scholarly journals Importance of Microstructural Analysis in Experimental Soil Stabilization

2020 ◽  
Vol 4 (5) ◽  
Author(s):  
Amin Chegenizadeh
2021 ◽  
Vol 11 (8) ◽  
pp. 3572
Author(s):  
Isam Adnan Khasib ◽  
Nik Norsyahariati Nik Daud ◽  
Noor Azline Mohd Nasir

Using geopolymer in soil stabilization has gained much attention recently due to its efficiency in improving soil properties and being environmentally friendly at the same time. This research aims to investigate the effect of palm oil fuel ash (POFA)-based geopolymer on soft soil stabilization. The mechanical and microstructural performance of two types of clay soil treated with geopolymer produce from POFA material was the focus of this study. In this respect, a series of unconfined compression and direct shear tests were conducted to investigate the mechanical properties of soils treated with POFA-based geopolymer. Furthermore, the microstructural changes in the treated samples were analyzed using field emission electron microscopy (FESEM) and energy dispersive X-ray (EDX). In accordance with the results, it was indicated that the shear strength of both soils soared by increasing the dosage of POFA-based geopolymer. Geopolymer with 40% POFA of the dry weight of soils yielded the highest UCS value at both curing periods, 7 and 28 days. Furthermore, the microstructural analysis revealed material modifications (N-A-S-H gel formation) related to strength enhancement. These results suggest the potentiality of using a POFA-based geopolymer binder to stabilize soft soil.


Author(s):  
C. M. Jantzen ◽  
D. G. Howitt

The mullite-SiO2 liquidus has been extensively studied, and it has been shown that the flattening of the liquidus is related to the existence of a metastable region of liquid immiscibility at sub-liquidus temperatures which is detectable by transmission electron microscopy (TEM) (Fig. 1).


Author(s):  
R.T. Blackham ◽  
J.J. Haugh ◽  
C.W. Hughes ◽  
M.G. Burke

Essential to the characterization of materials using analytical electron microscopy (AEM) techniques is the specimen itself. Without suitable samples, detailed microstructural analysis is not possible. Ultramicrotomy, or diamond knife sectioning, is a well-known mechanical specimen preparation technique which has been gaining attention in the materials science area. Malis and co-workers and Glanvill have demonstrated the usefulness and applicability of this technique to the study of a wide variety of materials including Al alloys, composites, and semiconductors. Ultramicrotomed specimens have uniform thickness with relatively large electron-transparent areas which are suitable for AEM anaysis.Interface Analysis in Type 316 Austenitic Stainless Steel: STEM-EDS microanalysis of grain boundaries in austenitic stainless steels provides important information concerning the development of Cr-depleted zones which accompany M23C6 precipitation, and documentation of radiation induced segregation (RIS). Conventional methods of TEM sample preparation are suitable for the evaluation of thermally induced segregation, but neutron irradiated samples present a variety of problems in both the preparation and in the AEM analysis, in addition to the handling hazard.


2013 ◽  
Vol 51 (6) ◽  
pp. 429-436 ◽  
Author(s):  
Jeong Eun Chae ◽  
Jun-Mo Yang ◽  
Kyung Jin Park ◽  
Jung Ho Yoo ◽  
Yun Chang Park ◽  
...  

2015 ◽  
Vol 10 (2) ◽  
pp. 2663-2681
Author(s):  
Rizk El- Sayed ◽  
Mustafa Kamal ◽  
Abu-Bakr El-Bediwi ◽  
Qutaiba Rasheed Solaiman

The structure of a series of AlSb alloys prepared by melt spinning have been studied in the as melt–spun ribbons  as a function of antimony content .The stability  of these structures has  been  related to that of the transport and mechanical properties of the alloy ribbons. Microstructural analysis was performed and it was found that only Al and AlSb phases formed for different composition.  The electrical, thermal and the stability of the mechanical properties are related indirectly through the influence of the antimony content. The results are interpreted in terms of the phase change occurring to alloy system. Electrical resistivity, thermal conductivity, elastic moduli and the values of microhardness are found to be more sensitive than the internal friction to the phase changes. 


Author(s):  
V.K. Ignatjev ◽  
◽  
D.A. Kozin ◽  
D.A. Stankevich ◽  
A.A. Orlov ◽  
...  

Author(s):  
SAMUEL BRITO ◽  
RODOLFO SOBRAL ◽  
Luiz Carlos Sacramento ◽  
Marcos Paulo de Souza Junior

2020 ◽  
Vol 86 (1) ◽  
pp. 32-37
Author(s):  
Valeria A. Brodskaya ◽  
Oksana A. Molkova ◽  
Kira B. Zhogova ◽  
Inga V. Astakhova

Powder materials are widely used in the manufacture of electrochemical elements of thermal chemical sources of current. Electrochemical behavior of the powders depends on the shape and size of their particles. The results of the study of the microstructure and particles of the powders of vanadium (III), (V) oxides and lithium aluminate obtained by transmission electron and atomic force microscopy, X-ray diffraction and gas adsorption analyses are presented. It is found that the sizes of vanadium (III) and vanadium (V) oxide particles range within 70 – 600 and 40 – 350 nm, respectively. The size of the coherent-scattering regions of the vanadium oxide particles lies in the lower range limit which can be attributed to small size of the structural elements (crystallites). An average volumetric-surface diameter calculated on the basis of the surface specific area is close to the upper range limit which can be explained by the partial agglomeration of the powder particles. Unlike the vanadium oxide particles, the range of the particle size distribution of the lithium aluminate powder is narrower — 50 – 110 nm. The values of crystallite sizes are close to the maximum of the particle size distribution. Microstructural analysis showed that the particles in the samples of vanadium oxides have a rounded (V2O3) or elongated (V2O5) shape; whereas the particles of lithium aluminate powder exhibit lamellar structure. At the same time, for different batches of the same material, the particle size distribution is similar, which indicates the reproducibility of the technologies for their manufacture. The data obtained can be used to control the constancy of the particle size distribution of powder materials.


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