Background of Branched Crack Formation in Surface Zone of Continuously-Cast Ti-Nb Microalloyed Steel Slab

2015 ◽  
Vol 1127 ◽  
pp. 143-149
Author(s):  
Pavel Bekeč ◽  
Margita Longauerová ◽  
Marek Vojtko ◽  
Ondrej Milkovič ◽  
Jiří Kadlec ◽  
...  
Keyword(s):  
Crack Formation ◽  
Microstructural Analysis ◽  
Thin Strip ◽  
Thick Sheet ◽  
Surface Zone ◽  
Slab Surface ◽  
Cast Slab ◽  
X Ray ◽  
Continuously Cast ◽  
Oscillation Marks

Branched cracks are undesirable and dangerous, and under the oxidized surface of a continuously-cast slab they are mostly difficult to identify. They can cause the formation of defects in thick sheet or on thin strip. This work deals with the study of the background to the formation of branched cracks in a continuously-cast slab, at pulling rate 0.43 m.min-1. The results of the work show that branched cracks extended to a depth of 10 mm below the slab surface and occurred mostly below oscillation marks. Cracks were mostly present in the edge parts of the slab, where they were also deeper in comparison with locations in the middle of the slab width. Microstructural analysis confirmed heterogeneity of ferrite grain sizes in the slab surface skin. The microstructure was formed predominantly of polyhedral ferritic-pearlitic grains, and on the ferritic grain boundaries the presence of tertiary cementite was observed. In the area around the cracks mainly non-equilibrium microstructure of acicular character was observed. A typical feature of these cracks after their opening is intercrystalline fracture. Wavelength-dispersive X-ray analysis of a sample with a branched crack showed chemical heterogeneity of harmful elements, mainly S and As. Large amounts of these elements point to their significant segregation. The formation of branched cracks is conditioned not only by segregation of impurities, but possibly also by the presence of undesirable brittle cementite networks. The presence of cementite was confirmed not only by microstructural analysis, but also diffraction of hard X-ray radiation. Precipitation of microalloying elements in connection with the cementite can lead to higher probability of surface crack formation, as also confirmed in this study.Keywords: slab, branched cracks, oscillation marks, segregation, precipitation

Precipitation in Surface Zone of Continuously-Cast Slab of ULC/IF Steel Microalloyed with Titanium

2014 ◽  
Vol 782 ◽  
pp. 73-80 ◽  
Author(s):  
Margita Longauerová ◽  
Maria Hurakova ◽  
Svätoboj Longauer
Keyword(s):  
Continuous Casting ◽  
Drawing Rate ◽  
Surface Zone ◽  
If Steel ◽  
Slab Surface ◽  
Cast Slab ◽  
Surface Areas ◽  
Elliptical Shape ◽  
Continuously Cast ◽  
Mean Size

The aim of this work was to analyze the morphology and distribution of the microalloy precipitates in the slab surface zone of ULC/IF steel microalloyed with titanium. The slab was made by continuous casting using two different slab pulling rates. Transient slabs were pulled with pulling rate 0.4 m/min at the start and 0.8 m/min at the end of the slab. It was confirmed that morphology of the particles evaluated in the surface areas of slab were globular, cubical or elliptical shape and have been identified as of TiS, TiN and TiC. At the lower drawing rate particles from the middle cut-out from an area with coarse ferritic grains at the slab surface attained an mean size of 2r = 41.8 nm, and from an area with fine ferritic grains they attained an mean size of 2r = 32.5 nm. At the higher drawing rate particles in the middle cut-out attained an mean size of 2r= 63.5 nm. The coarser particles were found in areas with coarse ferrite grains and at higher pulling speed.

Improvement of Continuously Cast Slab Surface and Performance of Rolling the Slab Free from Surface Conditioning

1981 ◽  
Vol 67 (8) ◽  
pp. 1229-1235 ◽  
Author(s):  
Minoru KITAMURA ◽  
Tosiyuki SOEJIMA ◽  
Sinzi KOYAMA ◽  
Yosihiro MATUDA ◽  
Junji ABU ◽  
...  
Keyword(s):  
Slab Surface ◽  
Cast Slab ◽  
Surface Conditioning ◽  
Continuously Cast ◽  
And Performance

Influence of Casting Rate on TiNb Microalloyed Steel Slab Surface Area Microstructure

2014 ◽  
Vol 782 ◽  
pp. 81-86 ◽  
Author(s):  
Pavel Bekeč ◽  
Margita Longauerová ◽  
Marek Vojtko
Keyword(s):  
Microalloyed Steel ◽  
Casting Rate ◽  
Surface Zone ◽  
Slab Surface ◽  
Aluminum Oxides ◽  
Grain Sizes ◽  
Steel Slab ◽  
Nb Microalloyed Steel ◽  
Oscillation Marks ◽  
Equilibrium Microstructure

Two slabs of Ti-Nb microalloyed steel were analysed in this work. The first slab was transitional with the initial pulling rate 0.43 m.min-1 and the final pulling rate 0.9 m.min-1. The second slab was cast at the real production pulling rate 1.03 m.min-1. The presence of larger amounts of oscillation marks was observed on the first slab at both pulling rates. The second slab showed no oscillation marks. At the lowest pulling rate, cracks were discovered below the slab surface, often below oscillation marks. Cracks were seldom observed at pulling rate 0.9 m.min-1. In the first slab, especially at the low pulling rate, the presence of cracks and pores was found. Pores were observed often with clusters of aluminum oxides. The microstructure of the slab surface zone was characterised by heterogeneity of ferrite grain sizes at all three pulling rates. This heterogeneity was manifested mainly in the marginal cut-outs at all pulling rates. In the marginal cut-outs the microstructure was granulometrically finer at all three pulling rates than in the central cut-outs. Non-equilibrium microstructure in the marginal cut-outs was also observed.

scholarly journals Laser Powder Bed Fusion Processing of Fe-Mn-Al-Ni Shape Memory Alloy—On the Effect of Elevated Platform Temperatures

Metals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 185
Author(s):  
Felix Clemens Ewald ◽  
Florian Brenne ◽  
Tobias Gustmann ◽  
Malte Vollmer ◽  
Philipp Krooß ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Crack Formation ◽  
Microstructural Analysis ◽  
Tensile Load ◽  
Grain Structure ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Cyclic Heat Treatment ◽  
Powder Bed ◽  
Cyclic Heat

In order to overcome constraints related to crack formation during additive processing (laser powder bed fusion, L-BPF) of Fe-Mn-Al-Ni, the potential of high-temperature L-PBF processing was investigated in the present study. The effect of the process parameters on crack formation, grain structure, and phase distribution in the as-built condition, as well as in the course of cyclic heat treatment was examined by microstructural analysis. Optimized processing parameters were applied to fabricate cylindrical samples featuring a crack-free and columnar grained microstructure. In the course of cyclic heat treatment, abnormal grain growth (AGG) sets in, eventually promoting the evolution of a bamboo like microstructure. Testing under tensile load revealed a well-defined stress plateau and reversible strains of up to 4%.

scholarly journals Effect of Molybdenum Content on the Corrosion and Microstructure of Low-Ni, Co-Free Maraging Steels

Metals ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 852
Author(s):  
Asiful H. Seikh ◽  
Hossam Halfa ◽  
Mahmoud S. Soliman
Keyword(s):  
Corrosion Resistance ◽  
Electrochemical Impedance ◽  
Microstructural Analysis ◽  
Xrd Analysis ◽  
X Ray Diffraction ◽  
Alloying Element ◽  
X Ray ◽  
Maraging Steels ◽  
Eds Analysis ◽  
Electroslag Refining

Molybdenum (Mo) is an important alloying element in maraging steels. In this study, we altered the Mo concentration during the production of four cobalt-free maraging steels using an electroslag refining process. The microstructure of the four forged maraging steels was evaluated to examine phase contents by optical microscopy, scanning electron microscopy (SEM), and X-ray diffraction (XRD) analysis. Additionally, we assessed the corrosion resistance of the newly developed alloys in 3.5% NaCl solution and 1 M H2SO4 solution through potentiodynamic polarization and electrochemical impedance spectroscopy (EIS) techniques. Furthermore, we performed SEM and energy-dispersive spectroscopy (EDS) analysis after corrosion to assess changes in microstructure and Raman spectroscopy to identify the presence of phases on the electrode surface. The microstructural analysis shows that the formation of retained austenite increases with increasing Mo concentrations. It is found from corrosion study that increasing Mo concentration up to 4.6% increased the corrosion resistance of the steel. However, further increase in Mo concentration reduces the corrosion resistance.

scholarly journals Micro-Fabric Analyzer (MFA): A New Semiautomated ArcGIS-Based Edge Detector for Quantitative Microstructural Analysis of Rock Thin-Sections

2021 ◽  
Vol 10 (2) ◽  
pp. 51 ◽  
Author(s):  
Roberto Visalli ◽  
Gaetano Ortolano ◽  
Gaston Godard ◽  
Rosolino Cirrincione
Keyword(s):  
Physical Properties ◽  
Electron Backscatter Diffraction ◽  
Microstructural Analysis ◽  
Image Features ◽  
Elemental Distribution ◽  
Edge Detector ◽  
Sandstone Sample ◽  
Thin Sections ◽  
X Ray ◽  
Distribution Maps

Micro-Fabric Analyzer (MFA) is a new GIS-based tool for the quantitative extrapolation of rock microstructural features that takes advantage both of the characteristics of the X-ray images and the optical image features. Most of the previously developed edge mineral grain detectors are uniquely based on the physical properties of the X-ray-, electron-, or optical-derived images; not permitting the exploitation of the specific physical properties of each image type at the same time. More advanced techniques, such as 3D microtomography, permit the reconstruction of tridimensional models of mineral fabric arrays, even though adjacent mineral grain boundaries with the same atomic density are often not detectable. Only electron backscatter diffraction (EBSD) allows providing high-performing grain boundary detection that is crystallographically differentiated per mineral phase, even though it is relatively expensive and can be executed only in duly equipped microanalytical laboratories by suitably trained users. Instead, the MFA toolbox allows quantifying fabric parameters subdivided per mineral type starting from a crossed-polarizers high-resolution RGB image, which is useful for identifying the edges of the individual grains characterizing rock fabrics. Then, this image is integrated with a set of micro-X-ray maps, which are useful for the quantitative extrapolation of elemental distribution maps. In addition, all this is achieved by means of low-cost and easy-to-use equipment. We applied the tool on amphibolite, mylonitic-paragneiss, and -tonalite samples to extrapolate the particle fabric on different metamorphic rock types, as well as on the same sandstone sample used for another edge detector, which is useful for comparing the obtained results.

scholarly journals An evaluation of critical strain for internal crack formation in continuously cast slabs.

1986 ◽  
Vol 26 (6) ◽  
pp. 540-546 ◽  
Author(s):  
Tooru MATSUMIYA ◽  
Michihisa ITO ◽  
Hiroyuki KAJIOKA ◽  
Shigehiro YAMAGUCHI ◽  
Yasushi NAKAMURA
Keyword(s):  
Critical Strain ◽  
Crack Formation ◽  
Internal Crack ◽  
Continuously Cast

Local Notch Toughness of Slab Surface Zone in ULC/IF and HSLA Steels

2015 ◽  
Vol 662 ◽  
pp. 209-212
Author(s):  
Margita Longauerová ◽  
Maria Hurakova ◽  
Pavel Bekeč ◽  
Svätoboj Longauer ◽  
Mária Fedorová ◽  
...  
Keyword(s):  
Hsla Steel ◽  
Notch Toughness ◽  
Grain Structure ◽  
Surface Zone ◽  
Slab Surface ◽  
Slab Width ◽  
Fine Grain ◽  
Hsla Steels ◽  
Ferrite Structure ◽  
Ferrite Grain Size

The aim of this work was to analyze changes in local toughness KCV using Charpy V-notch impact tests in the slab surface zone in relation to the microstructure in ULC/ IF steel and TiNb HSLA steel. Marked heterogeneity in KCV values was confirmed in the surface zone across the width of transitional slabs. Distinct local differences in notch toughness across the slab width were found to be linked primarily with changes in ferrite grain size. Low KCV values in the analyzed steels were linked with coarse grain structure, while much finer ferrite structure was identified in tough samples. The heterogeneity of KCV vales in the analyzed steels may be influenced by differences in thickness of the fine-grain slab surface zone, and by the presence of tertial cementite and (in HSLA steel) of pearlite as well.

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