Experimental Study on Synthesis of High Purity Mullite

2011 ◽  
Vol 328-330 ◽  
pp. 1343-1346
Author(s):  
Zhen Wu Shi ◽  
Nian Suo Xie
Keyword(s):  
Experimental Study ◽  
Phase Composition ◽  
Constant Temperature ◽  
High Purity ◽  
Sintering Temperature ◽  
Dissolution Mechanism ◽  
Resistance Furnace ◽  
Output Rate ◽  
Mullite Phase

In this paper, the influence of sintering temperature on the output rate of the mullite which was formed from andalusite ore of Mei County Shaanxi at different constant temperature 1350°C, 1450°C, 1550°C and the mechanism which mullite was transformed were studied. The morphology of mullite formed at 1450°C was obtained by SEM, and the phase composition of andalusite ore sintered at different temperature was analyzed by XRD. The results shows that the mullitization effect of andalusite ore of Mei County Shaanxi is excellent, and the yield of mullite mineral can reach the desired results of 100% after andalusite mineral of Mei County Shaanxi is kept warming for 3 hours at the sintering temperature of 1450°C and cooled naturally with box-type resistance furnace. The mullite phase synthesized by andalusite ore of Mei County Shaanxi depends on not only the decomposition of andalusite, but also the secondary mullitization and the dissolution mechanism.

The Effects of Mineral Composition and Sintering Temperature on Synthetic Mullite

2014 ◽  
Vol 633 ◽  
pp. 65-68
Author(s):  
Lei Li ◽  
Xiao Guang Zhang ◽  
Rui Long Wen ◽  
Cheng Biao Wang ◽  
Ming Hao Fang ◽  
...  
Keyword(s):  
Phase Composition ◽  
Flexural Strength ◽  
Physical Properties ◽  
Energy Saving ◽  
Environmental Protection ◽  
Mineral Composition ◽  
Sintering Temperature ◽  
Final Phase ◽  
Mullite Phase ◽  
Industrial Alumina

Mullite material was prepared from quartz (SiO2) and industrial alumina (γ-Al2O3). The effects of mineral composition and sintering temperature on the final phase composition and physical properties of mullite were investigated. The results shown that a large number of mullite phase was emerged in samples when the ratio of alumina to silica (A/S) was 2.55. At 1500 oC and 1600 oC, the flexural strength of the samples reached to 87.13 MPa and 89.50 MPa, respectively. Consider the environmental protection and energy saving, the optimal sintering temperature was 1500 °C.

Effect of spark plasma sintering temperature on structure and phase composition of Ti-Al-Nb-based alloys

2017 ◽  
Vol 59 (11-12) ◽  
pp. 1033-1036 ◽  
Author(s):  
Sherzod Kurbanbekov ◽  
Mazhyn Skakov ◽  
Viktor Baklanov ◽  
Batyrzhan Karakozov
Keyword(s):  
Phase Composition ◽  
Spark Plasma Sintering ◽  
Sintering Temperature ◽  
Plasma Sintering ◽  
Spark Plasma

Effect of Sintering Temperature and Time in Nickel Wick for Loop Heat Pipe with Flat Evaporator

2014 ◽  
Vol 602-605 ◽  
pp. 528-532
Author(s):  
Shen Chun Wu ◽  
Chang Yu Wu ◽  
Weie Jhih Lin ◽  
Jia Ruei Chen ◽  
Yau Ming Chen
Keyword(s):  
Heat Pipe ◽  
Constant Temperature ◽  
Heat Load ◽  
Sintering Temperature ◽  
Performance Testing ◽  
Effective Porosity ◽  
Temperature Curve ◽  
Loop Heat Pipe ◽  
Maximum Heat ◽  
Load Increase

This paper specifically addresses the effect of changing the constant temperature region of the sintering temperature curve in manufacturing nickel powder capillary structure (wick) on the performance of a flat loop heat pipe (FLHP). The sintering temperature curve is composed of three regions: a region of increasing temperature, a region of constant temperature, and a region of decreasing temperature, with the sintering time and temperature in the region of constant temperature having significant effect on the permeability of the wick. In this study, for wick manufacturing the temperatures in this region tested range from 550°C to 650°C and the time from 30 minutes to 60 minutes. The properties and internal parameters of the wick are measured, and the wick is placed into FLHP for performance testing. Experimental results show that at sintering temperature of 550°C and lasting about 45 minutes, maximum heat load is 200W, minimum thermal resistance is 0.32°C/W, permeability is , porosity is 66%, effective porosity is 3.8and heat flux is around 21W/cm2; related literatures have only reported maximum heat load increase of 25%.

Effect of Sintering Temperature on the Synthesis of High Purity Cordierite

2008 ◽  
Author(s):  
Y. P. Choo ◽  
T. Y. Chow ◽  
H. Mohamad ◽  
Abarrul Ikram ◽  
Agus Purwanto ◽  
...  
Keyword(s):  
High Purity ◽  
Sintering Temperature

scholarly journals Effect of the sintering temperature on the fabrication of alumina beads

2019 ◽  
Vol 16 (2) ◽  
pp. 125-135
Author(s):  
Ayse KALEMTAS
Keyword(s):  
Sintering Temperature ◽  
Sol Gel ◽  
Xrd Analysis ◽  
Liquid Phase Sintering ◽  
Sintered Ceramic ◽  
Mullite Phase ◽  
Commercial Grade ◽  
Composite Beads ◽  
Sintering Additive ◽  
Dta Analysis

In this study, kaolin bonded alumina-alginate composite beads were fabricated via a facile one-step sol-gel process by using sodium alginate. In order to achieve sintering of the beads at lower sintering temperatures a limited amount of CC31 commercial-grade kaolin was used as a sintering additive (Al2O3:CC31 commercial-grade kaolin=14:1). Produced composite beads were heat treated at 1300°, 1400° and 1500°C for 1 hour to achieve partial densification of the beads. TG-DTA analysis of the CC31 commercial-grade kaolin showed that mullite phase formation took place approximately at 1000°C. However, XRD measurements revealed that there is only alumina phase in the sintered ceramic beads. Due to the low amount of CC31 commercial-grade kaolin, mullite formation was not detectable via XRD analysis. No significant grain growth was observed at the sintered samples depending on the increasing sintering temperature. However, when the sintering temperature was increased, densification ratio and mechanical properties of the produced beads were enhanced significantly. Microstructural investigations of the sintered beads shown that with the help of the liquid phase sintering process, a good chemical bonding was achieved between the alumina particles.

scholarly journals Enhanced Performance of Fly Ash-Based Supports for Low-Cost Ceramic Membranes with the Addition of Bauxite

Membranes ◽  
2021 ◽  
Vol 11 (9) ◽  
pp. 711
Author(s):  
Wan Fan ◽  
Dong Zou ◽  
Jingrui Xu ◽  
Xianfu Chen ◽  
Minghui Qiu ◽  
...  
Keyword(s):  
Fly Ash ◽  
High Performance ◽  
Bending Strength ◽  
Ceramic Membrane ◽  
Sintering Temperature ◽  
Low Cost ◽  
Pure Water ◽  
Ceramic Membranes ◽  
Mullite Phase ◽  
Optimum Balance

Support is a necessary foundation for ceramic membranes to achieve high performance. Finding the optimum balance between high performance and low cost is still a significant challenge in the fabrication of ceramic supports. In this study, low-cost fly ash-based ceramic supports with enhanced performance were prepared by the addition of bauxite. The pore structure, mechanical strength, and shrinkage of fly ash/bauxite supports could be tuned by optimizing the bauxite content and sintering temperature. When the sintering temperature and bauxite content were controlled at 1300 °C and 40 wt%, respectively, the obtained membrane supports exhibited a high pure water permeance of approximately 5.36 m3·m−2·h−1·bar−1 and a high bending strength of approximately 69.6 MPa. At the same time, the optimized ceramic supports presented a typical mullite phase and excellent resistance to acid and alkali. This work provides a potential route for the preparation of ceramic membrane supports with characteristics of low cost and high performance.

Effect of Mineral Composition and Sintering Temperature on the Synthetic Cordierite

2014 ◽  
Vol 633 ◽  
pp. 61-64
Author(s):  
Lei Li ◽  
Rui Long Wen ◽  
Xiao Guang Zhang ◽  
Cheng Biao Wang ◽  
Ming Hao Fang ◽  
...  
Keyword(s):  
Phase Composition ◽  
High Temperature ◽  
Flexural Strength ◽  
Mineral Composition ◽  
Sintering Temperature ◽  
Raw Materials ◽  
Temperature Reaction ◽  
Final Phase ◽  
High Temperature Reaction ◽  
Industrial Alumina

Cordierite samples were prepared using quartz sand tailings, industrial alumina and magnesite tailings as raw materials by high-temperature reaction. The influence of mineral composition and sintering temperature on the final phase composition and physical properties of cordierite were studied. The results shown that a large number of cordierite generated at 1300 °C. When the ratio of Al2O3/SiO2 equals to 1.08, the flexural strength of samples increased to 27.66 MPa.

Spark Plasma Sintering of Paper-Derived Ti3AlC2-Based Composites: Influence of Sintering Temperature

2021 ◽  
Vol 1016 ◽  
pp. 1790-1796
Author(s):  
Maxim Syrtanov ◽  
Egor Kashkarov ◽  
Tatyana Murashkina ◽  
Nahum Travitzky
Keyword(s):  
Phase Composition ◽  
Spark Plasma Sintering ◽  
Sintering Temperature ◽  
Total Content ◽  
X Ray Diffraction ◽  
X Ray ◽  
Carbide Phases ◽  
Plasma Sintering ◽  
Spark Plasma ◽  
Scanning Electron

This paper describes the influence of sintering temperature on phase composition and microstructure of paper-derived Ti3AlC2 composites fabricated by spark plasma sintering. The composites were sintered at 100 MPa pressure in the temperature range of 1150-1350 °C. Phase composition and microstructure were analyzed by X-ray diffraction and scanning electron microscopy, respectively. The multiphase structure was observed in the sintered composites consisting of Ti3AlC2, Ti2AlC, TiC and Al2O3 phases. The decomposition of the Ti3AlC2 phase into Ti2AlC and TiC carbide phases was observed with temperature rise. The total content of Ti3AlC2 and Ti2AlC phases was reduced from 84.5 vol.% (1150 °C) to 69.5 vol.% (1350 °C). The density of composites affected by both the content of TiC phase and changes in porosity.

Experimental Study of Ion Dynamic Effects in Overlapping Helium Lines at Low Densities

1983 ◽  
Vol 38 (1) ◽  
pp. 37-46 ◽  
Author(s):  
A. Piel ◽  
H. Richter
Keyword(s):  
Experimental Study ◽  
High Purity ◽  
Line Shape ◽  
Plasma Source ◽  
Line Profiles ◽  
Dynamic Effects ◽  
Electron Densities ◽  
Plasma Parameters ◽  
Critical Comparison

Abstract The line profiles of the overlapping helium lines 447.1 nm and 492.2 nm have been investigated in an improved plasma source of high purity at electron densities of 1 × 1021 m−3 and 3 × 1021 m−3 . The plasma parameters Ne, Te and T0 were determined carefully by independent diagnostics, which enables a critical comparison with existing theories (BCS II and MMM). We observed ion dynamic effects which considerably modify the line shape of the forbidden components. Our experiments extend the existing observations towards higher ion temperatures. Systematic trends observed earlier are critically discussed.

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