Wear Assessment of Ti/SiC Surface Nano-Composite Layer and its Associated CP-Ti Substrate

2012 ◽  
Vol 445 ◽  
pp. 595-600 ◽  
Author(s):  
Ali Shamsipur ◽  
Seyed Farshid Kashani-Bozorg ◽  
Abbas Zarei Hanzaki
Keyword(s):  
Surface Layer ◽  
Wear Behavior ◽  
Composite Layer ◽  
Pure Titanium ◽  
Commercially Pure Titanium ◽  
Micro Hardness ◽  
Wear Properties ◽  
Friction Stir ◽  
Pin On Disc ◽  
Cp Ti

In the present investigation, the surface of a commercially pure titanium (CP-Ti) substrate was modified to Ti/SiC nanocomposite layer employing friction stir processing technique; nanosized SiC powder was introduced into the stir zone provided by a rotating and advancing tool. The fabricated nanocomposite surface layer exhibited a micro hardness value of ~535HV which is much greater than 160HV of the substrate material using Vickers micro hardness testing. In addition, the un-treated CP-Ti substrate showed sever wear regime in the pin-on-disc test against the hardened AISI 52100 steel. It suffers extensive typical adhesive wear dominated by plastic deformation as evidenced by scanning electron microscopy. Also, deep grooves were formed, i.e. evidence of abrasive wear. Contrary to this, enhanced wear properties were detected for the Ti/SiC nanocomposite surface layer, i.e. lower coefficient of friction and weight loss. The nanocomposite surface layer was found to be adherent to the underlying substrate during the pin-on-disc test. The superior wear behavior of the nanocomposite surface layer is attributed to its improved micro hardness value due to the presence of hard nanosize SiC particles in a refined titanium matrix.

The Influence of Laser Irradiation Parameters on Tribological Behaviour of Commercially Pure Titanium for Dental Prostheses

2016 ◽  
Author(s):  
Karibeeran Shanmuga Sundaram ◽  
Gurusami Kiliyappan ◽  
Senthil Kumaran Selvadurai
Keyword(s):  
Surface Roughness ◽  
Wear Resistance ◽  
Pure Titanium ◽  
Laser Surface ◽  
Commercially Pure Titanium ◽  
Laser Shock ◽  
Micro Hardness ◽  
Dental Prostheses ◽  
Commercially Pure ◽  
Cp Ti

Laser shock peening (LSP) is one of the innovative technique that produces a compressive residual stress on the surface of metallic materials, thereby significantly increasing its fatigue life in applications where failure is caused by surface-initiated cracks. The specimens were treated with laser shock waves with different processing parameters, and characterization studies were made on treated specimens. The purpose of the present study was to investigate the influence of Nd:YAG laser on commercially pure titanium (CP-Ti) used in prosthetic dental restorations. The treatment influenced change in microstructure, micro hardness, surface roughness, and wear resistance characteristics. Though CP-Ti is considered as an excellent material for dental applications due to its outstanding biocompatibility, it is not suitable when high mastication forces are applied. In the present study, pulsed Nd:YAG laser surface treatment technique was adopted to improve the wear resistance of CP-Ti. The wear test pin specimens of CP-Ti were investment cast with centrifugal titanium casting machine. The wear properties of specimens were evaluated after LSP on a “pin-on-disc” wear testing tribometer, as per ASTM G99-05 standards. The results of the wear experiment showed that the treated laser surface has higher wear resistance, micro hardness, and surface roughness compared to as-cast samples. The improvement of wear resistance may be attributed due to grain refinement imparted by LSP processes. The microstructure, wear surfaces, wear debris, and morphology of the specimen were analyzed by using optical electron microscope, scanning electron microscope, and X-ray diffraction (XRD). The data were compared using ANOVA and post-hoc Tukey tests. The characteristic change resulted in increase in wear resistance and decrease in wear rate. Hence, it is evident that the more reliable and removable partial denture metal frameworks for dental prostheses may find its applications.

High Energy Shot Peening of Commercially Pure Titanium TIG Weld Joint

2010 ◽  
Vol 148-149 ◽  
pp. 659-663
Author(s):  
Chun Huan Chen ◽  
Rui Ming Ren
Keyword(s):  
Surface Layer ◽  
Weld Joint ◽  
Shot Peening ◽  
Welded Joint ◽  
Pure Titanium ◽  
High Energy ◽  
Commercially Pure Titanium ◽  
Nanostructured Surface ◽  
Commercially Pure ◽  
Cp Ti

Commercially pure Titanium (CP-Ti) TIG weld joint was treated by means of high energy shot peening (HESP) using a shot peening equipment commonly used in industry. The nanostructured surface layer was characterized by XRD, TEM, SEM and Microhardometer. The results showed that surface nanocrystallization of CP-Ti TIG weld joint were realized by high energy shot peening treatment. The finest grain size in the top surface layer is about 40nm. The hardness of the surface layer is enhanced significantly after shot peening compared with that of the as-welded joint, which resulted in a remarkable surface hardening effect. Surface welded defects such as air pores are eliminated successfully so that relative uniform surface layer was obtained.

The Effect of Strain Rate on the Plastic Deformation Mode of CP-Ti during Surface Nanocrystallization

2011 ◽  
Vol 675-677 ◽  
pp. 239-242
Author(s):  
Chun Huan Chen ◽  
Cheng Jin ◽  
Rui Ming Ren
Keyword(s):  
Plastic Deformation ◽  
Surface Layer ◽  
Strain Rate ◽  
Shot Peening ◽  
Pure Titanium ◽  
Deformation Mode ◽  
Rate Variation ◽  
Commercially Pure Titanium ◽  
Surface Nanocrystallization ◽  
Cp Ti

The effect of the strain rate on the surface nanocrystallization of titanium is investigated both theoretically and experimentally in this paper. The strain rate variation and stress distribution from surface to the interior of titanium during shot peening are estimated firstly using finite element method. Then shot peening experiment is carried out on a commercially pure titanium (CP-Ti) plate, and the obtained surface microstructures is characterized by transmission electron microscopy (TEM). Combining theoretical simulations and experimental observations, the effect of strain rate on the strain accommodation mechanism and plastic deformation mode are discussed. It is concluded that the strain rate and stress achieve the highest at the top surface layer of CP-Ti, and the strain rate decrease dramatically from the surface to the interior. The strain rate at the top surface layer is up to 104 s-1, which leads to superplastic deformation of Ti. There is no mechanical twin in the surface layer, instead, deformation lamella and adiabatic shear bands are the dominating microstructures. By means of rotation recrystallization, those deformation bands evolve to nanocrystallines.

FABRICATION OF TI/SIC SURFACE NANO-COMPOSITE LAYER BY FRICTION STIR PROCESSING

2012 ◽  
Vol 05 ◽  
pp. 367-374 ◽  
Author(s):  
ALI SHAMSIPUR ◽  
SEYED FARSHID KASHANI-BOZORG ◽  
ABBAS ZAREIE-HANZAKI
Keyword(s):  
Friction Stir Processing ◽  
Composite Layer ◽  
Pure Titanium ◽  
Titanium Substrate ◽  
Commercially Pure Titanium ◽  
Nano Composite ◽  
Composite Surface ◽  
Friction Stir ◽  
Commercially Pure ◽  
Sic Particles

In the present investigation, novel Ti / SiC surface nano-composite layer was successfully fabricated by dispersing nano-sized SiC particles into commercially pure titanium plates employing friction stir processing technique. The process parameters such as tool rotation and advancing speeds were adjusted to produce defect-free surface composite layer, however, uniform distribution of the nano-size SiC particles in a matrix of titanium was achieved after the second pass. The micro hardness value of the Ti / SiC nano-composite surface layer was found to be ~534 HV; this is 3.3 times higher than that of the commercially pure titanium substrate. No reaction was detected between SiC powders and the titanium matrix after friction stir processing.

scholarly journals Nano-Surface Composite Coating Reinforced by Ta2C, Al2O3 and MWCNTs Nanoparticles for Aluminum Base via FSP

Coatings ◽  
2021 ◽  
Vol 11 (12) ◽  
pp. 1496
Author(s):  
Essam B. Moustafa ◽  
Waheed Sami Abushanab ◽  
Ammar Melaibari ◽  
Anastasia V. Mikhaylovskaya ◽  
Mohamed Shaaban Abdel-Wahab ◽  
...  
Keyword(s):  
Aluminum Alloy ◽  
Wear Behavior ◽  
Composite Layer ◽  
Wear Properties ◽  
2024 Aluminum Alloy ◽  
Advanced Technique ◽  
Multi Wall Carbon Nanotubes ◽  
Friction Stir ◽  
Surface Composite ◽  
Al 2024

In the present work, an advanced technique was applied to coat an Al 2024 alloy with a surface composite layer reinforced with various nanoparticles. The surface of Al 2024 aluminum alloy was modified with Ta2C, Al2O3 and multi wall carbon nanotubes MWCNTs nanoparticles by friction stir process (FSP). An improvement in the surface of the fabricated nanocomposite due to the refinement of the microstructure grains was achieved. In addition, a significant improvement in the hardness and wear behavior was observed. The reinforcement particles were incorporated into double and triple hybrid composite particles to determine the most effective combination for the controlled properties. The results showed that for the composite reinforced with a double hybrid of Al2O3 and MWCNTs, the microstructure grains of the fabricated nanocomposite surface were refined by 40 times. The hardness was significantly improved, i.e., it was increased by 48% by incorporating the triple reinforcement (Ta2C, Al2O3, and MWCNTs) into the surface of Al 2024 aluminum alloy. The results of wear properties were in agreement with the results of hardness; the maximum wear resistance was obtained for Al 2024-Ta2C + Al2O3 + MWCNTs, and the wear rate was reduced by 11 times.

ABRASIVE WEAR BEHAVIOR OF NITRIDED TEXTURED TITANIUM

2020 ◽  
Vol 27 (12) ◽  
pp. 2050025
Author(s):  
XINGLIANG LI ◽  
WEN YUE ◽  
JIAJIE KANG ◽  
LINA ZHU ◽  
BIN TIAN ◽  
...  
Keyword(s):  
Abrasive Wear ◽  
Wear Behavior ◽  
Surface Texturing ◽  
Pure Titanium ◽  
Laser Surface Texturing ◽  
Commercially Pure Titanium ◽  
Ion Nitriding ◽  
Wear Properties ◽  
Abrasive Wear Behavior ◽  
Titanium Grade

In order to improve the anti-friction and anti-wear performances of titanium and expand its application in aerospace and aircraft area, a commercially pure titanium grade 2 (TA2) was chosen and treated by compositing surface treatment. Dimple textures were prepared on the titanium surface by laser surface texturing (LST), and then the textured titanium was treated by ion nitriding. Tribological behaviors of the textured titanium and nitrided textured titanium were investigated under abrasive wear on a tribo-tester. The result shows that the anti-friction and anti-wear properties of textured titanium can be greatly improved by 47.1% and 79.3% after nitriding treatment, respectively. In addition, the dimple density has a significant effect on anti-friction and anti-wear behaviors.

CP-Ti Processed for Multiple Passes by ECAP at Room Temperature

2010 ◽  
Vol 667-669 ◽  
pp. 779-784
Author(s):  
Xi Rong Yang ◽  
Xi Cheng Zhao ◽  
Xiao Yan Liu
Keyword(s):  
Room Temperature ◽  
Elevated Temperatures ◽  
Pure Titanium ◽  
Commercially Pure Titanium ◽  
Micro Hardness ◽  
Angular Pressing ◽  
Commercially Pure ◽  
Series Of Experiments ◽  
Ram Speed ◽  
Cp Ti

A series of experiments were conducted to evaluate the feasibility that commercially pure titanium (CP-Ti) was pressed for multiple passes by equal channel angular pressing (ECAP) at room temperature. Samples of CP-Ti were processed at room temperature using the dies with channel angles of 90° and 120°, respectively. First, each billet was processed 4 passes by ECAP using a die with an angle of 120° and a ram speed of 0.5mm s-1. And in order to eliminate residual stress, immediate annealing at 473 K for an hour was conducted between two adjacent passes. Second, CP-Ti was successfully processed by ECAP for up to 8 passes using the same die and a ram speed of 2 mm s-1 by controlling the flow of metal. Finally, CP-Ti was successfully achieved using a conventional die with an angle of 90° between the channels at room temperature. Each billet was processed for two passes with a ram speed of 26 mm s-1. These experiments show that CP-Ti may be processed by ECAP at room temperature and special attention was paid on improvements in the yield stress, ultimate strength and micro-hardness of ECAPed-Ti that are slightly higher than the improvements attained after pressing at elevated temperatures.

scholarly journals Synthesis and Characterization of Commercial Pure Titanium-nickel Alloy Behavior Reinforced With Titanium Diboride

2020 ◽  
Author(s):  
O.E. Falodun ◽  
Samuel R Oke ◽  
Peter A Olubambi
Keyword(s):  
Nickel Alloy ◽  
Titanium Diboride ◽  
Wear Behavior ◽  
Pure Titanium ◽  
Alpha Phase ◽  
Commercially Pure Titanium ◽  
Wear Properties ◽  
Commercial Pure Titanium ◽  
Plasma Sintering ◽  
Titanium Nickel

Abstract Commercial pure titanium alloy with Ni-TiB2 ceramic additions (5, 10, 15 and 20 vol.%) were synthesized through the spark plasma sintering approach with sintering temperature of 1000 oC, the heating rate of 100 oC/min, holding time of 5 min at a constant pressure of 50 MPa. The study investigated the effect of Ni-TiB2 on the densification, phase change, microhardness, microstructure, and wear properties of the sintered titanium-based composites. Results showed that Ti-Ni-TiB2 composites relative density ranges from 97 to 99 %, while microhardness values increase with addition of nickel and titanium diboride from 228 to 587 HV0.1. The microstructural evolution shows that pure titanium transformed from lamellar phase to equiaxed alpha phase upon addition of nickel alloy and further get refined with a distinct grain boundary comprises of titanium diboride around the boundaries. The average coefficient of friction for the titanium-based composite was higher for commercially pure titanium (0.73) while the addition of TiB2 exhibit (0.66, 0.63, 0.58, 0.55 and 0.46 respectively) improvement in the wear behavior.

TiC/Ti Composite Layers Fabricated by Laser Surface Alloying

2007 ◽  
Vol 336-338 ◽  
pp. 1148-1150
Author(s):  
Jian Bin Zhang ◽  
Ding Fan ◽  
Jing Jie Dai ◽  
Yao Ning Sun
Keyword(s):  
Continuous Wave ◽  
Composite Layer ◽  
Pure Titanium ◽  
Surface Hardness ◽  
Laser Surface ◽  
Commercially Pure Titanium ◽  
Surface Alloying ◽  
Micro Hardness ◽  
Laser Surface Alloying ◽  
Commercially Pure

Laser surface alloying is an attractive processing to improve surface hardness, wear and corrosion resistance. In this paper, a continuous wave CO2 laser was used to irradiate commercially pure titanium surface with pre-placed active carbon powders in argon atmosphere. A compact, well-adherent, and crack-free TiC/Ti composite layer was obtained. The microstructure and phase constitution of the alloyed layers were determined and analyzed, and the micro-hardness was measured. The result of X ray diffraction (XRD) analysis shows that the alloyed layers contain TiC and Ti (martensite). The scanning electron microscopy (SEM) observation shows TiC growth morphologies have a well-developed dendrite, cellular dendrite, globular microstructure and cross-petal microstructure. The mechanism of the formation of titanium carbides is discussed. Micro-hardness of the laser surface alloyed layer was improved to 420 Hv as compared to 200 Hv of the as-received commercially pure titanium.

scholarly journals Comparison of Biocompatible Coatings Produced by Plasma Electrolytic Oxidation on cp-Ti and Ti-Zr-Nb Superelastic Alloy

Coatings ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 401
Author(s):  
Ruzil Farrakhov ◽  
Olga Melnichuk ◽  
Evgeny Parfenov ◽  
Veta Mukaeva ◽  
Arseniy Raab ◽  
...  
Keyword(s):  
Plasma Electrolytic Oxidation ◽  
Electrochemical Impedance ◽  
Pure Titanium ◽  
Commercially Pure Titanium ◽  
X Ray ◽  
Kinetic Coefficients ◽  
Electrolytic Oxidation ◽  
Plasma Electrolytic ◽  
Cp Ti ◽  
Peo Coatings

The paper compares the coatings produced by plasma electrolytic oxidation (PEO) on commercially pure titanium and a novel superelastic alloy Ti-18Zr-15Nb (at. %) for implant applications. The PEO coatings were produced on both alloys in the identical pulsed bipolar regime. The properties of the coatings were examined using scanning electron microscopy (SEM), X-ray diffraction (XRD), and energy-dispersive X-ray spectroscopy (EDX), potentiodynamic polarization (PDP), and electrochemical impedance spectroscopy (EIS). The PEO process kinetics was modeled based on the Avrami theorem and Cottrell equation using a relaxation method. The resultant coatings contain TiO2, for both alloys, and NbO2, Nb2O5, ZrO2 for Ti-18Zr-15Nb alloy. The coating on the Ti-18Zr-15Nb alloy has a higher thickness, porosity, and roughness compared to that on cp-Ti. The values of the kinetic coefficients of the PEO process—higher diffusion coefficient and lower time constant for the processing of Ti-18Zr-15Nb—explain this effect. According to the electrochemical studies, PEO coatings on Ti-18Zr-15Nb alloy provide better corrosion protection. Higher corrosion resistance, porosity, and roughness contribute to better biocompatibility of the PEO coating on Ti-18Zr-15Nb alloy compared to cp-Ti.

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