scholarly journals Fractal Characterization of Nanopore Structure in Shale, Tight Sandstone and Mudstone from the Ordos Basin of China Using Nitrogen Adsorption

Energies ◽  
2019 ◽  
Vol 12 (4) ◽  
pp. 583 ◽  
Author(s):  
Xiaohong Li ◽  
Zhiyong Gao ◽  
Siyi Fang ◽  
Chao Ren ◽  
Kun Yang ◽  
...  
Keyword(s):  
Pore Structure ◽  
Pressure Range ◽  
Ordos Basin ◽  
Fractal Dimensions ◽  
Nitrogen Adsorption ◽  
Relative Pressure ◽  
Tight Sandstone ◽  
Porosity And Permeability ◽  
The Ordos Basin ◽  
Nanopore Structure

The characteristics of the nanopore structure in shale, tight sandstone and mudstone from the Ordos Basin of China were investigated by X-ray diffraction (XRD) analysis, porosity and permeability tests and low-pressure nitrogen adsorption experiments. Fractal dimensions D1 and D2 were determined from the low relative pressure range (0 < P/P0 < 0.4) and the high relative pressure range (0.4 < P/P0 < 1) of nitrogen adsorption data, respectively, using the Frenkel–Halsey–Hill (FHH) model. Relationships between pore structure parameters, mineral compositions and fractal dimensions were investigated. According to the International Union of Pure and Applied Chemistry (IUPAC) isotherm classification standard, the morphologies of the nitrogen adsorption curves of these 14 samples belong to the H2 and H3 types. Relationships among average pore diameter, Brunner-Emmet-Teller (BET) specific surface area, pore volume, porosity and permeability have been discussed. The heterogeneities of shale nanopore structures were verified, and nanopore size mainly concentrates under 30 nm. The average fractal dimension D1 of all the samples is 2.1187, varying from 1.1755 to 2.6122, and the average fractal dimension D2 is 2.4645, with the range from 2.2144 to 2.7362. Compared with D1, D2 has stronger relationships with pore structure parameters, and can be used for analyzing pore structure characteristics.

scholarly journals Multifractal Characteristics and Classification of Tight Sandstone Reservoirs: A Case Study from the Triassic Yanchang Formation, Ordos Basin, China

Energies ◽  
2018 ◽  
Vol 11 (9) ◽  
pp. 2242 ◽  
Author(s):  
Zhihao Jiang ◽  
Zhiqiang Mao ◽  
Yujiang Shi ◽  
Daxing Wang
Keyword(s):  
Pore Structure ◽  
Ordos Basin ◽  
Type I ◽  
Tight Sandstone ◽  
Throat Radius ◽  
Yanchang Formation ◽  
Porosity And Permeability ◽  
Sandstone Reservoir ◽  
And Migration ◽  
Mercury Injection Capillary Pressure

Pore structure determines the ability of fluid storage and migration in rocks, expressed as porosity and permeability in the macroscopic aspects, and the pore throat radius in the microcosmic aspects. However, complex pore structure and strong heterogeneity make the accurate description of the tight sandstone reservoir of the Triassic Yanchang Formation, Ordos Basin, China still a problem. In this paper, mercury injection capillary pressure (MICP) parameters were applied to characterize the heterogeneity of pore structure, and three types of pore structure were divided, from high to low quality and defined as Type I, Type II and Type III, separately. Then, the multifractal analysis based on the MICP data was conducted to investigate the heterogeneity of the tight sandstone reservoir. The relationships among physical properties, MICP parameters and a series of multifractal parameters have been detailed analyzed. The results showed that four multifractal parameters, singularity exponent parameter (αmin), generalized dimension parameter (Dmax), information dimension (D1), and correlation dimension (D2) were in good correlations with the porosity and permeability, which can well characterize the pore structure and reservoir heterogeneity of the study area, while the others didn’t respond well. Meanwhile, there also were good relationships between these multifractal and MICP parameters.

Micro-Nanopore Structure and Fractal Characteristics of Tight Sandstone Gas Reservoirs in the Eastern Ordos Basin, China

2021 ◽  
Vol 21 (1) ◽  
pp. 234-245
Author(s):  
Peng Qiao ◽  
Yiwen Ju ◽  
Jianchao Cai ◽  
Jun Zhao ◽  
Hongjian Zhu ◽  
...  
Keyword(s):  
Fractal Dimension ◽  
Pore Structure ◽  
Ordos Basin ◽  
Gas Storage ◽  
Main Peak ◽  
Storage Space ◽  
Tight Sandstone ◽  
Fractal Characteristics ◽  
Sandstone Reservoirs ◽  
Nanopore Structure

The complex pore system in tight sandstone reservoirs controls the storage and transport of natural gas. Thus, quantitatively characterizing the micro-nanopore structure of tight sandstone reservoirs is of great significance to determining the accumulation and distribution of tight gas. The pore structure of reservoirs was determined through polarizing microscopy, scanning electron microscopy (SEM), and the combination of mercury injection capillary pressure (MICP) and nuclear magnetic resonance (NMR) experiments on Late Paleozoic conventional and tight sandstone samples from the Linxing Block, Ordos Basin. The results show that in contrast to conventional sandstone, dissolution pores, with diameters less than 8 μm, are the main contributors to the gas storage space of tight sandstone reservoirs. The pore size distribution derived from the MICP experiment demonstrates that the main peak of tight sandstones corresponds to a pore radius in the range of 247 nm to 371 nm, while the secondary peak usually corresponds to 18 nm. The results of the NMR test illustrate that the T2 spectra of tight sandstones are unimodal, bimodal and multimodal, and the main NMR peak is highly related to the MICP peak. Fractal theory was proposed to quantitatively characterize the complex pore structure and rough porous surface. The sandstones show fractal characteristics including nanopore fractal dimension DN obtained from the MICP and large pore fractal dimension DL obtained from the NMR experiment. Both DN and DL are positively correlated with porosity and negatively correlated with permeability, demonstrating that complex and heterogeneous pore structure could increase the gas storage space and reduce the connectivity.

Establishment of Models for Tight Sandstone Formation Evaluation in the Ordos Basin of Northwest China

2014 ◽  
Vol 989-994 ◽  
pp. 1372-1375 ◽  
Author(s):  
Xiao Lei Wei ◽  
Jun Li ◽  
Rui Xu ◽  
Ling Ling Zhi
Keyword(s):  
Ordos Basin ◽  
Northwest China ◽  
Tight Sandstone ◽  
Reserve Estimation ◽  
Formation Evaluation ◽  
Porosity And Permeability ◽  
Important Input ◽  
The Ordos Basin ◽  
Sandstone Formation ◽  
Relative Errors

Porosity and permeability are two important input parameters in formation evaluation. However, It faces a great challenge for formation porosity and permeability estimation in tight sandstone reservoirs in the Ordos basin of northwest China due to the greater contribution of rock matrix and complicated pore structure. In this paper, based on the analysis of conventional log responses and 324 core samples drilled from the target formations in different wells, the estimation models of reservoir porosity and permeability are established, and the reliability of these models are verified by comparing the calculated porosity and permeability by using the established models with core analyzed results. The absolute errors between these two kinds of porosities are all lower than 0.64%, and the relative errors between them are lower than 7.1%, these are coincided with the requirement of reserve estimation.

scholarly journals An Investigation of Fractal Characteristics of Marine Shales in the Southern China from Nitrogen Adsorption Data

2015 ◽  
Vol 2015 ◽  
pp. 1-12 ◽  
Author(s):  
Jian Xiong ◽  
Xiangjun Liu ◽  
Lixi Liang
Keyword(s):  
Fractal Dimension ◽  
Pore Structure ◽  
Southern China ◽  
Fractal Dimensions ◽  
Nitrogen Adsorption ◽  
Mean Value ◽  
Relative Pressure ◽  
Pore Surface ◽  
Adsorption Sites ◽  
Fractal Characteristics

We mainly focus on the Permian, Lower Cambrian, Lower Silurian, and Upper Ordovician Formation; the fractal dimensions of marine shales in southern China were calculated using the FHH fractal model based on the low-pressure nitrogen adsorption analysis. The results show that the marine shales in southern China have the dual fractal characteristics. The fractal dimensionD1at low relative pressure represents the pore surface fractal characteristics, whereas the fractal dimensionD2at higher relative pressure describes the pore structure fractal characteristics. The fractal dimensionsD1range from 2.0918 to 2.718 with a mean value of 2.4762, and the fractal dimensionsD2range from 2.5842 to 2.9399 with a mean value of 2.8015. There are positive relationships between fractal dimensionD1and specific surface area and total pore volume, whereas the fractal dimensionsD2have negative correlation with average pore size. The larger the value of the fractal dimensionD1is, the rougher the pore surface is, which could provide more adsorption sites, leading to higher adsorption capacity for gas. The larger the value of the fractal dimensionD2is, the more complicated the pore structure is, resulting in the lower flow capacity for gas.

Pore structure and its fractal dimensions of transitional shale: A cross-section from east margin of the Ordos Basin, China

Fuel ◽  
2019 ◽  
Vol 241 ◽  
pp. 417-431 ◽  
Author(s):  
Yong Li ◽  
Zhuangsen Wang ◽  
Zhejun Pan ◽  
Xinlei Niu ◽  
Yun Yu ◽  
...  
Keyword(s):  
Pore Structure ◽  
Cross Section ◽  
Ordos Basin ◽  
Fractal Dimensions ◽  
The Ordos Basin

PORE STRUCTURE OF TRANSITIONAL SHALES IN THE ORDOS BASIN, NW CHINA: EFFECTS OF COMPOSITION ON GAS STORAGE MECHANISM

2017 ◽  
Author(s):  
Fengyang Xiong ◽  
◽  
Zhenxue Jiang ◽  
Mohammad Amin Amooie ◽  
Mohamad Reza Soltanian ◽  
...  
Keyword(s):  
Pore Structure ◽  
Ordos Basin ◽  
Gas Storage ◽  
Nw China ◽  
Storage Mechanism ◽  
The Ordos Basin

scholarly journals Nanometer Pore Structure Characterization of Taiyuan Formation Shale in the Lin-Xing Area Based on Nitrogen Adsorption Experiments

Minerals ◽  
2021 ◽  
Vol 11 (3) ◽  
pp. 298
Author(s):  
Chenlong Ding ◽  
Jinxian He ◽  
Hongchen Wu ◽  
Xiaoli Zhang
Keyword(s):  
Specific Surface ◽  
Pore Structure ◽  
Surface Area ◽  
Specific Surface Area ◽  
Shale Gas ◽  
Pore Volume ◽  
Ordos Basin ◽  
Total Pore Volume ◽  
Nitrogen Adsorption ◽  
Taiyuan Formation

Ordos Basin is an important continental shale gas exploration site in China. The micropore structure of the shale reservoir is of great importance for shale gas evaluation. The Taiyuan Formation of the lower Permian is the main exploration interval for this area. To examine the nanometer pore structures in the Taiyuan Formation shale reservoirs in the Lin-Xing area, Northern Shaanxi, the microscopic pore structure characteristics were analyzed via nitrogen adsorption experiments. The pore structure parameters, such as specific surface area, pore volume, and aperture distribution, of shale were calculated; the significance of the pore structure for shale gas storage was analyzed; and the main controlling factors of pore development were assessed. The results indicated the surface area and hole volume of the shale sample to be 0.141–2.188 m2/g and 0.001398–0.008718 cm3/g, respectively. According to the IUPAC (International Union of Pure and Applied Chemistry) classification, mesopores and macropores were dominant in the pore structure, with the presence of a certain number of micropores. The adsorption curves were similar to the standard IV (a)-type isotherm line, and the hysteresis loop type was mainly similar to H3 and H4 types, indicating that most pores are dominated by open type pores, such as parallel plate-shaped pores and wedge-shaped slit pores. The micropores and mesopores provide the vast majority of the specific surface area, functioning as the main area for the adsorption of gas in the shale. The mesopores and macropores provide the vast majority of the pore volume, functioning as the main storage areas for the gas in the shale. Total organic carbon had no notable linear correlation with the total pore volume and the specific surface area. Vitrinite reflectance (Ro) had no notable correlation with the specific surface area, but did have a low “U” curve correlation with the total pore volume. There was no relationship between the quartz content and specific surface area and total pore volume. In addition, there was no notable correlation between the clay mineral content and total specific surface area and total pore volume.

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