scholarly journals A One-Pot Synthesis and Characterization of Antibacterial Silver Nanoparticle–Cellulose Film

Polymers ◽  
2020 ◽  
Vol 12 (2) ◽  
pp. 440 ◽  
Author(s):  
Qi-Yuan Chen ◽  
Sheng-Ling Xiao ◽  
Sheldon Q. Shi ◽  
Li-Ping Cai
Keyword(s):  
Composite Film ◽  
Food Packaging ◽  
Antibacterial Activities ◽  
Light Transmittance ◽  
Ag Nps ◽  
One Pot ◽  
One Pot Synthesis ◽  
The One

Using N,N-dimethylacetamide (DMAc) as a reducing agent in the presence of PVP-K30, the stable silver nanoparticles (Ag-NPs) solution was prepared by a convenient method for the in situ reduction of silver nitrate. The cellulose–Ag-NPs composite film (CANF) was cast in the same container using lithium chloride (LiCl) giving the Ag-NPs-PVP/DMAc solution cellulose solubility as well as γ-mercaptopropyltrimethoxysilane (MPTS) to couple Ag-NPs and cellulose. The results showed that the Ag-NPs were uniformly dispersed in solution, and the solution had strong antibacterial activities. It was found that the one-pot synthesis allowed the growth of and cross-linking with cellulose processes of Ag-NPs conducted simultaneously. Approximately 61% of Ag-NPs was successfully loaded in CANF, and Ag-NPs were uniformly dispersed in the surface and internal of the composite film. The composite film exhibited good tensile properties (tensile strength could reach up to 86.4 MPa), transparency (light transmittance exceeds 70%), thermal stability, and remarkable antibacterial activities. The sterilization effect of CANF0.04 against Staphylococcus aureus and Escherichia coli exceed 99.9%. Due to low residual LiCl/DMAc and low diffusion of Ag-NPs, the composite film may have potential for applications in food packaging and bacterial barrier.

scholarly journals Synthesis and morphological characterization of phenyl-modified macroporous–mesoporous hybrid silica monoliths

RSC Advances ◽  
2015 ◽  
Vol 5 (26) ◽  
pp. 20283-20294 ◽  
Author(s):  
Rafael Meinusch ◽  
Kristof Hormann ◽  
Romana Hakim ◽  
Ulrich Tallarek ◽  
Bernd M. Smarsly
Keyword(s):  
Mesoporous Silica ◽  
Morphological Characterization ◽  
Comprehensive Approach ◽  
One Pot ◽  
Silica Monoliths ◽  
One Pot Synthesis ◽  
Hybrid Silica ◽  
The One

We present a comprehensive approach to characterize the one-pot synthesis, macropore space morphology, and chromatographic performance of phenyl-modified macro–mesoporous silica monoliths.

Preparation and characterization of Ca-modified Co/Al2O3 and its catalytic application in the one-pot synthesis of 4H-pyrans

2020 ◽  
Vol 46 (6) ◽  
pp. 3109-3123
Author(s):  
Sakineh Khaledi ◽  
Mahboobe Rajabi ◽  
Ahmad Reza Momeni ◽  
Heshmat Allah Samimi ◽  
Jalal Albadi
Keyword(s):  
One Pot ◽  
One Pot Synthesis ◽  
Catalytic Application ◽  
The One

2-Phenyl-2,3-dihydrobenzo[d]thiazole: A Mild, Efficient, and Highly Active in situ Generated Chemoselective Reducing Agent for the One-Pot Synthesis of 5-Monoalkylbarbiturates in Water

Synlett ◽  
2017 ◽  
Vol 29 (04) ◽  
pp. 477-482 ◽  
Author(s):  
Dibakar Deka ◽  
Subarna Kalita
Keyword(s):  
Reducing Agent ◽  
High Yield ◽  
Purification Process ◽  
Reaction Conditions ◽  
One Pot ◽  
One Pot Synthesis ◽  
Highly Active ◽  
The One ◽  
Operational Simplicity

A metal- and catalyst-free reductive alkylation protocol for the one-pot synthesis of 5-monoalkylbarbiturates from barbituric acids and aldehydes using the in situ generated chemoselective reducing agent 2-phenyl-2,3-dihydrobenzo[d]thiazole from 2-aminothiophenol and benzaldehyde is described. The notable advantages of the protocol are operational simplicity, mild reaction conditions, high yield, short reaction time, and simple workup and purification process which make it highly attractive.

Synthesis and Characterization of Nanocrystalline In2O3 and Its Efficacy as a Catalyst for the One Pot Synthesis of Amidoalkyl Naphthols

2013 ◽  
Vol 43 (4) ◽  
pp. 471-478 ◽  
Author(s):  
Vishvanath D. Patil ◽  
Jyotsna S. Thakur ◽  
Shramesha Mhatre ◽  
Medha Gole ◽  
Aarti Jaiswal
Keyword(s):  
Synthesis And Characterization ◽  
One Pot ◽  
One Pot Synthesis ◽  
Amidoalkyl Naphthols ◽  
The One

Simple and versatile method for the one-pot synthesis of segmented poly(urethane urea)s via in situ -formed AB-type macromonomers

2010 ◽  
Vol 60 (4) ◽  
pp. 620-629 ◽  
Author(s):  
Fatemeh Shokrolahi ◽  
Hamid Yeganeh ◽  
Hamid Mirzadeh
Keyword(s):  
One Pot ◽  
One Pot Synthesis ◽  
The One

The one-pot synthesis of dextran-based nanoparticles and their application in in-situ fabrication of dextran-magnetite nanocomposites

2007 ◽  
Vol 19 (7) ◽  
pp. 2575-2580 ◽  
Author(s):  
Hongjing Dou ◽  
Bin Xu ◽  
Ke Tao ◽  
Minhua Tang ◽  
Kang Sun
Keyword(s):  
One Pot ◽  
One Pot Synthesis ◽  
In Situ Fabrication ◽  
The One

1,3,5-Tris(2-hydroxyethyl)isocyanurate functionalized graphene oxide: a novel and efficient nanocatalyst for the one-pot synthesis of 3,4-dihydropyrimidin-2(1H)-ones

2017 ◽  
Vol 41 (14) ◽  
pp. 6893-6901 ◽  
Author(s):  
Mohammad G. Dekamin ◽  
Fatemeh Mehdipoor ◽  
Amene Yaghoubi
Keyword(s):  
Graphene Oxide ◽  
Biginelli Reaction ◽  
Functionalized Graphene ◽  
One Pot ◽  
Functionalized Graphene Oxide ◽  
One Pot Synthesis ◽  
Catalytic Application ◽  
The One

The preparation and characterization of a novel 1,3,5-tris(2-hydroxyethyl)isocyanurate functionalized graphene oxide (GO–THEIC) nanomaterial and its catalytic application for the Biginelli reaction are described.

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