion coefficients of the three-phase gas-liquid-liquid system in a gas-agitated spray extraction column 10 cm i.d. at 20 °C were examined. The system used was water as continuous phase, toluene as dispersed phase, and air as gaseous phase. The rise in the gas phase superficial velocity increased the continuous-phase axial dispersion coefficient. A non-linear dependence between the continuous-phase axial dispersion coefficient and the continuous phase superficial velocity was observed. No correlation was found between the continuous-phase axial dispersion coefficient and dispersed phase superficial velocity. The increase in the gas phase hold-up corresponded to a slight increase in the continuous-phase axial dispersion coefficient. The increase in the dispersed phase hold-up generated a growth of the continuous-phase axial dispersion coefficient. A comparison was made of the continuous-phase axial dispersion coefficients of the three-phase (air-water-toluene) and two-phase (water-toluene) systems.

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