Piezoelectric Properties Study of KNN-LS Lead-Free Ceramics Synthesized by Sol-Gel Method

2014 ◽  
Vol 538 ◽  
pp. 15-18 ◽  
Author(s):  
Xin Jin ◽  
Xing Hua Fu ◽  
Wen Hong Tao ◽  
Yang Lu Hou
Keyword(s):  
Piezoelectric Coefficient ◽  
Piezoelectric Properties ◽  
Sintering Temperature ◽  
Perovskite Phase ◽  
Sol Gel ◽  
Second Phase ◽  
Gel Method ◽  
Sol Gel Method ◽  
Fine Grained ◽  
Lead Free Ceramics

Morphotropic phase boundary (MPB) composition, KNaNbO3-0.052LiSbO3(KNN-LS) was synthesized by sol-gel method at this experiment. Sb2O3 was used as economic Sb source and the final dried gel was calcined at 650°C for 2h to obtain white nanopowder. The sintering experiment was carried out at the temperature range of 980°C-1130°C, and perovskite phase structure could be observed apparently below 1080°C. When the temperature reached 1080°C and above, the second phase Na3LiNb6O17 appeared meanwhile the piezoelectric coefficient (d33) decreased quickly. Its proven that fine-grained particles and low sintering temperature could be obtained in sol-gel route.

scholarly journals Enhanced piezoelectric properties of (Bi0.5Na0.5)1－xBax TiO3 lead-free ceramics by sol-gel method

2004 ◽  
Vol 53 (7) ◽  
pp. 2357
Author(s):  
Zhao Ming-Lei ◽  
Wang Chun-Lei ◽  
Wang Jin-Feng ◽  
Chen Hong-Cun ◽  
Zhong Wei-Lie
Keyword(s):  
Piezoelectric Properties ◽  
Sol Gel ◽  
Lead Free ◽  
Gel Method ◽  
Sol Gel Method ◽  
Lead Free Ceramics

KNN-BF Lead-Free Piezoelectric Ceramics Synthesized by Sol-Gel Method

2015 ◽  
Vol 740 ◽  
pp. 3-6
Author(s):  
Guo Yuan Cheng ◽  
Xing Hua Fu ◽  
Xin Jin ◽  
Wen Hong Tao ◽  
Yu Qin Qiang
Keyword(s):  
Comparative Analysis ◽  
Citric Acid ◽  
Dielectric Loss ◽  
Sintering Temperature ◽  
Sol Gel ◽  
Piezoelectric Ceramics ◽  
Lead Free ◽  
Gel Method ◽  
Sol Gel Method ◽  
Metal Chelator

KNN-BF piezoelectric ceramics synthesized by sol-gel method in this experiment. By controlling bismuth and iron content in the system to study effects of them. We selected citric acid as metal chelator and ethylene glycol as esterification agent. PH maintained 5-6 during preparation of the sol. Sintering temperature of ceramic selected 1100°C. Preparation ceramics under these conditions and comparative analysis, the structure of ceramics is single perovskite and shap of crystals are square block. With the increase of x, properties of ceramics firstly increases and then decreases: d33, εr, Qm, Kpreaching the maximum, values of them were 136pC/N, 630(f =1KHz), 212, 0.41 respectively; dielectric loss to minimum is 0.07(f =1KHz); at this point, ceramics had best performance.

A Study on the Piezoelectric Properties of PZT and Doped PZT Thin Films by Sol-Gel Method

2010 ◽  
Vol 663-665 ◽  
pp. 650-653
Author(s):  
Jin Moo Byun ◽  
Jeong Sun Han ◽  
Jae Hyoung Park ◽  
Seong Eui Lee ◽  
Hee Chul Lee
Keyword(s):  
Thin Films ◽  
Piezoelectric Coefficient ◽  
Energy Harvester ◽  
Sol Gel ◽  
Pure Perovskite Structure ◽  
Pzt Thin Films ◽  
Gel Method ◽  
Sol Gel Method ◽  
Si Substrates ◽  
Pzt Thin Film

This study examined the effect of crystalline orientation and dopants such as Nb and Zn on the piezoelectric coefficient of sol-gel driven Pb1(Zr0.52Ti0.48)O3(PZT) and doped PZT thin films. Crack-free 1-μm-thick PZT and doped PZT thin films prepared by using 2-Methoxyethanol-based sol-gel method were fabricated on Pt/Ti/SiO2/Si substrates. The highly (111) oriented PZT thin films of pure perovskite structure could be obtained by controlling various parameters such as a PbTiO3 seed layer and a concentration of sol-gel solution. The Nb-Zn doped PZT thin films exhibited high piezoelectric coefficient which was about 50 % higher than that of undoped PZT thin film. The highest measured piezoelectric coefficient was 240 pC/N, which could be applicable to piezoelectrically operated MEMS actuator, sensor, or energy harvester devices.

La-Doped Nanometer TiO2 Powders Prepared by Sol-Gel Method

2016 ◽  
Vol 697 ◽  
pp. 97-100
Author(s):  
Zhi Cao Duan ◽  
Gui Min Jiang ◽  
Xue Quan Rong ◽  
Ji Kang Yan ◽  
Jing Hong Du ◽  
...  
Keyword(s):  
Sol Gel ◽  
Blue Shift ◽  
Phase Transformation Temperature ◽  
Second Phase ◽  
Temperature Phase ◽  
Gel Method ◽  
X Ray ◽  
Sol Gel Method ◽  
Doped Titania ◽  
La Doped

La-doped Titania powders were synthesized by sol-gel method. The influence of dopant on the phase transformation temperature, Phase compositions, chemical states, microstructures and the visible light absorbable range of titania were investigated, which were characterized by X-ray diffractometer (XRD), transmission electron microscopy (TEM), energy dispersion X-ray spectrum in scanning transmission electronic microscope (STEM-EDS) and UV-Vis spectrophotometer (UV-Vis). The results show that the dopant of La3+ significantly inhibited the phase transition and grain growth of TiO2.With the increasing of calcination temperature, the grain orientation of TiO2 are from clutter into order and the light absorption band edge of TiO2 are blue shift. La3+-doped titania precipitate La4Ti19O24 and the second phase precipitated on the surface of TiO2 with irregular spherical.

Microstructure and Properties of Fe/Al2O3 Gradient Coatings on Steel Substrate

2010 ◽  
Vol 150-151 ◽  
pp. 1325-1329
Author(s):  
Jian Fei Liu ◽  
Zhi Wang ◽  
Yin Sen Ding ◽  
Guo Pu Shi
Keyword(s):  
Adhesion Strength ◽  
Sintering Temperature ◽  
Steel Substrate ◽  
Sol Gel ◽  
Surface Hardness ◽  
Gel Method ◽  
Sol Gel Method ◽  
Chemical Combination ◽  
Gradient Coatings ◽  
Α Al2o3

The composites of Fe/Al2O3 gradient coatings on steel substrate were prepared by spraying and sol-gel method, and the microstructure and performances of the composites were analyzed. The results show that the adhesion strength of Fe/Al2O3 gradient coatings with FeAlNi transitional layers reaches 25.3MPa when the sintering temperature is 1220°C, and the surface hardness of coatings is four times higher than that of steel substrate. The coatings are mainly composed of α-Al2O3, AlFeO3 and NiFe2O4. There is no obvious hole or macro-interface, while some organization similar to the branch appears in the coatings. The bonding of Fe/Al2O3 gradient coatings and steel substrate mainly depends on adsorption, diffusion and chemical combination.

Effect of sintering temperature on structural, magnetic, magnetocaloric and critical behaviors of Ni-Cd-Zn ferrites prepared using sol-gel method

2018 ◽  
Vol 464 ◽  
pp. 91-102 ◽  
Author(s):  
Sobhi Hcini ◽  
Noura Kouki ◽  
Aref Omri ◽  
Abdessalem Dhahri ◽  
Mohamed Lamjed Bouazizi
Keyword(s):  
Sintering Temperature ◽  
Sol Gel ◽  
Gel Method ◽  
Sol Gel Method

Ferroelectric and piezoelectric properties of Ba(Ti0.89Sn0.11)O3 thin films prepared by sol–gel method

2015 ◽  
Vol 638 ◽  
pp. 168-172 ◽  
Author(s):  
Zhaowang Zhu ◽  
Xinli Guo ◽  
Zengmei Wang ◽  
Guoliang Yuan ◽  
Yiping Wang ◽  
...  
Keyword(s):  
Thin Films ◽  
Piezoelectric Properties ◽  
Sol Gel ◽  
Gel Method ◽  
Sol Gel Method ◽  
Ferroelectric And Piezoelectric Properties

Preparation of TiO2 Thin Films by Sol-Gel Method and Analysis of its Transmittance Based on Computer Image Processing

2020 ◽  
Vol 842 ◽  
pp. 121-126
Author(s):  
Ji Hui Luo ◽  
Qiu Yue Wen ◽  
Shu Liu ◽  
Ting Liu ◽  
Su Ting Wei ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Sintering Temperature ◽  
Raw Materials ◽  
Sol Gel ◽  
Light Transmittance ◽  
Anatase Structure ◽  
Gel Method ◽  
Sol Gel Method ◽  
Computer Image Processing ◽  
Imagej Software

TiO2 films were prepared by sol-gel method with butyl titanate, anhydrous ethanol, acetyl acetone and hydrochloric acid as raw materials, which were sintered at 380 °C and 530 °C respectively to obtain TiO2 films. XRD was used for analyzing the crystal structure of TiO2 film, and ImageJ software was used to detect the light transmittance of TiO2 film samples. The results show that the film sintered at 530 °C is brookite structure and the film sintered at 380 °C is anatase structure. The increase of sintering temperature is not conducive to the growth of TiO2 film grains. TiO2 films sintered at 380 °C have good light transmittance.

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