scholarly journals AFM Analysis of Micron and Sub-Micron Sized Bridges Fabricated Using the Femtosecond Laser on YBCO Thin Films

Micromachines ◽  
2020 ◽  
Vol 11 (12) ◽  
pp. 1088
Author(s):  
Patrice Umenne
Keyword(s):  
Femtosecond Laser ◽  
Focal Length ◽  
Laser Technique ◽  
Atomic Force ◽  
Convex Lens ◽  
Barium Copper ◽  
Translation Stage ◽  
Afm Analysis ◽  
G Code ◽  
Yttrium Barium

The research arose as a result of the need to use the femtosecond laser to fabricate sub-micron and nano-sized bridges that could be analyzed for the Josephson effect. The femtosecond laser has a low pulse duration of 130 femtoseconds. Hence in an optical setup it was assumed that it could prevent the thermal degradation of the superconductive material during fabrication. In this paper a series of micron and sub-micron sized bridges where fabricated on superconductive yttrium barium copper oxide (YBCO) thin film using the femtosecond laser, a spherical convex lens of focal length 30 mm and the G-code control programming language applied to a translation stage. The dimensions of the bridges fabricated where analyzed using the atomic force microscope (AFM). As a result, micron sized superconductive bridges of width 1.68 μm, 1.39 μm, 1.23 μm and sub-micron sized bridges of width 858 nm, 732 nm where fabricated. The length of this bridges ranged from 9.6 μm to 12.8 μm. The femtosecond laser technique and the spherical convex lens can be used to fabricate bridges in the sub-micron dimension.

Nanofluidic capillaries produced via femtosecond laser induced delamination of thin thermal oxide films from Si(100) substrates

2005 ◽  
Vol 901 ◽  
Author(s):  
Joel Patrick McDonald ◽  
Vanita R. Mistry ◽  
Katherine E. Ray ◽  
Steven M. Yalisove
Keyword(s):  
Femtosecond Laser ◽  
Oxide Films ◽  
Laser Pulses ◽  
Femtosecond Laser Pulses ◽  
Force Microscopy ◽  
Automated Translation ◽  
Atomic Force ◽  
Integrated Devices ◽  
Thermal Oxide ◽  
Translation Stage

AbstractHighly selective and repeatable delamination of thermal oxide films from Si(100) substrates has been performed using single and multiple femtosecond laser pulses forming bubbles or blisters. By overlapping the bubbles laterally, tubes or capillaries can be formed with a range of volumes suitable for nanofluidics. By scanning the sample through the laser using an automated translation stage, patterns of tubes with arbitrary complexity can be formed, while the scan velocity can easily control the volume of the tubes. The production time for capillaries in this fashion is considerably less than with other lithographic techniques, while the proximity of the tubes to the underlying silicon substrate yields the possibility for integrated devices. The mechanism responsible for the delamination will be discussed and the optimal laser and sample translation conditions will be presented which provide the most uniform tubes. Atomic force microscopy and optical microscopy of capillaries with a range of volumes will be presented.

scholarly journals Back to Nature: Combating Candida albicans Biofilm, Phospholipase and Hemolysin Using Plant Essential Oils

Antibiotics ◽  
2021 ◽  
Vol 10 (1) ◽  
pp. 81
Author(s):  
Ahmed M. El-Baz ◽  
Rasha A. Mosbah ◽  
Reham M. Goda ◽  
Basem Mansour ◽  
Taranum Sultana ◽  
...  
Keyword(s):  
Candida Albicans ◽  
Essential Oils ◽  
Docking Study ◽  
New Drugs ◽  
Molecular Docking Study ◽  
Plant Essential Oils ◽  
Force Microscopy ◽  
Atomic Force ◽  
Afm Analysis ◽  
Phenotypic Methods

Candida albicans is the causative agent of fatal systemic candidiasis. Due to limitations of antifungals, new drugs are needed. The anti-virulence effect of plant essential oils (EOs) was evaluated against clinical C. albicans isolates including cinnamon, clove, jasmine and rosemary oils. Biofilm, phospholipase and hemolysin were assessed phenotypically. EOs were evaluated for their anti-virulence activity using phenotypic methods as well as scanning electron microscopy (SEM) and atomic force microscopy (AFM). Among the C. albicans isolates, biofilm, phospholipase and hemolysins were detected in 40.4, 86.5 and 78.8% of isolates, respectively. Jasmine oil showed the highest anti-biofilm activity followed by cinnamon, clove and rosemary oils. SEM and AFM analysis showed reduced adherence and roughness in the presence of EOs. For phospholipase, rosemary oil was the most inhibitory, followed by jasmine, cinnamon and clove oils, and for hemolysins, cinnamon had the highest inhibition followed by jasmine, rosemary and clove oils. A molecular docking study revealed major EO constituents as promising inhibitors of the Als3 adhesive protein, with the highest binding for eugenol, followed by 1,8-cineole, 2-phenylthiolane and cinnamaldehyde. In conclusion, EOs have a promising inhibitory impact on Candida biofilm, phospholipase and hemolysin production, hence EOs could be used as potential antifungals that impact virulence factors.

DIRECT GROWTH OF EPITAXIAL La0.67Ca0.33MnO3 - δ THIN FILMS

2002 ◽  
Vol 09 (05n06) ◽  
pp. 1611-1615 ◽  
Author(s):  
G. CAMPILLO ◽  
L. F. CASTRO ◽  
P. VIVAS ◽  
E. BACA ◽  
P. PRIETO ◽  
...  
Keyword(s):  
Thin Films ◽  
Substrate Surface ◽  
Electrical Characterization ◽  
Annealing Treatment ◽  
Pure Oxygen ◽  
X Ray Diffraction ◽  
Atomic Force ◽  
Transmission Electron ◽  
Afm Analysis ◽  
Direct Growth

La 0.67 Ca 0.33 MnO 3 - δ thin films were deposited using a high-pressure dc-sputtering process. Pure oxygen at a pressure of 3.8 mbar was used as sputtering gas. The films were grown on (001) LaAlO 3 and (001) SrTiO 3 substrates at heater temperature of 850° without any annealing treatment. The formation of highly a-axis-oriented films with sharp interface with substrate surface is demonstrated by X-ray diffraction, transmission electron microscope (TEM), and atomic force microscope (AFM) analysis. Electrical characterization revealed a metal–insulator transition at T MI = 276 K, and magnetic characterization showed good magnetic properties with a PM–FM transition at TC ≈ 262 K.

Pulsed Microwave Processing of High-TC Superconducting Films

1992 ◽  
Vol 269 ◽  
Author(s):  
R. B. James ◽  
R. A. Alvarez ◽  
A. K. Stamper ◽  
X. J. Bao ◽  
T. E. Schlesinger ◽  
...  
Keyword(s):  
Phase Transition ◽  
Barium Copper Oxide ◽  
Precursor Film ◽  
Silicon Substrates ◽  
Molten Layer ◽  
Time Resolved ◽  
Barium Copper ◽  
In Situ Experiments ◽  
Yttrium Barium

ABSTRACTWe have used 2.0-μsec microwave pulses at a frequency of 2.856 GHz to rapidly heat thin amorphous yttrium-barium-copper-oxide (YBCO) films deposited onto silicon substrates. The samples were irradiated inside a WR-284 waveguide by single-pass TE10 pulses in a traveling wave geometry. X-ray diffractometry studies show that an amorphous-to-crystalline phase transition occurs for incident pulse powers exceeding about 6 MW, in which case the amorphous YBCO layer is converted to Y2BaCuO5. Microscopy of the irradiated film reveals that the phase transition is brought about by melting of the YBCO precursor film and crystallization of the molten layer upon solidification. Time-resolved in situ experiments of the microwave reflectivity (R) and transmissivity (T) show that there is an abrupt change in R for microwave pulse powers exceeding the melt threshold, so that measurements of R and T can be used to monitor the onset of surface melting.

Coupling In-Situ Techniques to Analyze Zinc Deposition and Dissolution for Energy Storage Applications

2013 ◽  
Vol 1491 ◽  
Author(s):  
Jayme Keist ◽  
Christine Orme ◽  
Frances Ross ◽  
Dan Steingart ◽  
Paul Wright ◽  
...  
Keyword(s):  
Liquid Electrolyte ◽  
Scattering Data ◽  
Zinc Deposition ◽  
Ionic Liquid Electrolyte ◽  
Force Microscopy ◽  
In Situ Techniques ◽  
X Ray Scattering ◽  
Atomic Force ◽  
Afm Analysis

ABSTRACTThis investigation describes preliminary results of in-situ analysis of zinc deposition within an ionic liquid electrolyte utilizing electrochemical atomic force microscopy (EC AFM). From the AFM analysis, the morphology of the zinc deposition was analyzed by quantifying the surface roughness using height-height correlation functions. These results will be used to analyze the scattering data obtained from zinc deposition analysis utilizing an electrochemical ultra-small angle x-ray scattering (EC USAXS). The goal of this research is to link the early nucleation and growth behavior to the formation of detrimental morphologies.

Superconducting Yttrium Barium Copper Oxide Thin Films Growing on the Strained Substrates

2008 ◽  
Vol 3 (4) ◽  
pp. 25-32
Author(s):  
Aleksandr V. Zakharov ◽  
Aleksandr B. Muravjev ◽  
Irina S. Pozygun ◽  
Gennadiy M. Seropyan ◽  
Sergey A. Sychev ◽  
...  
Keyword(s):  
Thin Films ◽  
Current Density ◽  
Superconducting Devices ◽  
Single Crystal Substrate ◽  
Superconducting Thin Film ◽  
Elastic Stresses ◽  
Barium Copper ◽  
Crystal Substrate ◽  
Long Time ◽  
Yttrium Barium

The article is devoted to formation of superconducting thin films on the single-crystal substrate where areas with different values of the critical current density are, that is needed for fabrication of superconducting devices. The method is based on an establishment of elastic mechanical stresses on the substrate crystal under the nanosecond focused pulsed laser irradiation. On the irradiated substrate the superconducting thin film having auxiliary elastic stresses not till the area is over the irradiated section of the substrate is grown. At the same time the critical film current density is suppressed for required values are used to fabricate Josephson junctions. Observations for a long time demonstrate superconducting transport film properties are not varied significantly during the maintenance.

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