Constitutive and Processing Map Analyses of Stainless Steel 316 under Hot Compression

2013 ◽  
Vol 378 ◽  
pp. 178-183
Author(s):  
Chui Hung Chiu ◽  
Horng Yu Wu ◽  
Cheng Tao Wu
Keyword(s):  
Stainless Steel ◽  
Flow Stress ◽  
Constitutive Equation ◽  
Strain Rate ◽  
Power Dissipation ◽  
Hot Deformation ◽  
Processing Map ◽  
Constitutive Law ◽  
Hyperbolic Sine ◽  
Stainless Steel 316

Hot deformation characteristics of stainless steel 316 were investigated at elevated temperatures. Hot compressive tests were carried out in the temperature and strain rate ranges from 800 to 1100 °C and 0.001 to 1 s1, respectively. The flow behaviors showed that the softening mechanisms were related to the dynamic recovery (DRV) and dynamic recrystallization (DRX). The constitutive equation relating flow stress, temperature, and strain rate was obtained based on the peak stress. Constitutive equation was constructed according to the hyperbolic sine constitutive law. The flow stress of stainless steel 316 was fitted well by the constitutive equation of the hyperbolic sine function. The constitutive analysis suggested that the hot deformation mechanism of the stainless steel was dislocation creep. The processing map obtained at a strain of 0.5 exhibited two domains with local maximum efficiency of power dissipation. Variation in efficiency of power dissipation was associated with the variation in ZenerHollomon parameter (Z).

scholarly journals Constitutive Equation and Hot Processing Map of a Nitrogen-Bearing Martensitic Stainless Steel

Metals ◽  
2020 ◽  
Vol 10 (11) ◽  
pp. 1502
Author(s):  
Xiao Li ◽  
Lifeng Hou ◽  
Yinghui Wei ◽  
Zhengyan Wei
Keyword(s):  
Stainless Steel ◽  
Constitutive Equation ◽  
Strain Rate ◽  
Hot Deformation ◽  
Processing Map ◽  
Martensitic Stainless Steel ◽  
True Strain ◽  
True Stress ◽  
Hot Working ◽  
Compression Tests

The hot deformation behavior of a nitrogen-bearing martensitic stainless steel was researched by the isothermal compression test in the temperature range of 950–1150 °C and strain rate range of 0.01–10 s−1 with a Gleeble-3800 thermal-mechanical simulating tester. A strain compensated sine-hyperbolic Arrhenius-type constitutive equation was developed to describe the relationship between true stress and deformation parameters such as temperature, strain rate and true strain. The hot deformation activation energy is calculated to be from 407 to 487 KJ mol−1. It is validated by the standard statistical parameters that the established constitutive equation can accurately predict the true stress. The processing maps at different true strains were constructed based on the dynamic material model (DMM) and the true stress data obtained from the hot compression tests. Two unstable regions which should be avoided during hot working were observed from the processing map. In addition, the optimum hot working parameters are located in the domain of 1000–1150 °C/0.1–1 s−1 with the peak power dissipation efficiency of 39.9%, in which complete dynamic recrystallization (DRX) occurs.

scholarly journals Hot Deformation Characteristics of 18Cr-5Ni-4Cu-N Stainless Steel Using Constitutive Equation and Processing Map

Metals ◽  
2020 ◽  
Vol 10 (1) ◽  
pp. 82
Author(s):  
Xiao-yang Fu ◽  
Pu-cun Bai ◽  
Ji-chun Yang
Keyword(s):  
Electron Microscopy ◽  
Solid Solution ◽  
Stainless Steel ◽  
Constitutive Equation ◽  
Grain Boundary ◽  
Strain Rate ◽  
Hot Deformation ◽  
Processing Map ◽  
Temperature Range ◽  
Calculation Results

The hot deformation of 18Cr-5Ni-4Cu nitrogen-alloyed austenitic stainless steel was tested with a Gleeble-1500D simulator in the temperature range of 1273–1473 K and in the strain rate range of 0.01–10 s−1. The Zener-Hollomon parameter method was used to construct a constitutive equation for high-temperature plastic deformation. The energy dissipation diagram of the material was calculated based on dynamic material modelling (DMM). The microstructural variations were characterized via X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM) with energy dispersive spectroscopy (EDS) and transmission electron microscopy (TEM). The thermodynamic calculation results showed that the addition of nitrogen to 18Cr-5Ni-4Cu steel promoted the formation of Cr2N and gas phases and expanded the austenite phase region; these results were consistent with the XRD test results of the solid solution sample. The hot deformation activation energy after nitrogen addition was 556.46 kJ∙mol−1. The processing map predicted that the optimum hot working regimes were in the temperature range of 1416–1461 K, where ln ε ˙ was 0.75–1 on the power dissipation map. At high temperatures and a small strain rate, dynamic recrystallization easily occurred. The TEM analyses showed that nano-scale M23C6 and Cr2N precipitated at the grain boundary, and NbC with a diameter of approximately 150 nm appeared along the grain boundary, resulting in grain boundary strengthening. The phase precipitation results were consistent with the Thermo-Calc calculation results. The nitrogen solid solution in the steel promoted the precipitation of nitrides, which caused grain boundary strengthening. Thus, the grain boundary stress increased and wedge-shaped grain boundary cracks formed.

scholarly journals Hot Deformation Behavior and Processing Maps of a New Ti-6Al-2Nb-2Zr-0.4B Titanium Alloy

Materials ◽  
2021 ◽  
Vol 14 (9) ◽  
pp. 2456
Author(s):  
Zhijun Yang ◽  
Weixin Yu ◽  
Shaoting Lang ◽  
Junyi Wei ◽  
Guanglong Wang ◽  
...  
Keyword(s):  
Titanium Alloy ◽  
Flow Stress ◽  
Constitutive Equation ◽  
Deformation Mechanism ◽  
Power Dissipation ◽  
Hot Deformation ◽  
Dissipation Rate ◽  
Dynamic Recovery ◽  
Processing Maps ◽  
Temperature Range

The hot deformation behaviors of a new Ti-6Al-2Nb-2Zr-0.4B titanium alloy in the strain rate range 0.01–10.0 s−1 and temperature range 850–1060 °C were evaluated using hot compressing testing on a Gleeble-3800 simulator at 60% of deformation degree. The flow stress characteristics of the alloy were analyzed according to the true stress–strain curve. The constitutive equation was established to describe the change of deformation temperature and flow stress with strain rate. The thermal deformation activation energy Q was equal to 551.7 kJ/mol. The constitutive equation was ε ˙=e54.41[sinh (0.01σ)]2.35exp(−551.7/RT). On the basis of the dynamic material model and the instability criterion, the processing maps were established at the strain of 0.5. The experimental results revealed that in the (α + β) region deformation, the power dissipation rate reached 53% in the range of 0.01–0.05 s−1 and temperature range of 920–980 °C, and the deformation mechanism was dynamic recovery. In the β region deformation, the power dissipation rate reached 48% in the range of 0.01–0.1 s−1 and temperature range of 1010–1040 °C, and the deformation mechanism involved dynamic recovery and dynamic recrystallization.

scholarly journals Hot Deformation Behaviour and Processing Map of Cast Alloy 825

2021 ◽  
Author(s):  
Munir Al-Saadi ◽  
Christopher Hulme-Smith ◽  
Fredrik Sandberg ◽  
Pär G. Jönsson
Keyword(s):  
Strain Rate ◽  
Vickers Hardness ◽  
Power Dissipation ◽  
Hot Deformation ◽  
Processing Map ◽  
Cast Alloy ◽  
True Strain ◽  
Processing Conditions ◽  
Temperature Range ◽  
Power Dissipation Efficiency

AbstractAlloy 825 is a nickel-based alloy that is commonly used in applications where both high strength and corrosion resistance are required, such as tanks in the chemical, food and petrochemical industries and oil and gas pipelines. Components made from Alloy 825 are often manufactured using hot deformation. However, there is no systematic study to optimise the processing conditions reported in literature. In this study, a processing map for as-cast Alloy 825 is established to maximise the power dissipation efficiency of hot deformation in the temperature range of 950 to 1250 °C at an interval of 50 °C and strain rate range of $$0.01\, {\text{s}}^{ - 1}$$ 0.01 s - 1 to $$10.0\, {\text{s}}^{ - 1}$$ 10.0 s - 1 to a true strain of $$0.7$$ 0.7 using a Gleeble-3500 thermomechanical simulator. The processing conditions are also correlated to the Vickers hardness of the final material, which is also characterised using optical microscopy and scanning electron microscopy, including electron backscattered diffraction. The true stress-true strain curves exhibit peak stresses followed by softening due to occurrence of dynamic recrystallization. The activation energy for plastic flow in the temperature range tested is approximately $$450\,{\text{ kJ mol}}^{ - 1}$$ 450 kJ mol - 1 , and the value of the stress exponent in the (hyperbolic sine-based) constitutive equation, $$n = 5.0$$ n = 5.0 , suggests that the rate-limiting mechanism of deformation is dislocation climb. Increasing deformation temperature led to a lower Vickers hardness in the deformed material, due to increased dynamic recrystallization. Raising the strain rate led to an increase in Vickers hardness in the deformed material due to increased work hardening. The maximum power dissipation efficiency is over $$35\%$$ 35 % , obtained for deformation in the temperature range 1100-1250 °C and a strain rate of $$0.01\, {\text{s}}^{ - 1}$$ 0.01 s - 1 -$$0.1\, {\text{s}}^{ - 1}$$ 0.1 s - 1 . These are the optimum conditions for hot working.

A Physically Based Flow Rule for the Simulation of Ti-6Al-4V Forging in the α - β Range

2007 ◽  
Vol 539-543 ◽  
pp. 3661-3666 ◽  
Author(s):  
A. Colin ◽  
Christophe Desrayaud ◽  
Marie Mineur ◽  
Frank Montheillet
Keyword(s):  
Flow Stress ◽  
Constitutive Equation ◽  
Strain Rate ◽  
Thermomechanical Processing ◽  
Deformation Behaviour ◽  
True Strain ◽  
Hot Forging ◽  
Constitutive Law ◽  
Flow Rule ◽  
Plastic Energy

The aim of this work is to study the flow instabilities occurring during hot forging of titanium alloy blades. In this view, the viscoplastic deformation behaviour of Ti-6Al-4V alloy is investigated by means of torsion tests under isothermal hot working conditions at temperatures ranging from 800 to 1020 °C and strain rates of 0.01, 0.1 and 1s−1. The thermomechanical processing is performed up to a true strain of 10. The flow stress data are analysed in terms of strain rate and temperature sensitivities. A constitutive equation that relates not only the dependence of the flow stress on strain, strain rate and temperature, but also for the fraction of each phase α and β is proposed. Two mechanical models are compared : the uniform strain rate model (Taylor) and the uniform plastic energy model (IsoW). The usual strain rate sensitivity and activation energy values of Ti-6Al-4V alloy are obtained by fitting the experimental data. Furthermore, specific values of strain rate sensitivities and activation energies are calculated for the α and β phases providing thus a constitutive law based on the physics of the α / β phase diagram. The flow stress is then related to strain by an empirical equation taking into account the flow softening observed after a true strain of 0.5 and the steady state flow reached after a true strain of 4. Comparison of the calculated and measured flow stresses shows that the constitutive equation predicts the experimental results with a reasonable accuracy. The above constitutive equation is then used for simulating forging processes by the finite element method. The calculations exhibit the localisation of deformation produced by shearing effects in the form of the classical X shape.

Artificial Neural Network to Predict the Hot Deformation Behavior of Super 13Cr Martensitic Stainless Steel

2011 ◽  
Vol 695 ◽  
pp. 361-364 ◽  
Author(s):  
Ying Han ◽  
Guan Jun Qiao ◽  
Dong Na Yan ◽  
De Ning Zou
Keyword(s):  
Neural Network ◽  
Artificial Neural Network ◽  
Stainless Steel ◽  
Flow Stress ◽  
Strain Rate ◽  
Hot Deformation ◽  
Deformation Behavior ◽  
Martensitic Stainless Steel ◽  
Ann Model ◽  
Hot Deformation Behavior

The hot deformation behavior of super 13Cr martensitic stainless steel was investigated using artificial neural network (ANN). Hot compression tests were carried out at the temperature range of 950°C to 1200°C and strain rate range of 0.1–50s–1at an interval of an order of magnitude. Based on the limited experimental data, the ANN model for the constitutive relationship existed between flow stress and strain, strain rate and deformation temperature was developed by back-propagation (BP) neural network method. A three layer structured network with one hidden layer and ten hidden neurons was trained and the normalization method was employed in training for avoiding over fitting. Modeling results show that the developed ANN model can efficiently predict the flow stress of the steel and reflect the hot deformation behavior in the whole deforming process.

Constitutive Analysis of Ni-Base Superalloy Hastelloy X under Hot Compression Based on Thermodynamics

2012 ◽  
Vol 252 ◽  
pp. 73-76
Author(s):  
Horng Yu Wu ◽  
Hsu Cheng Liu ◽  
Feng Jun Zhu ◽  
Chui Hung Chiu
Keyword(s):  
Flow Stress ◽  
Constitutive Equation ◽  
Strain Rate ◽  
Hot Deformation ◽  
Elevated Temperatures ◽  
Flow Behavior ◽  
Dislocation Creep ◽  
Hastelloy X ◽  
Constitutive Analysis ◽  
Base Superalloy

Hot deformation characteristics of Hastelloy X Ni-base superalloy were investigated at elevated temperatures. Hot compressive tests were carried out in the temperature and strain rate ranges from 900 to 1150 °C and 0.001 to 1 s–1, respectively. The constitutive equation relating flow stress, temperature, and strain rate was obtained based on the peak stresses. The flow behavior showed that the softening mechanisms were related to the dynamic recovery (DRV) and dynamic recrystallization (DRX). The flow stress of Hastelloy X was fitted well by the constitutive equation of the hyperbolic sine function. The constitutive analysis suggested that the hot deformation mechanism of the Hastelloy X was dislocation creep.

Flow Stress Behavior of 2205 Duplex Stainless Steel during Warm Tensile

2012 ◽  
Vol 538-541 ◽  
pp. 1605-1610 ◽  
Author(s):  
Ji Xiang Zhang ◽  
Zheng Jun Li ◽  
Guo Yin An ◽  
Zhi Xiang Wang
Keyword(s):  
Stainless Steel ◽  
Flow Stress ◽  
Constitutive Equation ◽  
Strain Rate ◽  
Duplex Stainless Steel ◽  
Flow Behavior ◽  
Testing Machine ◽  
2205 Duplex Stainless Steel ◽  
Stress Behavior ◽  
Flow Stress Behavior

The flow behavior of 2205 duplex stainless steel for ship sheet in the strain rate ranging from 0.001 s-1 to 0.1s-1 and temperature ranging from 473K to 1073 K is studied on AG-10TA universal material testing machine. The results show that the 2205 duplex stainless steel is a strain rate sensitive material, and the flow stress increases with the increase of strain rate and decreases with the increase of temperature. The average elongation of the 2205 duplex stainless steel is above 25% with the temperature ranging from 473K-873K, and the elongation is above 47% at 1073K; At last, the flow stress constitutive equation is established based on the Browman model, which describes the flow stress behavior of 2205 duplex stainless steel in the temperature ranging from 473K-873K. The curves predicted by the constitutive equation agreement with the experiment data well.

Research on Flow Stress for 00Cr12Ti Stainless Steel

2011 ◽  
Vol 199-200 ◽  
pp. 1945-1948
Author(s):  
Bai Lin Fan ◽  
Ke Zhi Guan ◽  
Gang Han Huang
Keyword(s):  
Stainless Steel ◽  
Flow Stress ◽  
Linear Regression ◽  
Mathematical Models ◽  
Strain Rate ◽  
Hot Deformation ◽  
Non Linear ◽  
Temperature Strain

Flow stress of hot deformation about 00Cr12Ti stainless steel was experimentally studied by A Gleeble1500 thermo-mechanical simulator. The effects of deformed temperature, strain rate and strain to flow stress were analyzed .multiple Non-linear regression mathematical models of flow stress were proposed. 00Cr12Ti flow stress varies with temperature more slowly through 00Cr12Ti compared with 0Cr13Mn.

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