scholarly journals The Effect of Predeformation on Creep Strength of 9% Cr Steel

Materials ◽  
2020 ◽  
Vol 13 (23) ◽  
pp. 5330
Author(s):  
Petr Král ◽  
Jiří Dvořák ◽  
Wolfgang Blum ◽  
Václav Sklenička ◽  
Zenji Horita ◽  
...  
Keyword(s):  
Plastic Deformation ◽  
High Pressure ◽  
Severe Plastic Deformation ◽  
Grain Boundaries ◽  
High Pressure Torsion ◽  
Tensile Creep ◽  
Initial Stresses ◽  
High Angle ◽  
Creep Tests ◽  
P92 Steel

Martensitic creep-resistant P92 steel was deformed by different methods of severe plastic deformation such as rotation swaging, high-pressure sliding, and high-pressure torsion at room temperature. These methods imposed significantly different equivalent plastic strains of about 1–30. It was found that rotation swaging led to formation of heterogeneous microstructures with elongated grains where low-angle grain boundaries predominated. Other methods led to formation of ultrafine-grained (UFG) microstructures with high frequency of high-angle grain boundaries. Constant load tensile creep tests at 873 K and initial stresses in the range of 50 to 300 MPa revealed that the specimens processed by rotation swaging exhibited one order of magnitude lower minimum creep rate compared to standard P92 steel. By contrast, UFG P92 steel is significantly softer than standard P92 steel, but differences in their strengths decrease with increasing stress. Microstructural results suggest that creep behavior of P92 steel processed by severe plastic deformation is influenced by the frequency of high-angle grain boundaries and grain coarsening during creep.

Structure and Properties of Grain Boundaries in Submicrocrystalline W Obtained by Severe Plastic Deformation

2009 ◽  
Vol 283-286 ◽  
pp. 629-638 ◽  
Author(s):  
Vladimir V. Popov ◽  
Ruslan Valiev ◽  
E.N. Popova ◽  
A.V. Sergeev ◽  
A.V. Stolbovsky ◽  
...  
Keyword(s):  
Thermal Stability ◽  
Plastic Deformation ◽  
High Pressure ◽  
Severe Plastic Deformation ◽  
Grain Boundaries ◽  
High Pressure Torsion ◽  
Submicrocrystalline Structure ◽  
Emission Mössbauer Spectroscopy ◽  
Structure And Properties ◽  
Initial State

Submicrocrystalline structure of W obtained by severe plastic deformation (SPD) by high pressure torsion (5 revolutions of anvils at 4000C) and its thermal stability have been examined by TEM. Grain boundaries of submicrocrystalline W have been studied by the method of the emission Mössbauer spectroscopy in the initial state and after annealing at 400-6000С.

The State of Grain Boundaries and Grain-Boundary Diffusion in Ultrafine-Grained Mo Obtained by Severe Plastic Deformation

2016 ◽  
Vol 367 ◽  
pp. 130-139 ◽  
Author(s):  
Vladimir V. Popov ◽  
A.V. Sergeev
Keyword(s):  
Plastic Deformation ◽  
High Pressure ◽  
Grain Boundary ◽  
Severe Plastic Deformation ◽  
Grain Boundaries ◽  
Boundary Diffusion ◽  
High Pressure Torsion ◽  
Grain Boundary Diffusion ◽  
Fast Diffusion ◽  
Non Equilibrium

The grain-boundary diffusion of Co in ultra-fine grained Mo processed by high-pressure torsion has been studied by emission Mössbauer spectroscopy and radio-tracer analysis. It is demonstrated that under the severe plastic deformation by high-pressure torsion the non-equilibrium grain boundaries are formed which are the ultra-fast diffusion paths. At annealing in the temperature range of 623-823 K the relaxation of the non-equilibrium boundaries proceeds and their properties approach to those of equilibrium boundaries of recrystallization origin.

Resolving the Strength-Ductility Paradox through Severe Plastic Deformation of a Cast Al-7% Si Alloy

2016 ◽  
Vol 879 ◽  
pp. 1043-1048
Author(s):  
Praveen Kumar ◽  
Megumi Kawasaki ◽  
Terence G. Langdon
Keyword(s):  
Plastic Deformation ◽  
Severe Plastic Deformation ◽  
Grain Boundaries ◽  
Room Temperature ◽  
High Pressure Torsion ◽  
High Energy ◽  
Grain Boundary Sliding ◽  
Simultaneous Increase ◽  
High Angle ◽  
Strength And Ductility

Ultrafine-grained (UFG) materials produced by severe plastic deformation (SPD) may show both enhanced ductility and strength and hence resolve the so-called strength-ductility paradox. To gain mechanistic insights into such resolution, the effect of high-pressure torsion (HPT) on the microstructure and mechanical behavior was studied using a cast Al-7 wt. % Si alloy. As expected, the grain size decreased while the fraction of high-angle grain boundaries and microhardness increased due to HPT processing. However, tensile testing at room temperature revealed a simultaneous increase in strength and ductility compared to the as-cast sample. The samples showing simultaneous increase in strength and ductility also showed an increased contribution from grain boundary sliding (GBS), even at room temperature, which is attributed to the existence of a high fraction of high-angle and high-energy grain boundaries. It is proposed that the occurrence of moderate GBS, providing ductility, in very small size grains provides Hall-Petch strengthening and this suggests a potential combination for simultaneously achieving high strength and high ductility in SPD-processed UFG materials.

Structure, Thermal Stability and Properties of Grain Boundaries of Submicrocrystalline Mo Obtained by Severe Plastic Deformation

2012 ◽  
Vol 326-328 ◽  
pp. 674-681 ◽  
Author(s):  
Vladimir V. Popov ◽  
Galina P. Grabovetskaya ◽  
A.V. Sergeev ◽  
I.P. Mishin
Keyword(s):  
Electron Microscopy ◽  
Thermal Stability ◽  
Transmission Electron Microscopy ◽  
Plastic Deformation ◽  
High Pressure ◽  
Severe Plastic Deformation ◽  
Grain Boundaries ◽  
High Pressure Torsion ◽  
Emission Mössbauer Spectroscopy ◽  
Transmission Electron

The structure of submicrocrystalline Mo, obtained by high pressure torsion, its thermal stability and the state of grain boundaries have been studied by transmission electron microscopy and emission Mössbauer spectroscopy.

scholarly journals Influence of High Pressure Sliding and Rotary Swaging on Creep Behavior of P92 Steel at 500 °C

Metals ◽  
2021 ◽  
Vol 11 (12) ◽  
pp. 2044
Author(s):  
Petr Kral ◽  
Jiri Dvorak ◽  
Vaclav Sklenicka ◽  
Zenji Horita ◽  
Yoichi Takizawa ◽  
...  
Keyword(s):  
High Pressure ◽  
Creep Resistance ◽  
Equivalent Strain ◽  
Creep Testing ◽  
Tensile Creep ◽  
Initial Stresses ◽  
Coarse Grained ◽  
Creep Tests ◽  
P92 Steel ◽  
Rotary Swaging

High-pressure sliding (HPS) and rotary swaging (RS) at room temperature were used to form severely deformed microstructures in martensitic creep-resistant P92 steel. The deformed microstructures contained markedly different ratios of low- and high-angle grain boundaries (LAGBs/HAGBs). The application of the RS method, with an imposed equivalent strain of 1.4, led to the formation of a heterogeneous microstructure with a high number of LAGBs, while the HPS method, with an imposed equivalent strain of 7.8, led to the formation of a relatively homogeneous ultrafine-grained microstructure with a significant predominance of HAGBs. Microstructure analyses after creep testing showed that the microstructure of RS- and HPS-processed P92 steel is quite stable, but a slight coarsening of subgrains and grains during creep testing can be observed. Constant load tensile creep tests at 500 °C and initial stresses ranging from 300 to 900 MPa revealed that the specimens processed by HPS exhibited higher creep strength (slower minimum creep rate) and ductility compared to the coarse-grained and RS-processed P92 steel. However, the HPS-processed P92 steel also exhibited lower values of stress exponent n than the other investigated states of P92 steel. For this reason, the differences in minimum creep rates determined for different states decrease with decreasing values of applied stress, and at applied stresses lower than 500 MPa, the creep resistance of the RS-processed state is higher than the creep resistance of the HPS-processed state.

scholarly journals The Effect of the In-Situ Heat Treatment on the Martensitic Transformation and Specific Properties of the Fe-Mn-Si-Cr Shape Memory Alloys Processed by HSHPT Severe Plastic Deformation

Materials ◽  
2021 ◽  
Vol 14 (16) ◽  
pp. 4621
Author(s):  
Carmela Gurau ◽  
Gheorghe Gurau ◽  
Felicia Tolea ◽  
Bogdan Popescu ◽  
Mihaela Banu ◽  
...  
Keyword(s):  
Plastic Deformation ◽  
High Pressure ◽  
Severe Plastic Deformation ◽  
High Speed ◽  
High Pressure Torsion ◽  
Electron Interaction ◽  
Sudden Increase ◽  
Neel Temperature ◽  
Néel Temperature

This work focuses on the temperature evolution of the martensitic phase ε (hexagonal close packed) induced by the severe plastic deformation via High Speed High Pressure Torsion method in Fe57Mn27Si11Cr5 (at %) alloy. The iron rich alloy crystalline structure, magnetic and transport properties were investigated on samples subjected to room temperature High Speed High Pressure Torsion incorporating 1.86 degree of deformation and also hot-compression. Thermo-resistivity as well as thermomagnetic measurements indicate an antiferromagnetic behavior with the Néel temperature (TN) around 244 K, directly related to the austenitic γ-phase. The sudden increase of the resistivity on cooling below the Néel temperature can be explained by an increased phonon-electron interaction. In-situ magnetic and electric transport measurements up to 900 K are equivalent to thermal treatments and lead to the appearance of the bcc-ferrite-like type phase, to the detriment of the ε(hcp) martensite and the γ (fcc) austenite phases.

Reversible Martensitic Transformation Produced by Severe Plastic Deformation of Metastable Austenitic Steel

2013 ◽  
Vol 738-739 ◽  
pp. 491-495 ◽  
Author(s):  
Igor Litovchenko ◽  
Alexander Tyumentsev ◽  
Alexander V. Korznikov
Keyword(s):  
Plastic Deformation ◽  
High Pressure ◽  
Martensitic Transformation ◽  
Severe Plastic Deformation ◽  
Dynamic Recrystallization ◽  
Austenitic Steel ◽  
High Pressure Torsion ◽  
Martensitic Transformations ◽  
Metastable Austenitic Steel ◽  
Nanostructured States

The peculiarities of martensitic transformations and formation of nanostructured states in metastable austenitic steel (Fe-18Cr-8Ni-Ti) after severe plastic deformation by high pressure torsion are investigated. It is shown that during severe plastic deformation with increased strain rate not only direct (γ→α΄) but also reverse (α΄→γ) martensitic transformations occur, which is revealed by the changes in the volume content of α΄ - martensite during deformation. The fragments thought to be formed by direct and reverse martensitic transformations and those of dynamic recrystallization of austenite are observed.

Mechanism of activation of TiFe intermetallics for hydrogen storage by severe plastic deformation using high-pressure torsion

2013 ◽  
Vol 103 (14) ◽  
pp. 143902 ◽  
Author(s):  
Kaveh Edalati ◽  
Junko Matsuda ◽  
Makoto Arita ◽  
Takeshi Daio ◽  
Etsuo Akiba ◽  
...  
Keyword(s):  
Plastic Deformation ◽  
High Pressure ◽  
Severe Plastic Deformation ◽  
Hydrogen Storage ◽  
High Pressure Torsion
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