Hot Workability Map for Near-α Titanium Alloy Ti-5.6Al-4.8Sn-2Zr-1Mo-0.35Si-0.7Nd

2012 ◽  
Vol 482-484 ◽  
pp. 1453-1456
Author(s):  
Ming Man Li ◽  
Qui Jian Xun ◽  
Shang Zhou Zhang

The characterizations of hot working behavior of a near-α titanium alloy using the approach of processing maps are described. Processing map in the α+β region exhibit a domain of the globularization process of lamellar structure and α dynamic recrystallization with a power dissipation efficiency of 0.6-0.9. In the β region the map exhibited a domain centered around 1060°C and 0.1 s-1with a power dissipation efficiency of 0.76 where the β phase undergoes dynamic recrystallization. At higher strain rate flow instability occurs in the α+β region due to adiabatic shear bands formation as well as in the β region due to flow inhomogeneity of β phase.

2011 ◽  
Vol 399-401 ◽  
pp. 1870-1877
Author(s):  
Gao Sheng Fu ◽  
Wen Duan Yan ◽  
Hong Ling Chen ◽  
Gui Qing Chen ◽  
Chao Zeng Cheng

Based on the theory of processing map proposed by PRASAD, the power dissipation maps, the hot deformation instability maps and the hot processing maps of 1235 Al alloys treated by different methods of purification were built, and the effects of purification and deformation conditions at elevated-temperature on hot workability of 1235 Al alloy were analyzed. At the same time the optimum processing region and flow instability region were determined. The results show that the hot processing map of 1235 Al alloy has two instability zones in the temperature range of 300-500°C and in the strain rate ranging from 0.01s-1to 10.0s-1up to a true strain of 0.7, that is, one zone lying in the range of lower temperature and higher strain rate, the other zone in the range of higher temperature and mid strain rate. The purification effect has significant impact on hot workability of the alloy. It is found that the optimum processing region of 1235 Al alloy treated by high-efficient purification treatment is present in the range of higher temperature and lower strain rate zone, and its power dissipation efficiency is about 46%; while the optimum processing region of 1235 Al alloys treated by conventional refining treatment is present in the range of mid-temperature and lower strain rate zone or in the range of higher temperature and strain rate zone, and its power dissipation efficiency is about 23-29%. The results of observation of the deformation microstructure of 1235 Al alloy are in accordance with that of the hot processing maps of the alloy, thus showing that the calculation results of the hot processing maps are reliable.


Processes ◽  
2021 ◽  
Vol 9 (3) ◽  
pp. 451
Author(s):  
Yexin Jiang ◽  
Xu Wang ◽  
Zhou Li ◽  
Zhu Xiao ◽  
Xiaofei Sheng ◽  
...  

The hot deformation behavior of Cu-20.0Ni-5.0Sn-0.25Zn-0.22Mn was investigated using a Gleeble-3500 thermal simulator with a temperature range from 720 °C to 880 °C and a strain rate range from 0.001 s−1 to 1 s−1. The results show that the flow stress increased with the increase of the strain rate and the decrease of the temperature. The constitutive equation of the alloy was established based on the peak flow stress. Figures of the power dissipation efficiency and flow instability with the variable of the true strain from 0.2 to 0.8 displayed the dynamic change of power dissipation efficiency and the instability area. The domain of 730–770 °C and 0.001–0.01 s−1 possessed a power dissipation efficiency over 40% throughout the whole deformation. The flow instability always appeared at a high strain rate from 0.1 s−1 to 1 s−1 during the whole deformation process. The nucleation site of the dynamic recrystallization generally appeared along the grain boundaries, indicating the discontinuous dynamic recrystallization mechanism. The appropriate conditions for deformation with a true strain of 0.9 is in a safe domain (820–860 °C with a strain rate of 0.001–0.01 s−1). There were four kinds of variation tendencies of the power dissipation efficiency with the increase of the true strain under various conditions, suggesting a changing situation for the main softening mechanisms.


2014 ◽  
Vol 906 ◽  
pp. 254-258
Author(s):  
Yan Hui Liu ◽  
Ze Kun Yao ◽  
Yong Quan Ning ◽  
Hong Zhen Guo ◽  
Zhang Long Zhao

Isothermal compression tests were carried out on Ti-6.0Al-7.0Nb biomedical titanium alloy at the temperatures of 750900°C (all below β phase transition temperature about 1010°C) and strain rates of 0.0011.0s-1. The processing maps were constructed to evaluate the efficiency of power dissipation (η) and recognize the flow instability regimes. True strain takes great effect on the efficiency of power dissipation η under the different temperatures and strain rates. The value of power dissipation η increases from 0.1 to 0.7 in most areas. When the strain is 0.9, the value of power dissipation η in most regimes is from 30% to 40%. There are two instability regimes respectively located around 780°C/1.0s-1 and 860-900°C/0.001-0.01s-1 when the strains are below 0.5. One of the instability regimes disappears when the strains are 0.5-0.7. When the strain is 0.9, there are still two instability regimes. The safe regime located around 780-840°C/0.1-0.01s-1, and hot deformation can be carried out in this area.


2013 ◽  
Vol 750-752 ◽  
pp. 721-724 ◽  
Author(s):  
Yan Chun Zhu ◽  
Wei Dong Zeng ◽  
Yong Qing Zhao ◽  
Wen Wen Peng

The damage and fracture behavior was researched in hot compression of as-cast Ti40 titanium alloy with single β phase. The main fracture modes consist of 45° shear fracture, inner cracking and longitudinal fracture on free-surface, which occur at 850°C/10s-1, 900~950°C/10s-1 and other deformation conditions respectively. Moreover, 45° transgranular cracking is the combination result of adiabatic shear bands due to local temperature rise and shear stress, the inner intergranular cracking is induced by the microvoids near the adiabatic shear bands propagted along grain boundry under shear stress, the surface longitudinal intergranular cracking is caused by the vaporization of oxide and function of hoop tensile stress. In addition, the material undergoes the complex fracture which has to be avoided or decreased in hot processing for obtaining satisfactory properties.


Metals ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 789
Author(s):  
Qiang Fu ◽  
Wuhua Yuan ◽  
Wei Xiang

In this study, isothermal compression tests of TB18 titanium alloy were conducted using a Gleeble 3800 thermomechanical simulator for temperatures ranging from 650 to 880 °C and strain rates ranging from 0.001 to 10 s−1, with a constant height reduction of 60%, to investigate the dynamic softening mechanisms and hot workability of TB18 alloy. The results showed that the flow stress significantly decreased with an increasing deformation temperature and decreasing strain rate, which was affected by the competition between work hardening and dynamic softening. The hyperbolic sine Arrhenius-type constitutive equation was established, and the deformation activation energy was calculated to be 303.91 kJ·mol−1 in the (α + β) phase zone and 212.813 kJ·mol−1 in the β phase zone. The processing map constructed at a true strain of 0.9 exhibited stability and instability regions under the tested deformation conditions. The microstructure characteristics demonstrated that in the stability region, the dominant restoration and flow-softening mechanisms were the dynamic recovery of β phase and dynamic globularization of α grains below transus temperature, as well as the dynamic recovery and continuous dynamic recrystallization of β grains above transus temperature. In the instability region, the dynamic softening mechanism was flow localization in the form of a shear band and a deformation band caused by adiabatic heating.


Author(s):  
Munir Al-Saadi ◽  
Christopher Hulme-Smith ◽  
Fredrik Sandberg ◽  
Pär G. Jönsson

AbstractAlloy 825 is a nickel-based alloy that is commonly used in applications where both high strength and corrosion resistance are required, such as tanks in the chemical, food and petrochemical industries and oil and gas pipelines. Components made from Alloy 825 are often manufactured using hot deformation. However, there is no systematic study to optimise the processing conditions reported in literature. In this study, a processing map for as-cast Alloy 825 is established to maximise the power dissipation efficiency of hot deformation in the temperature range of 950 to 1250 °C at an interval of 50 °C and strain rate range of $$0.01\, {\text{s}}^{ - 1}$$ 0.01 s - 1 to $$10.0\, {\text{s}}^{ - 1}$$ 10.0 s - 1 to a true strain of $$0.7$$ 0.7 using a Gleeble-3500 thermomechanical simulator. The processing conditions are also correlated to the Vickers hardness of the final material, which is also characterised using optical microscopy and scanning electron microscopy, including electron backscattered diffraction. The true stress-true strain curves exhibit peak stresses followed by softening due to occurrence of dynamic recrystallization. The activation energy for plastic flow in the temperature range tested is approximately $$450\,{\text{ kJ mol}}^{ - 1}$$ 450 kJ mol - 1 , and the value of the stress exponent in the (hyperbolic sine-based) constitutive equation, $$n = 5.0$$ n = 5.0 , suggests that the rate-limiting mechanism of deformation is dislocation climb. Increasing deformation temperature led to a lower Vickers hardness in the deformed material, due to increased dynamic recrystallization. Raising the strain rate led to an increase in Vickers hardness in the deformed material due to increased work hardening. The maximum power dissipation efficiency is over $$35\%$$ 35 % , obtained for deformation in the temperature range 1100-1250 °C and a strain rate of $$0.01\, {\text{s}}^{ - 1}$$ 0.01 s - 1 -$$0.1\, {\text{s}}^{ - 1}$$ 0.1 s - 1 . These are the optimum conditions for hot working.


Metals ◽  
2021 ◽  
Vol 11 (10) ◽  
pp. 1630
Author(s):  
Ke Wang ◽  
Yongqing Zhao ◽  
Weiju Jia ◽  
Silan Li ◽  
Chengliang Mao

Isothermal compressions of as-cast near-α Ti90 titanium alloy were carried out on a Gleeble-3800 simulator in the temperature range of 860–1040 °C and strain rates of 0.001–10 s−1. The deformation behavior of the alloy was characterized based on the analyses of flow curves, the constructions of Arrhenius constitutive equations and the processing map. The microstructure evolution of the alloy was analyzed using the optical microscopic (OM), transmission electron microscope (TEM), and electron backscatter diffraction (EBSD) techniques. The results show that the kinking and dynamic globularization of α lamellae is the dominant mechanism of flow softening in the α + β two-phase region, while the dynamic recovery (DRV) of β phase is the main softening mechanism in the β single-phase region. The dynamic globularization of α lamellae is mainly caused by the wedging of β phase into α laths and the shearing of α laths due to imposed shear strain. The activation of prismatic and pyramidal slip is found to be easier than that of basic slip during the deformation in the α + β two-phase region. In addition, the Schmid factor of equiaxial α is different from that of lamellar α, which also varies with the angle between its geometric orientation and compression direction (CD). Based on the processing map, the low η region within the temperature range of 860–918 °C with a strain rate range of 0.318–10 s−1 should be avoided to prevent the occurrence of deformation instability.


Author(s):  
Amir Hosein Sheikhali ◽  
Maryam Morakkabati

Abstract In this study, hot deformation behavior of SP-700 titanium alloy was investigated by hot compression tests in the temperature range of 700-9508C and at strain rates of 0.001, 0.1, and 1 s-1. Final mechanical properties of the alloy (hot compressed at different strain rates and temperatures) were investigated using a shear punch testing method at room temperature. The flow curves of the alloy indicated that the yield point phenomenon occurs in the temperature range of 800- 9508C and strain rates of 0.1 and 1 s-1. The microstructural analysis showed that dynamic globularization of the lamellar α phase starts at 7008C and completes at 8008C. The alpha phase was completely eliminated from b matrix due to deformation- induced transformation at 8508C. The microstructure of specimens compressed at 8508C and strain rates of 0.001 and 0.1 s-1showed the serration of beta grain boundaries, whereas partial dynamic recrystallization caused a necklace structure by increasing strain rate up to 1 s-1. The specimen deformed at 7008C and strain rate of 1 s-1was located in the instability region and localized shear bands formed due to the low thermal conductivity of the alloy. The processing map of the alloy exhibited a peak efficiency domain of 54% in the temperature range of 780-8108C and strain rates of 0.001- 0.008 s-1. The hot deformation activation energy of the alloy in the α/β region (305.5 kJ mol-1) was higher than that in the single-phase β region (165.2 kJ mol-1) due to the dynamic globularization of the lamellar a phase.


2018 ◽  
Vol 941 ◽  
pp. 1391-1396 ◽  
Author(s):  
Nitish Bibhanshu ◽  
Satyam Suwas

The hot workability of gamma titanium aluminide alloy, Ti-48Al-2V-2Nb, was assessed in the cast condition through a series of compression tests conducted over a range of temperatures (1000 to 1175 °C) and at the strain rate of 10 S-1. The mechanism of dynamics recrystallization has been investigated from SEM Z-contrast images and from the Electron backscattered diffraction EBSD as well. It has been observed that volume fraction of the recrystallized grains increases with increasing the deformation temperature. The major volume fraction of the recrystallized grains was observed in the shear band which was forming at an angle 45 ̊ with respect to the compression direction. The mechanism of breaking of the laths and the region of the dynamic recrystallization were also investigated from the SEM Z-contrast image and EBSD. The dynamic recrystallization occurred in the region of the broken laths and shear bands. The breaking of the laths was because of the kinking of the lamellae. The shear band, kinked lamellae and dynamic recrystallized region where all investigated simultaneously.


Materials ◽  
2020 ◽  
Vol 13 (16) ◽  
pp. 3623 ◽  
Author(s):  
Danying Zhou ◽  
Hua Gao ◽  
Yanhua Guo ◽  
Ying Wang ◽  
Yuecheng Dong ◽  
...  

A self-designed Ti-35421 (Ti-3Al-5Mo-4Cr-2Zr-1Fe wt%) titanium alloy is a new type of low-cost high strength titanium alloy. In order to understand the hot deformation behavior of Ti-35421 alloy, isothermal compression tests were carried out under a deformation temperature range of 750–930 °C with a strain rate range of 0.01–10 s−1 in this study. Electron backscatter diffraction (EBSD) was used to characterize the microstructure prior to and post hot deformation. The results show that the stress–strain curves have obvious yielding behavior at a high strain rate (>0.1 s−1). As the deformation temperature increases and the strain rate decreases, the α phase content gradually decreases in the α + β phase region. Meanwhile, spheroidization and precipitation of α phase are prone to occur in the α + β phase region. From the EBSD analysis, the volume fraction of recrystallized grains was very low, so dynamic recovery (DRV) is the dominant deformation mechanism of Ti-35421 alloy. In addition to DRV, Ti-35421 alloy is more likely to occur in continuous dynamic recrystallization (CDRX) than discontinuous dynamic recrystallization (DDRX).


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