scholarly journals Preparation Method of Corn Stalk Fiber Material and Its Performance Investigation in Asphalt Concrete

2019 ◽  
Vol 11 (15) ◽  
pp. 4050
Author(s):  
Zining Chen ◽  
Zhiguo Chen ◽  
Junyan Yi ◽  
Decheng Feng

In this study, a bioresource material, corn stalks, were converted by a combination of physical and chemical methods into a corn stalk fiber material that can be utilized in an asphalt pavement. Firstly, corn stalk fiber was produced with different comminution times, mass fractions of sodium hydroxide solution, reaction times, and reaction temperatures. An orthogonal experimental method was employed to determine the optimal production process. The results show that the optimal comminution time was 3.5 min, and corn stalk should be reacted with a sodium hydroxide solution at 80 °C for 30 min to obtain the best corn stalk fiber product. The mass ratios of corn stalk fibers, sodium hydroxide, and water should be 8:1:200. After an evaluation of the physical and mechanical properties of the corn stalk fibers, asphalt binders, and mixtures, it was concluded that this kind of corn stalk fiber can be a good substitute of pavement fiber.

1982 ◽  
Vol 35 (8) ◽  
pp. 1727 ◽  
Author(s):  
J Rosevear ◽  
JFK Wilshire

The sodium salt of 4-amino-3-nitrobenzenesulfonic acid (O-nitroaniline-p-sulfonic acid) has been prepared by the action of dilute sodium hydroxide solution on ethyl [(4-chlorosulfonyl-2-nitro)- phenyllcarbamate. Central to this synthesis is the finding that the N-ethoxycarbonyl group, when located ortho to a nitro group (but not to a bromo group), is readily removed by dilute sodium hydroxide solution.


2015 ◽  
Vol 22 (12) ◽  
pp. 4545-4550 ◽  
Author(s):  
Chong-qing Wang ◽  
Hui Wang ◽  
Guo-hua Gu ◽  
Jian-gang Fu ◽  
You-nian Liu

1997 ◽  
Vol 1997 (Supplement94) ◽  
pp. 217-225
Author(s):  
Tatsuya Fujiyoshi ◽  
Hiroyuki Masuda ◽  
Tokuji Nishinaka ◽  
Tetsuo Futami ◽  
Hiromi Shibuya

Insects ◽  
2021 ◽  
Vol 12 (2) ◽  
pp. 104
Author(s):  
Jennifer Pradelli ◽  
Fabiola Tuccia ◽  
Giorgia Giordani ◽  
Stefano Vanin

Diptera puparia may represent both in forensic and archaeo-funerary contexts the majority of the entomological evidence useful to reconstruct the peri and post-mortem events. Puparia identification is quite difficult due to the lack of identification keys and descriptions. In addition, external substances accumulated during the puparia permanence in the environment make the visualization of the few diagnostic characters difficult, resulting in a wrong identification. Six different techniques based on physical and chemical treatments have been tested for the removal of external substances from puparia to make identification at species level feasible. Furthermore, the effects of these methods on successful molecular analyses have also been tested as molecular identification is becoming an important tool to complement morphological identifications. The results of this study indicate that cleaning via warm water/soap, the sonication and treatment with a sodium hydroxide solution are the best methods to achieve a good quality of the samples.


Author(s):  
Е.П. Викторова ◽  
О.С. Агафонов ◽  
Е.В. Лисовая ◽  
М.Р. Жане ◽  
Т.А. Шахрай ◽  
...  

Разработан метод определения одного из основных физикохимических показателей качества жидких рапсовых лецитинов (РЛ) кислотного числа (КЧ) с применением ядерномагнитной релаксации (ЯМР). В качестве объекта исследований были образцы жидких РЛ с значениями КЧ 19,3 27,8 и 36,5 мг КОН/г, которые использовали для определения оптимального соотношения массовых долей в системе РЛ водный раствор гидроксида натрия концентрацией 1,0 моль/дм3, обеспечивающего полную нейтрализацию свободных жирных кислот и фосфолипидов, проявляющих кислотные свойства. Установлено, что для достижения стабильных результатов измерений аналитического параметра амплитуды сигналов ЯМР протонов мыла, количественно характеризующего содержание свободных жирных кислот и фосфолипидов, необходимыми условиями подготовки пробы жидкого РЛ являются: соотношение массовых долей системы РЛ четыреххлористый углерод 1 : 4 соответственно, системы РЛ раствор гидроксида натрия 1 : 1 соответственно продолжительность перемешивания системы РЛ четыреххлористый углерод раствор гидроксида натрия 2 мин. Выявлена линейная зависимость между КЧ жидких РЛ и амплитудой сигналов ЯМР протонов мыла Ам: КЧ 2,226 0,900Ам. A method for determining one of the main physical and chemical indicators of the quality of liquid rapeseed lecithins (RL) acid number using nuclear magnetic relaxation (NMR) was developed. Samples of the liquid RL with values of acid number 19,3 27,8 and 36,5 mg KOH/g has been the object of research. Samples of liquid RL were used to determine the optimal ratio of mass fractions in the system of RL aqueous solution of sodium hydroxide concentration of 1,0 mol/dm3, providing complete neutralization of free fatty acids and phospholipids exhibiting acidic properties. It was found that to achieve stable results of measurements of the analytical parameter the amplitude of the NMR signals of soap protons, quantitatively characterizing the content of free fatty acids and phospholipids, the preparation of liquid RL samples is necessary: the ratio of the mass fractions of the RL carbon tetrachloride system as 1 : 4, respectively, the RL sodium hydroxide system as 1 : 1, respectively the mixing time of the RL carbon tetrachloride system is 2 min. A linear relationship between acid number fluid RL and the amplitude of the NMR signals of protons of soap As detected: Acid number 2,226 0,900 As


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