scholarly journals Experimental Investigation of Mechanical Properties of Black Shales after CO2-Water-Rock Interaction

Materials ◽  
2016 ◽  
Vol 9 (8) ◽  
pp. 663 ◽  
Author(s):  
Qiao Lyu ◽  
Pathegama Ranjith ◽  
Xinping Long ◽  
Bin Ji
Author(s):  
Qiao Lyu ◽  
P.G. Ranjith ◽  
Xinping Long ◽  
Bin Ji

The effects of CO2-water-rock interactions on the mechanical properties of shale are essential for estimating the possibility of sequestrating CO2 in shale reservoirs. In this study, uniaxial compressive strength (UCS) tests together with an acoustic emission (AE) system and SEM & EDS analysis were performed to investigate the mechanical properties and microstructural changes of black shales with different saturation times (10 days, 20 days and 30 days) in water dissoluted with sub-/super-critical CO2. According to the experimental results, the values of UCS, Young’s modulus and brittleness index decrease gradually with increasing saturation time in water with sub-/super-critical CO2. Compared to intact samples, 30-days’ saturation causes reductions of 56.43% in UCS and 54.21% in Young’s modulus for sub-critical saturated samples, and 66.05% in UCS and 56.32% in Young’s modulus for super-critical saturated samples, respectively. The brittleness index also decreases drastically from 84.3% for intact samples to 50.9% for samples saturated in water with sub-critical CO2, to 47.9% for samples saturated in water with super-critical carbon dioxide (SC-CO2). SC-CO2 causes a greater reduction of shale’s mechanical properties. The crack propagation results obtained from the AE system show that longer saturation time produces higher peak cumulative AE energy. SEM images show that many pores occur when shale samples are saturated in water with sub-/super-critical CO2. The EDS results show that CO2-water-rock interactions increase the percentages of C and Fe and decrease the percentages of Al and K on the surface of saturated samples when compared to intact samples.


Processes ◽  
2018 ◽  
Vol 6 (10) ◽  
pp. 199 ◽  
Author(s):  
Xiaojie Yang ◽  
Jiamin Wang ◽  
Dinggui Hou ◽  
Chun Zhu ◽  
Manchao He

Taking Nanfen open-pit iron mine in Liaoning Province as the engineering background, this study analyzes the effect of water-rock circulation on the mechanical properties of rock through a combination of macro-mechanical experiments and microstructure tests in the laboratory. Uniaxial compression experiments and acoustic wave tests are used to determine the degradation law of the mechanical properties of chlorite under the periodic action of water. The experimental results show that dry-wet cycles have a continuous and gradual effect on the rock sampled: Its uniaxial compressive strength, elastic modulus, and acoustic velocity all decrease gradually with an increase in the number of cycles. After 15 wet-dry cycles, the uniaxial compressive strength and elastic modulus of the rock decreased by 34.21% and 44.63%, respectively. Electron microscope scans of the rock indicate that the particle size, characteristics, and pore distribution at the rock surface had changed significantly after water-rock interaction. Finally, a drainage system and sliding force monitoring devices have been arranged at the mine site that can effectively reduce the impact of water-rock interaction on the stability of the mine. This combination of macro-experiments and micro-analysis allowed the weakening effect of dry-wet cycles on slope rock to be studied quantitatively, providing a theoretical reference for stability evaluation in geotechnical engineering.


2020 ◽  
Vol 2020 ◽  
pp. 1-15 ◽  
Author(s):  
Wen-bo An ◽  
Laigui Wang ◽  
He Chen

Weathering is one of the important geological hazards to many stone cultural relics carved on feldspar sandstone (such as the Datong Yungang Grottoes). To study the mechanical properties of the weathered Yungang Grottoes, feldspar sandstone was subjected to comparative dry-wet cycle tests with water-rock interaction (Group A) and salt-rock interaction (Group B). The variation patterns of the macroscopic physical and mechanical parameters as well as the micro/mesoscopic structures of the two groups of feldspar sandstone with the number of dry-wet cycles were measured. The results showed that for the Group A and Group B sandstones, as the number of dry-wet cycles increased the saturated water absorption and the longitudinal wave velocity increased, with the maximum variation rates reaching 28.02%, 36.98%, 16.20%, and 33.27%. The peak strength and elastic modulus gradually decreased, with the maximum variation rate reaching 48.53%, 73.44%, 26.61%, and 72.39%. The surface height deviation increased by as much as 1.06 μm and 3.34 μm. The mechanism of weathering for the water-rock interaction included three effects, namely, the hydrolysis of the K-Na feldspar, the water swelling of the clay minerals such as kaolinite, and the dissolution of the soluble minerals. The mechanism of weathering for the salt-rock interaction included salt crystallization in the pores or fissures and chemical reactions between the minerals (such as feldspar and calcite) and sulfate, in addition to the above three effects. Therefore, the crystallization stress of the salt exerted the most notable effect on the deterioration of the feldspar sandstone. The results are expected to provide a reference for the stability evaluation and protection of the rock mass of the Grottoes.


2010 ◽  
Vol 7 (2) ◽  
pp. 57
Author(s):  
Jamaludin Kasim ◽  
Shaikh Abdul Karim Yamani ◽  
Ahmad Firdaus Mat Hedzir ◽  
Ahmad Syafiq Badrul Hisham ◽  
Mohd Arif Fikri Mohamad Adnan

An experimental investigation was performed to evaluate the properties of cement-bonded particleboard made from Sesendok wood. The target board density was set at a standard 1200 kg m". The effect offarticle size, wood to cement ratio and the addition ofsodium silicate and aluminium silicate on the wood cement board properties has been evaluated. A change ofparticle size from 1.0 mm to 2.0 mm has a significant effect on the mechanical properties, however the physical properties deteriorate. Increasing the wood to cement ratio from 1:2.25 to 1:3 decreases the modulus ofrupture (MOR) by 11% and the addition ofsodium silicate improves valuesfurther by about 28% compared to the addition ofaluminum silicate. The modulus ofelasticity (MOE) in general increases with increasing cement content, but is not significantly affected by the addition ofsodium silicate or aluminium silicate, although the addition of their mixture (sodium silicate andaluminium silicate) consistentlyyields greater MOE values. Water absorption and thickness swelling is significantly affected by the inclusion ofadditives and better values are attained using higher wood to cement ratios.


2020 ◽  
Author(s):  
Marie Haut-Labourdette ◽  
◽  
Daniele Pinti ◽  
André Poirier ◽  
Marion Saby ◽  
...  

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